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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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All sourcesNASA NTRSDOE OSTI
NASA NTRS2004

Passive Acoustic Tomography Tested for Measuring Gas Temperatures

The requirements of higher performance, better fuel economy, and lower emissions place an increasing premium on knowing the internal operating parameters of jet engines. One of the most important is the gas temperature in the post combustor section of the engine. Typically the gas temperature is measured with a thermocouple probe or by some optical technique such as Rayleigh scattering. Probes, while providing valuable information, have several limitations. The probe signal must be corrected for radiation and conduction losses, probes provide only a point measurement, and probes must be constructed of materials whose melting points are lower than the temperature of the environment into which they are inserted. Some of the disadvantages of probes are overcome by various optical techniques. Nothing needs to be inserted into the flow, and the temperature can be directly related to the signal by known physical laws. However, optical techniques require optical access (i.e., a window) and a light source (such as a laser), and they are very sensitive to the presence of particles in the flow. To overcome these problems, researchers from the NASA Glenn Research Center and The University of Nevada are developing a technique that uses sound instead of light to measure gas temperature. Like optical techniques, it is nonintrusive--no probe need be exposed to the combustion environment--and the temperature is directly related to a measured quantity--the speed of sound, which is proportional to the square root of the absolute temperature. The temperature profile inside the engine is constructed from the differences in arrival time between correlated signals from an array of microphones placed around the circumference of the engine. In much the same way as a complete picture of the inside of your body can be constructed from an array of x-ray photographs taken at different angles, the temperature profile in the engine is constructed from the angular array of microphones. It is tomography by sound waves. Active acoustic tomography, in which a sound pulse is injected into the flow and the time delays between members of an array of microphones are used to construct the temperature field has been used successfully in the stacks of power plants. However, the flow field inside a jet engine is much too noisy for it to be possible to detect an externally injected sound pulse. Instead we are developing passive acoustic tomography, which uses the sound already present in the flow.

Fralick, Gustave C.↗
DOE OSTI2023

Structure of metallochaperone in complex with the cobalamin-binding domain of its target mutase provides insight into cofactor delivery

G-protein metallochaperone MeaB in bacteria [methylmalonic aciduria type A (MMAA) in humans] is responsible for facilitating the delivery of adenosylcobalamin (AdoCbl) to methylmalonyl-CoA mutase (MCM), the only AdoCbl-dependent enzyme in humans. Genetic defects in the switch III region of MMAA lead to the genetic disorder methylmalonic aciduria in which the body is unable to process certain lipids. Here, we present a crystal structure of Methylobacterium extorquens MeaB bound to a nonhydrolyzable guanosine triphosphate (GTP) analog guanosine-5'-[(β,γ)-methyleno]triphosphate (GMPPCP) with the Cbl-binding domain of its target mutase enzyme (MeMCM cbl ). This structure provides an explanation for the stimulation of the GTP hydrolyase activity of MeaB afforded by target protein binding. We find that upon MCM cbl association, one protomer of the MeaB dimer rotates ~180°, such that the inactive state of MeaB is converted to an active state in which the nucleotide substrate is now surrounded by catalytic residues. Importantly, it is the switch III region that undergoes the largest change, rearranging to make direct contacts with the terminal phosphate of GMPPCP. These structural data additionally provide insights into the molecular basis by which this metallochaperone contributes to AdoCbl delivery without directly binding the cofactor. Our data suggest a model in which GTP-bound MeaB stabilizes a conformation of MCM that is open for AdoCbl insertion, and GTP hydrolysis, as signaled by switch III residues, allows MCM to close and trap its cofactor. Substitutions of switch III residues destabilize the active state of MeaB through loss of protein:nucleotide and protein:protein interactions at the dimer interface, thus uncoupling GTP hydrolysis from AdoCbl delivery.

59 BASIC BIOLOGICAL SCIENCES↗
NASA NTRS2000

Formal Analysis of the Remote Agent Before and After Flight

This paper describes two separate efforts that used the SPIN model checker to verify deep space autonomy flight software. The first effort occurred at the beginning of a spiral development process and found five concurrency errors early in the design cycle that the developers acknowledge would not have been found through testing. This effort required a substantial manual modeling effort involving both abstraction and translation from the prototype LISP code to the PROMELA language used by SPIN. This experience and others led to research to address the gap between formal method tools and the development cycle used by software developers. The Java PathFinder tool which directly translates from Java to PROMELA was developed as part of this research, as well as automatic abstraction tools. In 1999 the flight software flew on a space mission, and a deadlock occurred in a sibling subsystem to the one which was the focus of the first verification effort. A second quick-response "cleanroom" verification effort found the concurrency error in a short amount of time. The error was isomorphic to one of the concurrency errors found during the first verification effort. The paper demonstrates that formal methods tools can find concurrency errors that indeed lead to loss of spacecraft functions, even for the complex software required for autonomy. Second, it describes progress in automatic translation and abstraction that eventually will enable formal methods tools to be inserted directly into the aerospace software development cycle.

Havelund, Klaus↗
NASA NTRS2011

Tomographic Reconstruction of Mercury's Exosphere from MESSENGER Flyby Data

The exosphere of Mercury is among the best-studied examples of a common type of atmosphere, a surface-bounded exosphere. Mercury's exosphere was probed in 2008-2009 with Ultraviolet and Visible Spectrometer (UVVS) measurements obtained during three planetary flybys by the MErcury Surface, Space ENvironment, GEochemistry, and Ranging (MESSENGER) spacecraft [1-3]. The measurements detailed the distribution of two previously known metallic constituents of Mercury's exosphere, Na and Ca, and indicated the presence in the gas phase of yet another metallic species, Mg. Such measurements can answer fundamental scientific questions regarding the relative importance of possible source and loss processes for exospheric species ejected from a surface boundary [4]. The trajectory of MESSENGER during the last of its three flybys provided the best spatial coverage prior to orbit insertion. The measurements by MESSENGER of Na, Ca, and Mg during the third flyby have been analyzed with a novel tomographic method. This approach maximizes the amount of information that can be extracted from line-of-sight measurements because it yields three-dimensional distributions of neutrals consistent with the data.

Killen, Rosemary M.↗
DOE OSTI2022

A Novel Anatomic Reconstruction for Posterior Tibialis Tendon in Treatment of Flexible Adult‐Acquired Flatfoot Deformity

Objective To present a novel approach for the anatomic reconstruction of the posterior tibialis tendon (PTT) in restoring plantar insertions and evaluate its efficiency in treating flexible adult‐acquired flatfoot deformity (AAFD) caused by PTT dysfunction. Methods For AAFD treatment, a novel PTT reconstruction method was presented. The current study involved 16 patients, including three men, and 13 women, from August 2017 to July 2019. The mean age was 43.2 ± 15.1 years (21–64 years). The innovative PTT repair method was used on all patients. The treatment involved performing a traditional Flexor Digitorum Longus (FDL) transfer in the navicular tuberosity and suturing the plantar insertions to FDL as tension was applied to tighten the plantar structures of the foot. The results were retrospectively analyzed. The clinical outcome was assessed using the pain visual analogue scale (VAS), the satisfaction VAS, and the American Orthopedic Foot and Ankle Society ankle–hindfoot scale (AOFAS‐AH). Isokinetic testing was performed using a dynamometer at 60°/s and 120°/s for inversion/eversion and plantarflexion/dorsiflexion, respectively, to determine the mean peak torque. Radiographic measurements were employed to assess the outcomes. Results Bone surgeries combined with the modified anatomic PTT reconstruction were performed on patients with medializing calcaneal osteotomy in 12 (75%) patients and subtalar joint fusion in four (25%) patients. The branch linking to the plantar insertions was detected in every case, with an average width of 3.5 ± 0.8 mm (3.1–4.3 mm). All patients were followed up for the mean of 16.8 ± 1.8 months (range, 15–20 months). The average postoperative functional scores, including pain VAS, satisfaction VAS, total AOFAS‐AH, and all AOFAS‐AH sub‐scales, steadily improved during the follow‐up. In the last follow‐up, isokinetic testing revealed no loss of plantarflexion strength ( p = 0.350 and 0.098) and significant improvement in the inversion strength ( p = 0.007 and 0.008) in the operated ankles at 60°/s and 120°/s. Radiographic outcomes, particularly the talar head uncovering, improved significantly after more than a year ( p < 0.001 for all). Conclusions The novel technique for PTT reconstruction in restoring the plantar insertions serves as an effective procedure in treating AAFD caused by PTT dysfunction in terms of delivering a consistent improvement in ankle inversion strength, medial longitudinal arch restoring, and satisfactory clinical outcomes.

Hu, Yong↗
DOE OSTI2025

Effect of cell compression on the performance and the structure of proton exchange membrane water electrolyzer (PEMWE) assembly

Here, in the field of water electrolysis, the proton exchange membrane water electrolyzer (PEMWE) is currently the most advanced technology for producing hydrogen without emitting CO 2 . Although PEMWE plants are already in operation, further research is needed to improve cell efficiency and reduce the use of rare materials, such as iridium oxide catalysts for the oxygen evolution reaction (OER). One of the main causes of performance loss in PEMWE is the relatively low electric conductivity of the porous transport layer (PTL) and of the anode catalyst layer, which results in ohmic losses and low catalyst utilization during high current density operation. The objective of this study is to investigate how optimization of the PTL and electrode interface can increase the cell performance. To this end, we tested different cell assemblies using fibrous and sintered PTLs, decreasing membrane thickness, reducing iridium loading, and inserting a microporous layer to increase contact surface area. Electrochemical characterization of each cell configuration was systematically performed at various compression levels as the pressure is a crucial parameter influencing the electrode/PTL contact area. In parallel, X-ray microcomputed tomography (micro-CT) was employed to investigate the effects of cell hydration and compression on the structure of PEMWE components. This study combining electrochemistry and micro-CT imaging presents how optimizing the electrode/PTL contact surface area, minimizes ohmic losses, and enables PEMWE operation with low iridium loading at high current densities.

Catalyst - PTL interface↗
DOE OSTI2025

Physical and thermal property changes under uniform oxidation in nuclear graphite

Material property changes of fine- and medium-grain nuclear graphite grades were measured after subjection to uniform oxidation. The cores of high temperature reactors are composed of large nuclear graphite block components. Here, these large core components are designed to provide neutron moderation and reflection, create a large thermal sink to assist in operational control, and form the solid core structure containing the nuclear fuel, coolant channels, and the safety critical channels for control rod insertion. Oxidation is a principle degradation mechanism affecting all aspects of the nuclear graphite component functions. This study addresses the underlying physical property changes of nuclear-graphite components for oxidized mass loss ranges beyond the current recommended ASME code rule limits to ensure structural integrity within the graphite components (a maximum mass loss = 10%).

11 - NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗
DOE OSTI2024

Simultaneous Solid Electrolyte Deposition and Cathode Lithiation for Thin Film Batteries and Lithium Iontronic Devices

Here we show that the deposition of the solid-state electrolyte LiPON onto films of V 2 O 5 leads to their uniform lithiation of up to 2.2 Li per V 2 O 5 , without affecting the Li concentration in the LiPON and its ionic conductivity. Our results indicate that Li incorporation occurs during LiPON deposition, in contrast to earlier mechanisms proposed to explain postdeposition Li transfer between LiPON and LiCoO 2 . We use our discovery to demonstrate symmetric thin film batteries with a capacity of >270 mAh/g, at a rate of 20C, and 1600 cycles with only 8.4% loss in capacity. We also show how autolithiation can simplify fabrication of Li iontronic transistors attractive for emerging neuromorphic computing applications. Our discovery that LiPON deposition results in autolithiation of the underlying insertion oxide has the potential to substantially simplify and enhance the fabrication process for thin film solid state Li ion batteries and emerging lithium iontronic neuromorphic computing devices.

25 ENERGY STORAGE↗
DOE OSTI2024

CRISPR-prime editing, a versatile genetic tool to create specific mutations with a single nucleotide resolution in Leptospira

ABSTRACT Leptospirosis, caused by pathogenic bacteria from the genusLeptospira, is a global zoonosis responsible for more than one million human cases and 60,000 deaths annually. The disease also affects many domestic animal species. Historically, genetic manipulation ofLeptospirahas been difficult to perform, resulting in limited knowledge on pathogenic mechanisms of disease and the identification of virulence factors. The application of CRISPR/Cas9 and its variations have helped fill these gaps but the generation of knockout mutants remains challenging because double-strand breaks (DSBs) inflicted by Cas9 nuclease are lethal toLeptospiracells. The novel CRISPR prime editing (PE) strategy is the first precise genome-editing technology that allows deletions, insertions, and base substitutions without introducing DSBs. This revolutionary technique utilizes a nickase Cas9 that cleaves a single strand of DNA, coupled with an engineered reverse transcriptase and a modified single-guide RNA (termed prime editing guide RNA) containing an extended 3′ end with the desired edits. We demonstrate the application of CRISPR-PE in both saprophytic and pathogenicLeptospirafrom multiple species and serovars by introducing deletions or insertions into target DNA with a remarkable precision of just one nucleotide. Additionally, we demonstrate the ability to genetically manipulateLeptospira borgpetersenii, a prevalent pathogenic species of humans, domestic cattle, and wildlife animals. Rapid plasmid loss by mutated strains in liquid culture allows for the generation of knockout strains without selective markers, which can be readily used to elucidate virulence factors and develop optimized bacterin and/or live vaccines against leptospirosis. IMPORTANCE Leptospirosis is a geographically widespread bacterial zoonosis. Genetic manipulation of pathogenicLeptospiraspp. has been laborious and difficult to perform, limiting our ability to understand how leptospires cause disease. The application of the CRISPR/Cas9 system toLeptospiraenhanced our ability to generate knockdown and knockout mutants; however, the latter remains challenging. Here, we demonstrate the application of the CRISPR prime editing technique inLeptospira, allowing the generation of knockout mutants in several pathogenic species, with mutations comprising just a single nucleotide resolution. Notably, we generated a mutant in theLeptospira borgpeterseniibackground, a prevalent pathogenic species of humans and cattle. Our application of this method opens new avenues for studying pathogenic mechanisms ofLeptospiraand the identification of virulence factors across multiple species. These methods can also be used to facilitate the generation of marker-less knockout strains for updated and improved bacterin and/or live vaccines.

Microbiology↗
NASA NTRS1992

Noncontact Measurement Of Critical Current In Superconductor

Critical current measured indirectly via flux-compression technique. Magnetic flux compressed into gap between superconductive hollow cylinder and superconductive rod when rod inserted in hole in cylinder. Hall-effect probe measures flux density before and after compression. Method does not involve any electrical contact with superconductor. Therefore, does not cause resistive heating and consequent premature loss of superconductivity.

Israelsson, Ulf E.↗
NASA NTRS2012

JUNO Photovoltaic Power at Jupiter

This paper summarizes the Juno modeling team work on predicting the Juno solar array performance at critical mission points including Juno Orbit Insertion (JOI) and End of Mission (EOM). This report consists of background on Juno solar array design, a summary of power estimates, an explanation of the modeling approach used by Aerospace, a detailed discussion of loss factors and performance predictions, a thermal analysis, and a review of risks to solar array performance

solar powered mission↗
DOE OSTI2023

Insertion reactions and structural studies of [(NHC)CuH] 2 with nitrogen-based substrates

The stoichiometric and catalytic reactions of Cu-H dimers supported by N-heterocyclic carbenes (NHCs) have mainly focused on the insertions of aldehydes, ketones, CO 2 , and unsaturated hydrocarbons. Here we investigated the stoichiometric reactions of dimeric [(NHC)CuH] 2 (NHC = IPr*, 6Dipp) with unsaturated nitrogen-based substrates of PhN=NPh, N 3 Ad, pyrazine, and N 2 O. The spectroscopic and structural chacterizations of the resulting monomeric, two-coordinate Cu(I) complexes containing diphenyl hydrazido, triazenido, pyrazinyl, and hydroxide ligands are discussed. The hydrazido complex of (IPr*)Cu(NPh-NHPh) and triazenido complex of (IPr*)Cu(HNNNAd) are resistant to N—N bond cleavage and loss of N 2 , respectively, to form the corresponding amido complexes even when heated at 80 °C over several hours.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2025

Asymmetrical cavity design that bypasses mode mixings in axion haloscope experiments

Microwave cavities used in axion haloscope experiments typically employ a tuning rod as a means to widen the range of resonance frequencies at which it is sensitive to axion-to-photon conversion. A realistic tuning mechanism requires a gap between the cavity end caps and the tuning rod to ensure movement, and causes some modes to hybridize with the resonant mode that is being tracked for the experiment. These so-called mode mixings lead to gaps in the frequency range that practically lose sensitivity to axions. Here, to solve this problem, we present a cavity design which, for two tuning rod configurations corresponding to a lower and higher frequency range, have a dielectric rod inserted at a specific location that makes the cavity asymmetrical. Moving the tuning rod closer to the dielectric insert changes the location and frequency of the mode mixing compared to when it is farther away from it. This design is easily realizable in practical experiments and makes possible an axion dark matter search with minimal loss in sensitivity due to mode mixings. We also show that the same design has the same desired effect when cavity dimensions are scaled down to be smaller and are at higher resonance frequencies.

Axion↗
NASA NTRS1987

Polyphase alloys as rechargeable electrodes in advanced battery systems

The rechargeability of electrochemical cells is often limited by negative electrode problems. These may include loss of capacity, increased impedance, macroscopic shape change, dendrite growth, or a tendency for filamentary or whisker growth. In principle, these problems can be reduced or eliminated by the use of alloys that undergo either displacement or insertion reactions at reactant species activities less than unity, rather than pure elements. The fundamental reasons for some of these problems with elemental electrodes, as well as the basic principles involved in the different behavior of alloys, are briefly discussed. More information is now available concerning the thermodynamic and kinetic properties of a number of alloys of potential interest for use as electrodes in elevated temperature lithium battery systems. Recent results have extended these results down to ambient temperatures, indicating that some such materials may be of interest for use with new low temperature molten salt electrolytes, or with organic solvent electrolytes. The all solid mixed conductor matrix concept is also reviewed.

Huggins, Robert A.↗
NASA NTRS2010

Implementation of an Autonomous Multi-Maneuver Targeting Sequence for Lunar Trans-Earth Injection

Using a fully analytic initial guess estimate as a first iterate, a targeting procedure that constructs a flyable burn maneuver sequence to transfer a spacecraft from any closed Moon orbit to a desired Earth entry state is developed and implemented. The algorithm is built to support the need for an anytime abort capability for Orion. Based on project requirements, the Orion spacecraft must be able to autonomously calculate the translational maneuver targets for an entire Lunar mission. Translational maneuver target sequences for the Orion spacecraft include Lunar Orbit Insertion (LOI), Trans-Earth Injection (TEI), and Trajectory Correction Maneuvers (TCMs). This onboard capability is generally assumed to be supplemental to redundant ground computation in nominal mission operations and considered as a viable alternative primarily in loss of communications contingencies. Of these maneuvers, the ability to accurately and consistently establish a flyable 3-burn TEI target sequence is especially critical. The TEI is the sole means by which the crew can successfully return from the Moon to a narrowly banded Earth Entry Interface (EI) state. This is made even more critical by the desire for global access on the lunar surface. Currently, the designed propellant load is based on fully optimized TEI solutions for the worst case geometries associated with the accepted range of epochs and landing sites. This presents two challenges for an autonomous algorithm: in addition to being feasible, the targets must include burn sequences that do not exceed the anticipated propellant load.

Whitley, Ryan J.↗
DOE OSTI2025

Lattice Refinements for Nonlinear Integrable Optics in IOTA

Nonlinear integrable optics of the type proposed by Danilov and Nagaitsev place strict constraints on the lattice parameters in the matching section outside of the nonlinear insert. In particular, the effects of energy spread in the beam have significant effects on the stability of the system. Typical chromatic compensation using sextupoles has significant perturbative effects on the dynamics but is operationally necessary to suppress fast losses. Fast decoherence of kicked beam measurements limits the available signal for studies. Refinements to the IOTA lattice parameters based on this experience with electron beam operation are presented.

Wieland, John [Fermilab] (ORCID:0000000289718523)↗
DOE OSTI2025

Lattice refinements for nonlinear integrable optics in IOTA

Nonlinear integrable optics of the type proposed by Danilov and Nagaitsev place strict constraints on the lattice parameters in the matching section outside of the nonlinear insert. In particular, the effects of energy spread in the beam have significant effects on the stability of the system. Typical chromatic compensation using sextupoles has significant perturbative effects on the dynamics but is operationally necessary to suppress fast losses. Fast decoherence of kicked beam measurements limits the available signal for studies. Refinements to the IOTA lattice parameters based on this experience with electron beam operation are presented.

Wieland, J. [Fermilab; Michigan State U.] (ORCID:0↗
NASA NTRS1988

A 2.3-GHz low-noise cryo-FET amplifier

A cryogenic cooled, low-noise Field Effect Transistor (FET) amplifier assembly for use at 2.2 to 2.3 GHz was developed for the DSN to meet the requirements of a Very Long Baseline Interferometry (VLBI) upgrade. An amplifier assembly was developed at JPL that uses a commercial closed-cycle helium refrigerator (CCR) to cool a FET amplifier to an operating temperature of 15 K. A cooled probe waveguide-to-coaxial transition similar to that used in the research and development Ultra-Low-Noise S-band Traveling Wave Maser (TWM) is used to minimize input line losses. Typical performance includes an input flange equivalent noise contribution of 14.5 K, a gain slope of less than 0.05 dB/MHz across a bandwidth of 2.2 to 2.3 GHz, an input VSWR of 1.5:1 at 2.25 GHz, and an insertion gain of 45 + or - 1 dB across the bandwidth of 2.2 to 2.3 GHz. Three 2.3 GHz FET/CCR assemblies were delivered to the DSN in the spring of 1987.

Loreman, J.↗