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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 361 records · Page 20
All sourcesNASA NTRSDOE OSTI
NASA NTRS2018

Plasticity and Damage Modeling of Stress Asymmetry and Dynamic Behavior of AFS Additive Manufactured Aluminum Alloy 2219

The Solid State Additive Manufacturing (AM) process referred as MELD that fabricated the samples in this study, provides a new path for repairing, coating, joining and additive manufacturing metals and metal matrix composites. This research will be the first application of a physics-based microstructure dependent internal state variable (ISV) plasticity and damage material model to capture the mechanical response of an AM Aluminum Alloy (AA) 2219 via the MELD process. In this research, a microstructure-based internal state variable (ISV) plasticity-damage model was used to capture the mechanical behavior of AFS 2219 aluminum alloy. Aeroprobe Corporation, creator and patent holder for the MELD process, fabricated the material by pushing a solid filler rod of AA2219-T861 material through a hollow rotating tool onto an AA2219 T851 plate substrate. As feedstock, solid or powder precursor metals are pushed through a nonconsumable rotating cylindrical tool. Herein, added layers are deposited and metallurgically bonded to substrate material or previously deposited layers by the heat generated from the rotating tool through plastic deformation of the filler material. Once a layer has been added, the tool height increases, and starts the deposition of the next layer. This process results in beneficial properties such as grain refinement, homogenization and reduced porosity (fully dense). This process will experience temperatures similar to those in the weld nugget zone (WNZ) in friction stir welding (FSW), ranging from 0.6-0.9 Tm, with Tm being the melting point of the material. MELD is highly scalable with AA deposition rates reaching over 1000 cm3/hr, which allows for MELD being used for repairs, coatings, and building components. A motivating factor driving the research for physics-based history dependent material modeling of MELD components is the ability to accurately capture the stress-state and strain rate dependence in the material caused by variations in material microstructure from the MELD processing of new or repaired components. The ISV model incorporates microstructural content and is consistent with continuum level kinematics, kinetics, and thermodynamics. These features allow the ISV model to capture large deformations at the structural scale using the kinematic and isotropic hardening, while microscale damage is obtained from the microstructural features. The benefits of the ISV model arise from the inclusion of structure-property relationships identified from microstructural characterization and experimentation. The Bauschinger effect (BE) is an important concept, vital in the accurate prediction of cyclic stress-strain response of ductile materials such as metals. The ISV model has been successfully used to capture the behavior and damage, and the BE of different aluminum alloys and steels. The ISV model uses kinematic and isotropic hardening to help capture deformations of the material at the macro scale. To understand this hardening relationship, calculating the kinematic and isotropic hardening relationship in the material is warranted for a high-fidelity model. Electron Backscattered Diffraction (EBSD) was used to characterize the as-fabricated microstructure, where a fully-dense equiaxed grain morphology with average grain size of 2.5 μm was observed. Microhardness mapping of the as-built structures, monotonic tension and compression experiments at both quasi-static (0.001/s) strain rates, tension-followed-by-compression and compression-followed-by-tension experiments were performed to obtain the set of plasticity and damage constants necessary to capture strain rate and stress state behavior of this additive material. To calibrate the plasticity-damage model, a single set of constants were determined to capture the different stress states the MELD AA2219. One set of the constants was determined from experimental true stress-strain curves for the tension and compression data. Additionally, microstructural information and data from the open literature were used as the other model constants. This research is a first of its kind for AFS AA2219, includes correlating the ISV model to the monotonic experimental results that capture the isotropic and kinematic plasticity mechanical response.

Rivera, O. G.↗
DOE OSTI2022

Multi-state Catalysts Modulated by Mechanical Force (Final Report)

The development of more efficient catalytic processes and new approaches to control catalytic activity and selectivity are central to the realization of more selective, atom economic, and energy efficient routes to value added chemicals and polymers. The reactivity and selectivity of a transition metal catalyst is intimately related to the ligand-sphere geometry and, in many cases, the ideal ligand geometry for one step of a catalytic cycle is poorly matched to the ideal ligand geometry for another, resulting in sub-optimal efficiency. Macroscopic mechanical forces are both large, potentially much larger than interatomic forces, and are directional and localized to an extent that differentiates them from other forms of energy input such as heat or light. As such, mechanical force represents a heretofore untapped approach to modulate catalyst geometry, with the potential to reversibly modulate catalyst geometry on the timescale of catalytic turnover or monomer enchainment. This project has addressed the fundamental challenges in material-to-molecule strain coupling associated with the development of a new class of mechanically responsive catalysts (mechanocatalysts) in which active organotransition metal catalysts are strategically embedded in a flexible polymer network such that application of external mechanical force (stretching or deformation) leads to modulation of catalyst geometry, and hence reactivity and selectivity. Our efforts during the tenure of this grant were directed toward the elucidation of force-reactivity relationships of elementary transformations that occur within the first coordination sphere of a transition metal complex employing stiff stilbene photoswitches tethered to a flexible bidentate phosphine ligand derived from MeOBiphep as molecular force probes which provide a range of compressive and extension forces to the coupled transition metal complex depending on the geometry of the stiff stilbene and length of the tethering chains. During the tenure of this grant, we have quantified the rate of C(sp 2 )-C(sp 2 ) reductive elimination from platinum(II) diaryl complexes containing bis(phosphine) force probe ligands as a function of mechanical force; compressive forces decreased the rate of reductive elimination whereas extension forces increased the rate relative to the strain-free MeOBiphep complex with a 3.4-fold change in rate over a ~290 pN range of restoring forces. In a similar manner, we have quantified the rate of oxidative addition of bromobenzene to low-ligated palladium(0) complexes containing force probe ligands as a function of mechanical force; compressive forces increase the rate of oxidative addition, whereas tensile forces decrease the rate with a ~6 fold change in rate across ~340 pN of force applied to the complexes. In both cases, experimental and computational analyses argue strongly against any significant force-induced perturbation of ground state geometry within the first coordination sphere of the reactant complexes. Rather, the force/rate behavior observed for these transformations across these ranges of forces is attributed to the coupling of force to the nuclear motion comprising the reaction coordinates for reductive elimination and oxidative addition. These results together inform the development of catalysts whose activity can be tuned by an external force that is adjusted within a catalytic cycle and suggest opportunities to experimentally map geometry changes associated with reactions in transition metal complexes and potential strategies for force-modulated catalysis.

99 GENERAL AND MISCELLANEOUS↗
DOE OSTI2024

Revealing the unusual rate-dependent mechanical behaviors of nematic liquid crystal elastomers

Liquid crystal elastomers (LCEs) exhibit unique mechanical properties of soft elasticity and enhanced energy dissipation with rate dependency. They are potentially transformative materials for applications in mechanical impact mitigation and vibration isolation. However, previous studies have primarily focused on the mechanics of LCEs under equilibrium and quasistatic loading conditions. Critical knowledge gaps exist in understanding their rate-dependent behaviors, which are a complex mixture of traditional network viscoelasticity and the soft elastic behaviors with changes in the mesogen orientation and order parameter. Together, these inelastic mechanisms lead to unusual rate-dependent energy absorption responses of LCEs. In this work, we developed a viscoelastic constitutive theory for monodomain nematic LCEs to investigate how multiple underlying sources of inelasticity manifest in the rate-dependent and dissipative behaviors of monodomain LCEs. Here, the theoretical modeling framework combines the neo-classical network theory with evolution rules for the mesogen orientation and order parameter with conventional viscoelasticity. The model is calibrated with uniaxial tension and compression data spanning six decades of strain rates. The established 3D constitutive model enables general loading predictions taking the initial mesogen orientation and order parameter as inputs. Additionally, parametric studies were performed to further understand the rate dependence of monodomain LCEs in relation to their energy absorption characteristics. Based on the parametric studies, particularly loading scenarios are identified as conditions where LCEs outperform conventional elastomers regarding energy absorption.

42 ENGINEERING↗
DOE OSTI2022

Effect of laser scanning speed on the microstructure, phase transformation and mechanical property of NiTi alloys fabricated by $\mathrm{LPBF}$

This study investigated the effects of laser scanning speed on the microstructure, phase transformation and properties of NiTi alloys fabricated by laser powder bed fusion (LPBF). In this study, the contributions of metallurgical factors under different scanning speeds, such as Ni evaporation, Ni4Ti3 precipitation, dislocations and internal stress, to the transformation temperature and transformation latent heat were clarified through specially designed experiments. Ni evaporation is found to have the most profound effect, followed by precipitation. Increasing scanning speed is found to reduce Ni loss, thus cause less increase in the transformation temperature and transformation heat of the LPBF-NiTi alloys. Increasing scanning speed also increases the microstructure non-uniformity and thus widens the transformation temperature interval. The orientations of residual stress exhibit strong crystallographic stiffness dependence. The LPBF-NiTi alloys with different scanning speeds all exhibited high strains (>13.4%) and excellent shape memory effect. A LPBF-NiTi honeycomb structure exhibited 96% shape recovery rate after a 60% pre-compressive deformation. Besides, there is an optimum scanning speed for minimum porosity and smallest average pore size. However, the pore structure is found to have weak influence on the tensile behaviour of the LPBF-NiTi alloys, possibly due to the high defect tolerance of the martensitic transformation.

36 MATERIALS SCIENCE↗
NASA NTRS1964

Dynamic buckling estimates

Dynamic buckling estimates for sensitive structures subjected to finite-time loading

COMPRESSION BUCKLING↗
NASA NTRS1972

Computer program for natural gas flow through nozzles

Subroutines, FORTRAN 4 type, were developed for calculating isentropic natural gas mass flow rate through nozzle. Thermodynamic functions covering compressibility, entropy, enthalpy, and specific heat are included.

Johnson, R. C.↗
NASA NTRS1982

Goertler instability in compressible boundary layers along curved surfaces with suction and cooling

The Goertler instability of the laminar compressible boundary layer flows along concave surfaces is investigated. The linearized disturbance equations for the three-dimensional, counter-rotating streamwise vortices in two-dimensional boundary layers are presented in an orthogonal curvilinear coordinate. The basic approximation of the disturbance equations, that includes the effect of the growth of the boundary layer, is considered and solved numerically. The effect of compressibility on critical stability limits, growth rates, and amplitude ratios of the vortices is evaluated for a range of Mach numbers for 0 to 5. The effect of wall cooling and suction of the boundary layer on the development of Goertler vortices is investigated for different Mach numbers.

El-Hady, N.↗
NASA NTRS1989

Vector quantization

During the past ten years Vector Quantization (VQ) has developed from a theoretical possibility promised by Shannon's source coding theorems into a powerful and competitive technique for speech and image coding and compression at medium to low bit rates. In this survey, the basic ideas behind the design of vector quantizers are sketched and some comments made on the state-of-the-art and current research efforts.

Gray, Robert M.↗
NASA NTRS1989

Performance of all-metal demountable cryogenic seals at superfluid helium temperatures

Two all-metal demountable cryogenic seals with an outside diameter of 36.6 mm, inside diameter of 27.2 mm, and thickness of 0.51 mm were leak-tested at room temperature (300 K), liquid nitrogen temperature (21 cycles at 77 K), liquid helium temperature (9 cycles at 4.2 K), and susperfluid helium temperature (4 cycles at 1.6 K). Each seal was mounted and demounted for 13 cycles. Thickness measurements at 90 deg intervals along the circumference showed a maximum seal compression of 0.038 mm. Leak-rate measurements at all temperatures showed no detectable leak above the helium background level, typically 0.1 x 10(-9) std-cc/sec, during testing.

Salerno, Louis J.↗
NASA NTRS1989

The oblique behavior of low-frequency electromagnetic waves excited by newborn cometary ions

The free energy in oxygen or hydrogen ions freshly created in the solar wind stimulates low-frequency electromagnetic waves whose growth does not always maximize at parallel propagation. Exploration of the wave vector plane discloses the frequent occurrence of islets of oblique growth unconnected to the unstable parallel modes. Contour plots of the growth rate, real frequency, polarization, and magnetic compression characterize the oblique wave behavior for large values of the initial pitch angle of the cometary particles. Although wave-particle (Landau and cyclotron) resonances feed most of the surveyed oblique instabilities, some are seemingly fluidlike. The results, obtained from the numerical solution of the kinetic dispersion and wave equations, imply that newborn ions can easily excite significant oblique hydromagnetic wave activity. Cometary environments provide the adopted plasma model, but the study is helpful in the interpretation of other low-frequency wave observations in space.

Brinca, Armando L.↗
NASA NTRS1989

Performance of all-metal demountable cryogenic seals at superfluid helium temperatures

Two all-metal demountable cryogenic seals with an outside diameter of 36.6 mm, inside diameter of 27.2 mm, and thickness of 0.51 mm were leak-tested at room temperature (300 K), liquid nitrogen temperature (21 cycles at 77 K), liquid helium temperature (9 cycles at 4.2 K), and superfluid helium temperature (4 cycles at 1.6 K). Each seal was mounted and demounted for 13 cycles. Thickness measurements at 90 deg intervals along the circumference showed a maximum seal compression of 0.038 mm. Leak-rate measurements at all temperatures showed no detectable leak above the helium background level, typically 0.1 x 10(-9) std-cc/sec, during testing.

Salerno, Louis J.↗
NASA NTRS1991

Computation of turbulent high speed mixing layers using a two-equation turbulence model

A two-equation turbulence model was extended to be applicable for compressible flows. A compressibility correction based on modelling the dilational terms in the Reynolds stress equations were included in the model. The model is used in conjunction with the SPARK code for the computation of high speed mixing layers. The observed trend of decreasing growth rate with increasing convective Mach number in compressible mixing layers is well predicted by the model. The predictions agree well with the experimental data and the results from a compressible Reynolds stress model. The present model appears to be well suited for the study of compressible free shear flows. Preliminary results obtained for the reacting mixing layers are included.

Narayan, J. R.↗
NASA NTRS1991

Scientific requirements for space science data systems

In the 1990's space plasma physics studies will increasingly involve correlative analysis of observations from multiple instruments and multiple spacecraft. The solar terrestrial physics missions in the 1990's will be designed around simultaneous observations from spacecraft monitoring the solar wind, the polar magnetosphere and the near and distant magnetotail. Within these regions, clusters of spacecraft flying in formation will increasingly involve comparative magnetospheric studies. No single lab will have the expertise to process and analyze all of the different types of data so the data repositories will be distributed. Catalog and browse systems will be required to help select events for study. Data compression techniques may be useful in designing the data bases used for selecting events for study. Data compression onboard the spacecraft will be necessary, since instrument data rates will be much larger than available telemetry rates. However, considerable care will be necessary to avoid losing valuable data when applying data compression algorithms.

Walker, Raymond J.↗
NASA NTRS1992

Bandwidth compression of noisy signals with square-wave subcarrier

This article discusses a method for downconverting the square-wave subcarrier of spacecraft signals, such as the one from Galileo, which results in a compression bandwidth that lowers the sample rate significantly. The study is focused on three issues. The first is the selection of an adequate down-mixing signal for the resulting signal to have a format similar to that of the original signal, except at a lower subcarrier frequency. The second is the control of the noise level so that the signal to noise ratio is not degraded due to the downconversion. The third is to determine the bandwidth of the downconverted signal considering the uncertainty of the residual carrier frequency.

Feria, Y.↗
NASA NTRS1932

The comparative performance of superchargers

This report presents a comparison of superchargers on the basis of the power required to compress the air at a definite rate, and on the basis of the net engine power developed at altitudes from 0 to 40,000 feet. The investigation included geared centrifugal, turbine-driven centrifugal, roots, and vane-type superchargers. It also includes a brief discussion of the mechanical limitations of each supercharger and explains how the method of control affects the power requirements.

Schey, Oscar W↗
NASA NTRS1994

Subband And Transform Compression Of Video Signals

Class of hierarchical subband coders developed primarily for compression of image data at video rates. Coders offer good performance with limited computational complexity and with flexibility inherent in subband decomposition.

Sauer, Ken↗