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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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All sourcesNASA NTRSDOE OSTI
DOE OSTI2013

Method development for determining the hydraulic conductivity of fractured porous media

Plausible, but unvalidated, theoretical model constructs for unsaturated hydraulic conductivity of fractured porous media are currently used in Performance Assessment (PA) modeling for cracked saltstone and concrete (Flach 2011). The Nuclear Regulatory Commission (NRC) has expressed concern about the lack of model support for these assumed Moisture Characteristic Curves (MCC) data, as noted in Requests for Additional Information (RAIs) PA-8 and SP-4 (Savannah River Remediation, LLC, 2011). The objective of this task was to advance PA model support by developing an experimental method for determining the hydraulic conductivity of fractured cementitious materials under unsaturated conditions, and to demonstrate the technique on fractured saltstone samples. The task was requested through Task Technical Request (TTR) HLW-SSF-TTR-2012-0016 and conducted in accordance with Task Technical & Quality Assurance Plan (TTQAP) SRNL-TR-2012-00090. Preliminary method development previously conducted by Kohn et al. (2012) identified transient outflow extraction as the most promising method for characterizing the unsaturated properties of fractured porous media. While the research conducted by Kohn et al. (2012) focused on fractured media analogs such as stacked glass slides, the current task focused directly on fractured saltstone. For this task, four sample types with differing fracture geometries were considered: 1) intact saltstone, 2) intact saltstone with a single saw cut, smooth surface fracture, 3) micro-fractured saltstone (induced by oven drying), and 4) micro-fractured saltstone with a single, fully-penetrating, rough-surface fracture. Each sample type was tested initially for saturated hydraulic conductivity following method ASTM D 5084 using a flexible wall permeameter. Samples were subsequently tested using the transient outflow extraction method to determine cumulative outflow as a function of time and applied pressure. Of the four sample types tested, two yielded datasets suitable for analysis (sample types 3 and 4). The intact saltstone sample (sample type 1) did not yield any measureable outflow over the pressure range of the outflow test (0-1000 cm H 2 O). This was expected because the estimated air entry pressure for intact saltstone is on the order of 100,000 cm H 2 O (Dixon et al., 2009). The intact saltstone sample with a single saw cut smooth surface fracture (sample type 2) did not produce useable data because the fracture completely drained at less than 10 cm H 2 O applied pressure. The cumulative outflow data from sample types 3 and 4 were analyzed using an inverse solution of the Richard’s equation for water flow in variably saturated porous media. This technique was implemented using the computer code Hydrus-1D (Šimunek et al., 2008) and the resulting output included the van Genuchten-Mualem water retention and relative permeability parameters and predicted saturated hydraulic conductivity (Van Genuchten, 1980; Van Genuchten et al., 1991). Estimations of relative permeability and saturated conductivity are possible because the transient response of the sample to pressure changes is recorded during the multi-step outflow extraction test. Characteristic curves were developed for sample types 3 and 4 based on the results of the transient outflow method and compared to that of intact saltstone previously reported by Dixon et al. (2009). The overall results of this study indicate that the outflow extraction method is suitable for measuring the hydraulic properties of micro-fractured porous media. The resulting cumulative outflow data can be analyzed using the computer code Hydrus-1D to generate the van Genuchten curve fitting parameters that adequately describe fracture drainage. The resulting characteristic curves are consistent with blended characteristic curves that combine the behaviors of low pressure drainage associated with fracture flow with high pressure drainage from the bulk saltstone matrix.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2014

Order-parameter-aided temperature-accelerated sampling for the exploration of crystal polymorphism and solid-liquid phase transitions

The problem of predicting polymorphism in atomic and molecular crystals constitutes a significant challenge both experimentally and theoretically. From the theoretical viewpoint, polymorphism prediction falls into the general class of problems characterized by an underlying rough energy landscape, and consequently, free energy based enhanced sampling approaches can be brought to bear on the problem. In this paper, we build on a scheme previously introduced by two of the authors in which the lengths and angles of the supercell are targeted for enhanced sampling via temperature accelerated adiabatic free energy dynamics [T. Q. Yu and M. E. Tuckerman, Phys. Rev. Lett. 107, 015701 (2011)]. Here, that framework is expanded to include general order parameters that distinguish different crystalline arrangements as target collective variables for enhanced sampling. The resulting free energy surface, being of quite high dimension, is nontrivial to reconstruct, and we discuss one particular strategy for performing the free energy analysis. The method is applied to the study of polymorphism in xenon crystals at high pressure and temperature using the Steinhardt order parameters without and with the supercell included in the set of collective variables. The expected fcc and bcc structures are obtained, and when the supercell parameters are included as collective variables, we also find several new structures, including fcc states with hcp stacking faults. We also apply the new method to the solid-liquid phase transition in copper at 1300 K using the same Steinhardt order parameters. Our method is able to melt and refreeze the system repeatedly, and the free energy profile can be obtained with high efficiency.

36 MATERIALS SCIENCE↗
NASA NTRS2010

Miniature Low-Mass Drill Actuated by Flextensional Piezo Stack

Recent experiments with a flextensional piezoelectric actuator have led to the development of a sampler with a bit that is designed to produce and capture a full set of sample forms including volatiles, powdered cuttings, and core fragments. The flextensional piezoelectric actuator is a part of a series of devices used to amplify the generated strain from piezoelectric actuators. Other examples include stacks, bimorphs, benders, and cantilevers. These devices combine geometric and resonance amplifications to produce large stroke at high power density. The operation of this sampler/drill was demonstrated using a 3x2x1-cm actuator weighing 12 g using power of about 10-W and a preload of about 10 N. A limestone block was drilled to a depth of about 1 cm in five minutes to produce powdered cuttings. It is generally hard to collect volatiles from random surface profiles found in rocks and sediment, powdered cuttings, and core fragments. Toward the end of collecting volatiles, the actuator and the bit are covered with bellows-shaped shrouds to prevent fines and other debris from reaching the analyzer. A tube with a miniature bellows (to provide flexibility) is connected to the bit and directs the flow of the volatiles to the analyzer. Another modality was conceived where the hose is connected to the bellows wall directly to allow the capture of volatiles generated both inside and outside the bit. A wide variety of commercial bellows used in the vacuum and microwave industries can be used to design the volatiles capture mechanism. The piezoelectric drilling mechanism can potentially be operated in a broad temperature range from about-200 to less than 450 C. The actuators used here are similar to the actuators that are currently baselined to fly as part of the inlet funnel shaking mechanism design of MSL (Mars Science Laboratory). The space qualification of these parts gives this drill a higher potential for inclusion in a future mission, especially when considering its characteristics of low mass, small size, low power, and low axial loads for sampling.

Sherrit, Stewart↗
DOE OSTI2015

The stacked thermal Sunyaev–Zel’Dovich signal of locally brightest galaxies in Planck full mission data: Evidence for galaxy feedback?

We use the Planck full mission temperature maps to examine the stacked thermal Sunyaev–Zel’dovich (tSZ) signal of 188,042 “locally brightest galaxies” (LBGs) selected from the Sloan Digital Sky Survey Data Release 7. Our LBG sample closely matches that of Planck Collaboration XI (PCXI), but our analysis differs in several ways. We work directly in terms of physically observable quantities, requiring minimal assumptions about the gas pressure profile. We explicitly model the dust emission from each LBG and simultaneously measure both the stacked tSZ and dust signals as a function of stellar mass M{sub ∗}. There is a small residual bias in stacked tSZ measurements; we measure this bias and subtract it from our results, finding that the effects are non-negligible at the lowest masses in the LBG sample. Finally, we compare our measurements with two pressure profile models, finding that the profile from Battaglia et al. provides a better fit to the results than the Arnaud et al. “universal pressure profile.” However, within the uncertainties, we find that the data are consistent with a self-similar scaling with mass—more precise measurements are needed to detect the relatively small deviations from self-similarity predicted by these models. Consistent with PCXI, we measure the stacked tSZ signal from LBGs with stellar masses down to log{sub 10}(M{sub ∗}/M{sub ⊙}) ∼ 11.1–11.3. For lower stellar masses, however, we do not see evidence for a stacked tSZ signal. We note that the stacked dust emission is comparable to, or larger than, the stacked tSZ signal for log{sub 10}(M{sub ∗}/M{sub ⊙})≲11.3. Future tSZ analyses with larger samples and lower noise levels should be able to probe deviations from self-similarity and thus provide constraints on models of feedback and the evolution of hot halo gas over cosmic time.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2019

The 3XMM/SDSS Stripe 82 Galaxy Cluster Survey – II. X-ray and optical properties of the cluster sample

ABSTRACT We present X-ray and optical properties of the optically confirmed galaxy cluster sample from the 3XMM/SDSS Stripe 82 cluster survey. The sample includes 54 galaxy clusters in the redshift range of 0.05–1.2, with a median redshift of 0.36. We first present the X-ray temperature and luminosity measurements that are used to investigate the X-ray luminosity–temperature relation. The slope and intercept of the relation are consistent with those published in the literature. Then, we investigate the optical properties of the cluster galaxies including their morphological analysis and the galaxy luminosity functions (GLFs). The morphological content of cluster galaxies is investigated as a function of cluster mass and distance from the cluster centre. No strong variation of the fraction of early- and late-type galaxies with cluster mass is observed. The fraction of early-type galaxies as a function of cluster radius varies as expected. The individual GLFs of red sequence galaxies were studied in the five ugriz bands for 48 clusters. The GLFs were then stacked in three mass bins and two redshift bins. Twenty clusters of the present sample are studied for the first time in X-rays, and all are studied for the first time in the optical range. Altogether, our sample appears to have X-ray and optical properties typical of ‘average’ cluster properties.

Takey, Ali↗
DOE OSTI2024

Deterministic fabrication of graphene hexagonal boron nitride moiré superlattices

The electronic properties of moiré heterostructures depend sensitively on the relative orientation between layers of the stack. For example, near-magic-angle twisted bilayer graphene (TBG) commonly shows superconductivity, yet a TBG sample with one of the graphene layers rotationally aligned to a hexagonal Boron Nitride (hBN) cladding layer provided experimental observation of orbital ferromagnetism. To create samples with aligned graphene/hBN, researchers often align edges of exfoliated flakes that appear straight in optical micrographs. However, graphene or hBN can cleave along either zig-zag or armchair lattice directions, introducing a 30° ambiguity in the relative orientation of two flakes. By characterizing the crystal lattice orientation of exfoliated flakes prior to stacking using Raman and second-harmonic generation for graphene and hBN, respectively, we unambiguously align monolayer graphene to hBN at a near-0°, not 30°, relative twist angle. We confirm this alignment by torsional force microscopy of the graphene/hBN moiré on an open-face stack, and then by cryogenic transport measurements, after full encapsulation with a second, nonaligned hBN layer. This work demonstrates a key step toward systematically exploring the effects of the relative twist angle between dissimilar materials within moiré heterostructures.

boron nitride↗
DOE OSTI2015

Relationship between crystal structure and thermo-mechanical properties of kaolinite clay: Beyond standard density functional theory

In this study, the structural, mechanical and thermodynamic properties of 1 : 1 layered dioctahedral kaolinite clay, with ideal Al 2 Si 2 O 5 (OH) 4 stoichiometry, were investigated using density functional theory corrected for dispersion interactions (DFT-D2). The bulk moduli of 56.2 and 56.0 GPa predicted at 298 K using the Vinet and Birch–Murnaghan equations of state, respectively, are in good agreement with the recent experimental value of 59.7 GPa reported for well-crystallized samples. The isobaric heat capacity computed for uniaxial deformation of kaolinite along the stacking direction reproduces calorimetric data within 0.7–3.0% from room temperature up to its thermal stability limit.

36 MATERIALS SCIENCE↗
DOE OSTI2012

Structural studies of high-K{sub u} metastable CoPt thin films with long-range order

The symmetries of CoPt thin films in different phases, including disordered A1, ordered L1{sub 1}, and L1{sub 0} were examined by making measurements along the (10.1) diffraction rod. The films were deposited by sputtering on MgO(111) substrates at different temperatures (T{sub a}). The stacking sequence of close-packed atomic planes in 50 nm-thick samples with T{sub a} {>=} 200 deg. C was identified as ABCABC, indicating that the distribution of defects in the film was random, so the symmetry was preserved with increasing T{sub a}. In the RT-prepared film, a considerable amount of ({approx}62.9 vol.%) disordered CoPt with hexagonal symmetry was detected, vanishing as T{sub a} increased. Defect-induced modification of symmetry was observed in the L1{sub 1} film as its thickness was reduced to 10 nm. A pseudo-hcp component of around 7.1 vol.% was present in the film, as a result of the periodic distribution of defects. The defects in the structure may also explain the broadened magnetic alignment.

36 MATERIALS SCIENCE↗
DOE OSTI2021

Gradient cell–structured high-entropy alloy with exceptional strength and ductility

We report that similar to conventional materials, most multicomponent high-entropy alloys (HEAs) lose ductility as they gain strength. In this study, we controllably introduced gradient nanoscaled dislocation cell structures in a stable single-phase HEA with face-centered cubic structure, thus resulting in enhanced strength without apparent loss of ductility. Upon application of strain, the sample-level structural gradient induces progressive formation of a high density of tiny stacking faults (SFs) and twins, nucleating from abundant low-angle dislocation cells. Furthermore, the SF-induced plasticity and the resultant refined structures, coupled with intensively accumulated dislocations, contribute to plasticity, increased strength, and work hardening. These findings offer a promising paradigm for tailoring properties with gradient dislocation cells at the nanoscale and advance our fundamental understanding of the intrinsic deformation behavior of HEAs.

36 MATERIALS SCIENCE↗
DOE OSTI2016

ALMA spectroscopic survey in the Hubble Ultra Deep Field: the infrared excess of UV-selected z = 2–10 galaxies as a function of UV-continuum slope and stellar mass

We make use of deep 1.2 mm continuum observations (12.7 μJy beam{sup −1} rms) of a 1 arcmin{sup 2} region in the Hubble Ultra Deep Field to probe dust-enshrouded star formation from 330 Lyman-break galaxies spanning the redshift range z = 2–10 (to ∼2–3 M {sub ⊙} yr{sup −1} at 1σ over the entire range). Given the depth and area of ASPECS, we would expect to tentatively detect 35 galaxies, extrapolating the Meurer z ∼ 0 IRX–β relation to z ≥ 2 (assuming dust temperature T {sub d} ∼ 35 K). However, only six tentative detections are found at z ≳ 2 in ASPECS, with just three at >3σ. Subdividing our z = 2–10 galaxy samples according to stellar mass, UV luminosity, and UV-continuum slope and stacking the results, we find a significant detection only in the most massive (>10{sup 9.75} M {sub ⊙}) subsample, with an infrared excess (IRX = L {sub IR}/L {sub UV}) consistent with previous z ∼ 2 results. However, the infrared excess we measure from our large selection of sub-L {sup ∗} (<10{sup 9.75} M {sub ⊙}) galaxies is 0.11{sub −0.42}{sup +0.32} ± 0.34 (bootstrap and formal uncertainties) and 0.14{sub −0.14}{sup +0.15} ± 0.18 at z = 2–3 and z = 4–10, respectively, lying below even an IRX–β relation for the Small Magellanic Cloud (95% confidence). These results demonstrate the relevance of stellar mass for predicting the IR luminosity of z ≳ 2 galaxies. We find that the evolution of the IRX–stellar mass relationship depends on the evolution of the dust temperature. If the dust temperature increases monotonically with redshift (∝(1+z){sup 0.32}) such that T {sub d} ∼ 44–50 K at z ≥ 4, current results are suggestive of little evolution in this relationship to z ∼ 6. We use these results to revisit recent estimates of the z ≥ 3 star formation rate density.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2012

THE WiggleZ DARK ENERGY SURVEY: GALAXY EVOLUTION AT 0.25 {<=} z {<=} 0.75 USING THE SECOND RED-SEQUENCE CLUSTER SURVEY

We study the evolution of galaxy populations around the spectroscopic WiggleZ sample of star-forming galaxies at 0.25 {<=} z {<=} 0.75 using the photometric catalog from the Second Red-Sequence Cluster Survey (RCS2). We probe the optical photometric properties of the net excess neighbor galaxies. The key concept is that the marker galaxies and their neighbors are located at the same redshift, providing a sample of galaxies representing a complete census of galaxies in the neighborhood of star-forming galaxies. The results are compared with those using the RCS WiggleZ Spare-Fibre (RCS-WSF) sample as markers, representing galaxies in cluster environments at 0.25 {<=} z {<=} 0.45. By analyzing the stacked color-color properties of the WiggleZ neighbor galaxies, we find that their optical colors are not a strong function of indicators of star-forming activities such as EW([O II]) or Galaxy Evolution Explorer (GALEX) near-UV luminosity of the markers. The galaxies around the WiggleZ markers exhibit a bimodal distribution on the color-magnitude diagram, with most of them located in the blue cloud. The optical galaxy luminosity functions (GLFs) of the blue neighbor galaxies have a faint-end slope {alpha} of {approx} - 1.3, similar to that for galaxies in cluster environments drawn from the RCS-WSF sample. The faint-end slope of the GLF for the red neighbors, however, is {approx} - 0.4, significantly shallower than the {approx} - 0.7 found for those in cluster environments. This suggests that the buildup of the faint end of the red sequence in cluster environments is in a significantly more advanced stage than that in the star-forming and lower galaxy density WiggleZ neighborhoods. We find that the red galaxy fraction (f{sub red}) around the star-forming WiggleZ galaxies has similar values from z {approx} 0.3 to z {approx} 0.6 with f{sub red} {approx} 0.28, but drops to f{sub red} {approx} 0.20 at z {approx}> 0.7. This change of f{sub red} with redshift suggests that there is either a higher rate of star-forming galaxies entering the luminosity-limited sample at z {approx}> 0.7, or a decrease in the quenching rate of star formation at that redshift. Comparing to that in a dense cluster environment, the f{sub red} of the WiggleZ neighbors is both considerably smaller and has a more moderate change with redshift, pointing to the stronger and more prevalent environmental influences on galaxy evolution in high-density regions.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2016

Effect of top electrode material on radiation-induced degradation of ferroelectric thin film structures

The effects of gamma irradiation on the dielectric and piezoelectric responses of Pb[Zr{sub 0.52}Ti{sub 0.48}]O{sub 3} (PZT) thin film stacks were investigated for structures with conductive oxide (IrO{sub 2}) and metallic (Pt) top electrodes. The samples showed, generally, degradation of various key dielectric, ferroelectric, and electromechanical responses when exposed to 2.5 Mrad (Si) {sup 60}Co gamma radiation. However, the low-field, relative dielectric permittivity, ε{sub r}, remained largely unaffected by irradiation in samples with both types of electrodes. Samples with Pt top electrodes showed substantial degradation of the remanent polarization and overall piezoelectric response, as well as pinching of the polarization hysteresis curves and creation of multiple peaks in the permittivity-electric field curves post irradiation. The samples with oxide electrodes, however, were largely impervious to the same radiation dose, with less than 5% change in any of the functional characteristics. The results suggest a radiation-induced change in the defect population or defect energy in PZT with metallic top electrodes, which substantially affects motion of internal interfaces such as domain walls. Additionally, the differences observed for stacks with different electrode materials implicate the ferroelectric–electrode interface as either the predominant source of radiation-induced effects (Pt electrodes) or the site of healing for radiation-induced defects (IrO{sub 2} electrodes).

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2013

Quantitative description of microstructure defects in hexagonal boron nitrides using X-ray diffraction analysis

A routine for simultaneous quantification of turbostratic disorder, amount of puckering and the dislocation and stacking fault density in hexagonal materials was proposed and tested on boron nitride powder samples that were synthesised using different methods. The routine allows the individual microstructure defects to be recognised according to their effect on the anisotropy of the X-ray diffraction line broadening. For quantification of the microstructure defects, the total line broadening is regarded as a linear combination of the contributions from the particular defects. The total line broadening is obtained from the line profile fitting. As testing material, graphitic boron nitride (h-BN) was employed in the form of hot-isostatically pressed h-BN, pyrolytic h-BN or a h-BN, which was chemically vapour deposited at a low temperature. The kind of the dominant microstructure defects determined from the broadening of the X-ray diffraction lines was verified by high resolution transmission electron microscopy. Their amount was attempted to be verified by alternative methods. - Highlights: • Reliable method for quantification of microstructure defects in BN was suggested. • The method is based on the analysis of anisotropic XRD line broadening. • This XRD line broadening is unique and characteristic of the respective defect. • Thus, the quantification of coexistent microstructure defects is possible. • The method was tested on hexagonal BN, which was produced by different techniques.

36 MATERIALS SCIENCE↗
DOE OSTI2020

Accurate determination of production data of the non-standard positron emitter 86 Y via the 86 Sr(p,n)-reaction

In view of several significant discrepancies in the excitation function of the 86 Sr(p,n) 86g+xm Y reaction which is the method of choice for the production of the non-standard positron emitter 86 Y for theranostic application, we carried out a careful measurement of the cross sections of this reaction from its threshold up to 16.2 MeV at Forschungszentrum Jülich (FZJ) and from 14.3 to 24.5 MeV at LBNL. Thin samples of 96.4% enriched 86 SrCO 3 were prepared by sedimentation and, after irradiation with protons in a stacked-form, the induced radioactivity was measured by high-resolution γ -ray spectrometry. The projectile flux was determined by using the monitor reactions nat Cu(p,xn) 62,63,65 Zn and nat Ti(p,x) 48 V, and the calculated proton energy for each sample was verified by considering the ratios of two reaction products of different thresholds. Additionally, the experimental cross section data obtained agreed well with the results of a nuclear model calculation based on the code TALYS. From the cross section data, the integral yield of 86 Y was calculated. Over the optimum production energy range E p = 14 → 7 MeV the yield of 86 Y amounts to 291 MBq/μA for 1 h irradiation time. This value is appreciably lower than the previous literature values calculated from measured and evaluated excitation functions. It is, however, more compatible with the experimental yields of 86 Y obtained in clinical scale production runs. The levels of the isotopic impurities 87m Y, 87g Y, and 88 Y were also estimated and found to be <2% in sum.

38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEA↗
DOE OSTI2016

SDSS-IV MaNGA IFS GALAXY SURVEY—SURVEY DESIGN, EXECUTION, AND INITIAL DATA QUALITY

The MaNGA Survey (Mapping Nearby Galaxies at Apache Point Observatory) is one of three core programs in the Sloan Digital Sky Survey IV. It is obtaining integral field spectroscopy for 10,000 nearby galaxies at a spectral resolution of R ∼ 2000 from 3622 to 10354 Å. The design of the survey is driven by a set of science requirements on the precision of estimates of the following properties: star formation rate surface density, gas metallicity, stellar population age, metallicity, and abundance ratio, and their gradients; stellar and gas kinematics; and enclosed gravitational mass as a function of radius. We describe how these science requirements set the depth of the observations and dictate sample selection. The majority of targeted galaxies are selected to ensure uniform spatial coverage in units of effective radius (R{sub e}) while maximizing spatial resolution. About two-thirds of the sample is covered out to 1.5 R{sub e} (Primary sample), and one-third of the sample is covered to 2.5 R{sub e} (Secondary sample). We describe the survey execution with details that would be useful in the design of similar future surveys. We also present statistics on the achieved data quality, specifically the point-spread function, sampling uniformity, spectral resolution, sky subtraction, and flux calibration. For our Primary sample, the median r -band signal-to-noise ratio is ∼70 per 1.4 Å pixel for spectra stacked between 1 R{sub e} and 1.5 R{sub e}. Measurements of various galaxy properties from the first-year data show that we are meeting or exceeding the defined requirements for the majority of our science goals.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2015

THE SCUBA-2 COSMOLOGY LEGACY SURVEY: ALMA RESOLVES THE REST-FRAME FAR-INFRARED EMISSION OF SUB-MILLIMETER GALAXIES

We present high-resolution (0.''3) Atacama Large Millimeter Array 870 μm imaging of 52 sub-millimeter galaxies (SMGs) in the Ultra Deep Survey field to investigate the size and morphology of the sub-millimeter (sub-mm) emission on 2-10 kpc scales. We derive a median intrinsic angular size of FWHM = 0.''30 ± 0.''04 for the 23 SMGs in the sample detected at a signal-to-noise ratio (S/N) >10. Using the photometric redshifts of the SMGs we show that this corresponds to a median physical half-light diameter of 2.4 ± 0.2 kpc. A stacking analysis of the SMGs detected at S/N <10 shows they have sizes consistent with the 870 μm bright SMGs in the sample. We compare our results to the sizes of SMGs derived from other multi-wavelength studies, and show that the rest-frame ∼250 μm sizes of SMGs are consistent with studies of resolved {sup 12}CO (J = 3-2 to 7-6) emission lines, but that sizes derived from 1.4 GHz imaging appear to be approximately two times larger on average, which we attribute to cosmic ray diffusion. The rest-frame optical sizes of SMGs are around four times larger than the sub-millimeter sizes, indicating that the star formation in these galaxies is compact relative to the pre-existing stellar distribution. The size of the starburst region in SMGs is consistent with the majority of the star formation occurring in a central region, a few kiloparsecs in extent, with a median star formation rate surface density of 90 ± 30 M {sub ☉} yr{sup –1} kpc{sup –2}, which may suggest that we are witnessing an intense period of bulge growth in these galaxies.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2016

Organic doping of rotated double layer graphene

Charge transfer techniques have been extensively used as knobs to tune electronic properties of two- dimensional systems, such as, for the modulation of conductivity \ mobility of single layer graphene and for opening the bandgap in bilayer graphene. The charge injected into the graphene layer shifts the Fermi level away from the minimum density of states point (Dirac point). In this work, we study charge transfer in rotated double-layer graphene achieved by the use of organic dopant, Tetracyanoquinodimethane. Naturally occurring bilayer graphene has a well-defined A-B stacking whereas in rotated double-layer the two graphene layers are randomly stacked with different rotational angles. This rotation is expected to significantly alter the interlayer interaction. Double-layer samples are prepared using layer-by-layer assembly of chemical vapor deposited single-layer graphene and they are identified by characteristic resonance in the Raman spectrum. The charge transfer and distribution of charges between the two graphene layers is studied using Raman spectroscopy and the results are compared with that for single-layer and A-B stacked bilayer graphene doped under identical conditions.

77 NANOSCIENCE AND NANOTECHNOLOGY↗
DOE OSTI2014

Structure and strain relaxation effects of defects in In{sub x}Ga{sub 1–x}N epilayers

The formation of trench defects is observed in 160 nm-thick In{sub x}Ga{sub 1–x}N epilayers with x≤0.20, grown on GaN on (0001) sapphire substrates using metalorganic vapour phase epitaxy. The trench defect density increases with increasing indium content, and high resolution transmission electron microscopy shows an identical structure to those observed previously in InGaN quantum wells, comprising meandering stacking mismatch boundaries connected to an I₁-type basal plane stacking fault. These defects do not appear to relieve in-plane compressive strain. Other horizontal sub-interface defects are also observed within the GaN pseudosubstrate layer of these samples and are found to be pre-existing threading dislocations which form half-loops by bending into the basal plane, and not basal plane stacking faults, as previously reported by other groups. The origins of these defects are discussed and are likely to originate from a combination of the small in-plane misorientation of the sapphire substrate and the thermal mismatch strain between the GaN and InGaN layers grown at different temperatures.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗