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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 361 records · Page 20
All sourcesNASA NTRSDOE OSTI
NASA NTRS1999

Miniature Quadrupole Mass Spectrometer Array

JPL is funded by Code U to develop a Miniature QMSA for an EVA flight test. The initial intent was to fly an experiment internal to the astronaut suit during a shuttle EVA. Following discussions with JSC the suit application was abandoned in favor of other more urgent needs. The JSC EVA office was particularly interested in hydrazine detection on the astronaut suit. While discussing and exploring the implementation of such an experiment, managers at JSC suggested combining the interests of two JSC groups. The Life Support and Thermal Systems Branch, Crew and Thermal Systems Division has a need for an ammonia detection instrument, while the EVA office has a need for hydrazine detection. The two groups were pursuing separate single-purpose solutions. Instead, the JPL QMSA offers a single instrument solution via a portable instrument to be used by an astronaut on an EVA. Such an instrument would serve both the ammonia leak detection and the hydrazine contamination needs. The need for the QMSA was defined as urgent and targeted for a January 1999 flight. While the original JPL task (as funded by Code U) was for an experiment flight with JPL delivery in October 1998, this task was for a qualified flight instrument with a planned JPL delivery in August 1998. This schedule was very demanding and dictated a fast-tract implementation.

Karmon, D.↗
NASA NTRS2001

A Quadrupole Ion Trap Mass Spectrometer for Quantitative Analysis of Nitrogen-Purged Compartments within the Space Shuttle

To enter orbit the Space Shuttle burns 1.8 million liters of liquid hydrogen combined with 0.8 million liters of liquid oxygen through three rocket engines mounted in the aft. NASA monitors the nitrogen-purged aft compartment for increased levels of hydrogen or oxygen in order to detect and determine the severity of a cryogenic fuel leak. Current monitoring is accomplished with a group of mass spectrometer systems located as much as 400 feet away from the shuttle. It can take up to 45 seconds for gas to reach the mass spectrometer, which precludes monitoring for leaks in the final moments before liftoff (the orbiter engines are started at T-00:06 seconds). To remedy the situation, NASA is developing a small rugged mass spectrometer to be used as point-sources around the Space Shuttle.

Ottens, Andrew K.↗
NASA NTRS2005

Simultaneous quantification of poly-dispersed anionic, amphoteric and nonionic surfactants in simulated wastewater samples using C18 high-performance liquid chromatography-quadrupole ion-trap mass spectrometry

This paper describes the development of a guantitative method for direct and simultaneous determination of three frequently encountered surfactants, amphoteric (cocoamphoacetate, CAA), anionic (sodium laureth sulfate, SLES), and nonionic (alcohol ethoxylate, AE) using a reversed-phase C18 HPLC coupled with an ESI ion-trap mass spectrometer (MS). Chemical composition, ionization characteristics and fragmentation pathways of the surfactants are presented. Positive ESI was effective for all three surfactants in agueous methanol buffered with ammonium acetate. The method enables rapid determinations in small sample volumes containing inorganic salts (up to 3.5 g L(-1)) and multiple classes of surfactants with high specificity by applying surfactant specific tandem mass spectrometric strategies. It has dynamic linear ranges of 2-60, 1.5-40, 0.8-56 mg L(-1) with R2 egual or greater than 0.999, 0.98 and 0.999 (10 microL injection) for CAA, SLES, and AE, respectively.

Chromatography, High Pressure Liquid/methods↗
NASA NTRS2003

Quadrupole mass spectrometer driver with higher signal levels

Driving a quadrapole mass spectrometer includes obtaining an air core transformer with a primary and a secondary, matching the secondary to the mass spectrometer, and driving the primary based on first and second voltage levels. Driving of the primary is via an isolating stage that minimizes low level drive signal coupling.

Chutjian, Ara↗
NASA NTRS2013

Auxiliary Frequency Parametric Excitation of Quadrupole Mass Spectrometers

The apparatus introduces a second adjustable resonant point in a QMS at a frequency that is close to a multiple of the fundamental frequency by adjusting driving point impedance characteristics of the QMS. The apparatus measures the first and second resonant point of the QMS to account for changes in the operational characteristics of the QMS.

Gershman, Daniel↗
NASA NTRSDate not supplied

In-Situ Reaction Monitoring for Lunar Applications Utilizing a Single Quadrupole Residual Gas Analyzer

With a revived focus to create a permanent presence on the moon and in preparation for future Mars exploration ,it is imperative that all resources are utilized to their fullest potential.[1] In-Situ Resource Utilization (ISRU)will be critical for future mission success as it would enable independent operation of missions while minimally relying on the complex supply chain created between the Earth, moon and Mars.One of the most critical resources that have been identified for ISRU is the creation of liquid oxygen (LO2)for not only breathable air, but also for rocket propellant.On the moon and potentially Mars, one of the most O2rich resources is in the presence of regolith.[2],[3]Although there are numerous minerals within regolith and various processes to extract O2, this is not the scope of this poster

Thomas T Barnes III↗