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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 361 records · Page 20

Quantifying Damage Accumulation During Ductile Plastic Deformation Using Synchrotron Radiation

Under this grant, we have developed and demonstrated the ability of near-field High Energy Diffraction Microscopy (nf-HEDM) to map crystal orientation fields over three dimensions in deformed polycrystalline materials. Experimental work was performed at the Advanced Photon Source (APS) at beamline 1-ID. Applications of this new capability to ductile deformation of copper and zirconium samples were demonstrated as was the comparison of the experimental observations to computational plasticity models using a fast Fourier transform based algorithm that is able to handle the large experimental data sets. No such spatially resolved, direct comparison between measured and computed microstructure evolutions had previously been possible. The impact of this work is reflected in numerous publications and presentations as well as in the investments by DOE and DOD laboratories of millions of dollars in applying the technique, developing sophisticated new hardware that allows the technique to be applied to a wide variety of materials and materials problems, and in the use of the technique by other researchers. In essence, the grant facilitated the development of a new form of three dimensional microscopy and its application to technologically critical states of polycrystalline materials that are used throughout the U.S. and world economies. On-going collaborative work is further optimizing experimental and computational facilities at the APS and is pursuing expanded facilities.

36 MATERIALS SCIENCE↗

Numerical Simulation of Systems of Shear Bands in Ductile Metal with Inclusions

These are slides for a presentation on numerical simulation of systems of shear bands in ductile metal with inclusions, performed at Los Alamos National Laboratory. The conclusions are the following: A shear band is much thinner (0.1 μm) than the spacing between inclusions (100μm). Therefore fully resolved simulation is not feasible; asymptotic analysis allows modeling of a shear band as a velocity discontinuity within a moderately sized cell; formation criterion (critical strain) is determined by rate-dependent viscoplastic flow rule; inclusions cause shear bands to form at smaller strain; under expansion, shear bands form at the same strain than under compression; this can be applied to crystal plasticity.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Mechanisms for Ductile Rupture - FY16 ESC Progress Report

Ductile rupture in metals is generally a multi-step process of void nucleation, growth, and coalescence. Particle decohesion and particle fracture are generally invoked as the primary microstructural mechanisms for room-temperature void nucleation. However, because high-purity materials also fail by void nucleation and coalescence, other microstructural features must also act as sites for void nucleation. Early studies of void initiation in high-purity materials, which included post-mortem fracture surface characterization using scanning electron microscopy (SEM) and high-voltage electron microscopy (HVEM) and in-situ HVEM observations of fracture, established the presence of dislocation cell walls as void initiation sites in high-purity materials. Direct experimental evidence for this contention was obtained during in-situ HVEM tensile tests of Be single crystals. Voids between 0.2 and 1 μm long appeared suddenly along dislocation cell walls during tensile straining. However, subsequent attempts to replicate these results in other materials, particularly α -Fe single crystals, were unsuccessful because of the small size of the dislocation cells, and these remain the only published in-situ HVEM observations of void nucleation at dislocation cell walls in the absence of a growing macrocrack. Despite this challenge, other approaches to studying void nucleation in high-purity metals also indicate that dislocation cell walls are nucleation sites for voids.

36 MATERIALS SCIENCE↗

Methodologies for Evaluation of Corrosion Protection for Ductile Iron Pipe

Repairing the nation’s infrastructure and ensuring its future durability are key issues facing the United States. It is important that these critical issues are addressed with appropriate and economical solutions based on the best modern scientific information. For example, in 2013 the American Society of Civil Engineers (ASCE), in its Report Card for America’s Infrastructure, gave the state of the critical water/wastewater infrastructure an overall grade of “D.” According to the ASCE, 6 billion gallons of drinking water disappear every day, mostly due to leaks in old pipes. Corrosion of water pipes plays a role in their durability and, for external pipe corrosion, the corrosivity of soils varies by location and is based on several factors, including soil resistivity. There is universal agreement that water pipes require some type of corrosion mitigation strategy (i.e., bare pipe is not installed). However, in specifying which strategy to employ for ductile iron pipe (DIP) in different soil types, the recommendations of the US Bureau of Reclamation (USBR) Technical Memorandum 8140-CC-2004-1 were subject to considerable debate. So much so that in 2009, this report was the subject of a study by the National Academy, which did not resolve the debate about the most effective and affordable solutions. Zinc-coatings have been explored in other parts of the world. Despite being widely used in Europe for almost 60 years, zinc coating was barely mentioned in either the 2004 or 2009 studies, which appeared to focus on North American data.

36 MATERIALS SCIENCE↗

Improving Ductility of Hydride Embrittled Zirconium (Final Report)

One of the main limiting factors on the lifetimes of nuclear fuel rod claddings is the formation of hydrides and associated detrimental effects on mechanical properties. In this study, we examined the behavior of hydrides in zirconium and zircaloy-4 after tensile stress is applied to determine whether the more ductile γ-ZrH phase was stabilized by the mechanical stress. We did not find a significant increase in the ratio of γ-ZrH phase to δ-ZrH1.5 phases after tensile stress is applied in previously hydrided metals. Previous reports indicate that this stabilization does occur when zircaloy is stressed and hydrided simultaneously, indicating that the formation of the γ-ZrH phase may reverse upon relaxation or may require the stress in-situ during the hydriding process to form in significant quantities.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Determination of Constraint-Independent Crack Tip Opening Angle for Stable Crack Growth in High-Strength Ductile Steels

The crack tip opening angle (CTOA) is one of fracture toughness parameters that has been used for decades in describing large stable crack growth in thin-walled aerospace structures under the low-constraint conditions. Recently, the pipeline industry has developed a growing interest in using the CTOA parameter to serve as the minimum required fracture toughness to arrest dynamic crack propagation in modern gas transmission pipelines made of high-strength ductile steel. To meet this industrial need, the CTOA test standard ASTM E3039 was therefore developed for measuring the constant critical CTOA. ASTM E3039 recommends a drop weight tearing test (DWTT) specimen with a shallow crack for standard CTOA testing, but its CTOA may depend on the low constraint condition of the DWTT specimen at the crack tip. Verifying the constraint independence of the DWTT-measured CTOA thus becomes indispensable for applying CTOA toughness to the running fracture control in the pipeline design. For this purpose, the present paper evaluates critical CTOA values in a set of fracture toughness tests on single-edge notched bend (SENB) specimens with shallow and deep cracks, based on four CTOA estimation models. Among these, the Ln(P)-LLD linear fit model is similar to that recommended by ASTM E3039 for CTOA calculation. Fracture test data for X80 pipeline steel and HY80 structural steel were considered in the CTOA evaluation. The results showed that the four CTOA models were able to determine a constraint independent CTOA value for stable crack growth in the SENB specimens. As a result, a single, reliable, constant CTOA value could be determined regardless of the specimen geometry or the crack-tip constraint conditions. Therefore, the CTOA measured using ASTM E3039 is constraint-independent and transferable to use in cases of actual cracks propagating in gas transmission pipelines.

36 MATERIALS SCIENCE↗

High-strength tungsten alloy with improved ductility

Alloy combines superior strength at elevated temperatures with improved ductility at lower temperatures relative to unalloyed tungsten. Composed of tungsten, rhenium, hafnium, and carbon, the alloy is prepared by consumable electrode vacuum arc-melting and can be fabricated into rod, plate, and sheet.

Klopp, W. D.↗

Heat treatment procedure to increase ductility of degraded nickel alloy

Tests demonstrate the room temperature ductility of degraded Rene 41 can be increased to acceptable values by solution heat treatment at a temperature of 2050 degrees to 2150 degrees F /1 to 2 hours/ and cooling through a controlled temperature range followed by normal aging in air /16 hours at 1400 degrees F/.

Prager, M.↗