In situ imaging of three dimensional freeze printing process using rapid x-ray synchrotron radiography
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Guang Yang↗
SEARCH · Engineering Papers
Results for “synchrotron imaging”
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HST observations of 3C 66B - A double-stranded optical jet
The central region of the synchrotron jet in 3C 66B imaged with ultrahigh spatial resolution by the Faint Object Camera on the HST is discussed. A close correspondence between the general characteristics of the smoothed optical image and the radio map is observed, implying that the young and old relativistic particles occupy similar regions to within about 130 pc. Focus is placed on the double-stranded filamentary nature of the jet, and it is speculated that this could reflect edge-brightening effects due to enhanced radiation from a skinlike structure surrounding the jet. It is noted that the similarity of optical and radio morphologies points to the fact that localized particle acceleration occurs along the jet; however, the filamentary structure and a low filling factor of radiation agree with a model in which the electrons are accelerated within the nucleus and are transported along the jet in a channel having low magnetic field.
Macchetto, F.↗
X-Ray Analysis of the Proper Motion and Pulsar Wind Nebula for PSR J1741-2054
We obtained six observations of PSR J1741-2054 using the Chandra ACIS-S detector totaling approx.300 ks. By registering this new epoch of observations to an archival observation taken 3.2 yr earlier using X-ray point sources in the field of view, we have measured the pulsar proper motion at micron = 109 +/- 10 mas yr(exp. -1) in a direction consistent with the symmetry axis of the observed H(alpha) nebula. We investigated the inferred past trajectory of the pulsar but find no compelling association with OB associations in which the progenitor may have originated. We confirm previous measurements of the pulsar spectrum as an absorbed power law with photon index gamma = 2.68 +/- 0.04, plus a blackbody with an emission radius of (4.5(+3.2/-2.5))d(0.38) km, for a DM-estimated distance of 0.38d(0.38) kpc and a temperature of 61.7 +/- 3.0 eV. Emission from the compact nebula is well described by an absorbed power law model with a photon index of gamma = 1.67 +/- 0.06, while the diffuse emission seen as a trail extending northeast of the pulsar shows no evidence of synchrotron cooling. We also applied image deconvolution techniques to search for small-scale structures in the immediate vicinity of the pulsar, but found no conclusive evidence for such structures.
Analysis↗
Grazing incidence optics; Proceedings of the Meeting, Orlando, FL, Apr. 3, 4, 1986
Papers are presented on the diffraction-limited performance of grazing incidence optical systems; transverse ray aberrations of Wolter type 1 telescopes; hybrid X-ray telescope systems; surface characterization of grazing incidence optics in the extreme UV and X-ray regions; and the surface roughness properties of synchrotron radiation optics. Topics discussed include the simulation of free-abrasive grinding of grazing incidence mirrors with vertical-honing and flexible blades; mirrors for the Extreme Ultraviolet Explorer; the design and development of conical X-ray imaging mirrors; thermal loading considerations for synchrotron radiation mirrors; and grazing incidence optics for synchrotron radiation insertion-device beams. Consideration is given to the interpretation of glancing incidence scattering measurements; damage processes in short wavelength coated FEL optics; the replication of grain incidence optics; and the assembly and alignment of the Technology Mirror Assembly.
Osantowski, John F.↗
Effect of Tube-Based X-Ray Microtomography Imaging on the Amino Acid and Amine Content of the Murchison CM2 Chondrite
X-ray and synchrotron X-ray micro-computed tomography (micro-CT) are increasingly being used for three dimensional reconnaissance imaging of chondrites and returned extraterrestrial material prior to detailed chemical and mineralogical analyses. Although micro-CT imaging is generally considered to be a non-destructive technique since silicate and metallic minerals in chondrites are not affected by X-ray exposures at the intensities and wavelengths typically used, there are concerns that the use of micro-CT could be detrimental to the organics in carbonaceous chondrites. We recently conducted a synchrotron micro-CT experiment on a powdered sample of the Murchison CM2 carbonaceous chondrite exposed to a monochromatic high energy (approximately 48 kiloelectronvolts) total X-ray radiation dose of approximately 1 kilogray (kGy) using the Advanced Photon Source beamline 13-BMD (13-Bending Magnet-D Beamline) at Argonne National Laboratory and found that there were no detectable changes in the amino acid abundances or enantiomeric compositions in the chondrite after exposure relative to a Murchison control sample that was not exposed. However, lower energy bremsstrahlung X-rays could interact more with amino acids and other lower molecular weight amines in meteorites. To test for this possibility, three separate micro-CT imaging experiments of the Murchison meteorite using the GE Phoenix v/tome/x s 240 kilovolt microfocus high resolution tungsten target X-ray tube instrument at the American Museum of Natural History (AMNH) were conducted and the amino acid abundances and enantiomeric compositions were determined. We also investigated the abundances of the C1-C5 amines in Murchison which were not analyzed in the first study.
Microtomography Imaging↗
X-Ray Micro- and Nano-Tomography Analysis of Bennu Samples: A Preliminary Report
X-ray tomography (XCT) is an effective technique for obtaining the 3D structures of returned samples. XCT using synchrotron radiation provides high-resolution CT images with quantitative information. The XCT systems at SPring-8, an SR facility in Japan, have been used to analyze samples returned from the asteroids Itokawa and Ryugu. In this study, we plan to apply SR-XCT to samples returned from the asteroid Bennu.
A Tsuchiyama↗
The electron spectra in the synchrotron nebula of the supernova remnant G 29.7-0.3
EXOSAT results obtained with the imaging instrument (CMA) and the medium energy proportional counters (ME) are discussed. Assuming that the featureless power-law spectrum obtained in the 2 to 10 keV range is synchrotron radiation from relativistic electrons, one derives constraints on magnetic field strength and age of the nebula. The energy spectra of the electrons responsible for the emission in the radio and X-ray ranges are discussed. The great similarity of the physical properties of G 29.7-0.3 and of three synchrotron nebulae containing a compact object observed to pulse in X-rays makes G 29.7 - 0.3 a very promising candidate for further search for pulsed emission. Further observations at infrared wavelengths might reveal the break(s) in the emitted spectrum expected from the radio and X-ray power-law indices and give us more information on the production of the electron populations responsible for the emission of the nebula.
Koch-Miramond, L.↗
High Angular Resolution ALMA Images of Dust and Molecules in the SN 1987A Ejecta
We present high angular resolution (∼80 mas) ALMA continuum images of the SN1987A system, together with CO J = 21, J = 65, and SiO J = 54 to J = 76 images, which clearly resolve the ejecta (dust continuum and molecules) and ring (synchrotron continuum) components. Dust in the ejecta is asymmetric and clumpy, and overall the dust fills the spatial void seen in Hα images, filling that region with material from heavier elements. The dust clumps generally fill the space where CO J = 6 5 is fainter, tentatively indicating that these dust clumps and CO are locationally and chemically linked. In these regions, carbonaceous dust grains might have formed after dissociation of CO. The dust grains would have cooled by radiation, and subsequent collisions of grains with gas would also cool the gas, suppressing the CO J = 6 5 intensity. The data show a dust peak spatially coincident with the molecular hole seen in previous ALMA CO J = 2 1 and SiO J = 5 4 images. That dust peak, combined with CO and SiO line spectra, suggests that the dust and gas could be at higher temperatures than the surrounding material, though higher density cannot be totally excluded. One of the possibilities is that a compact source provides additional heat at that location. Fits to the far-infrared–millimeter spectral energy distribution give ejecta dust temperatures of 18–23 K. We revise the ejecta dust mass to Mdust = 0.2–0.4 Mfor carbon or silicate grains, or a maximum of <0.7 Mfor a mixture of grain species, using the predicted nucleosynthesis yields as an upper limit.
Interstellar dust↗
Direct Measurement of the Composition of Aqueous Fluids from the Parent Body of Asteroid 162173 Ryugu
Imaging using X-ray absorption contrast by synchrotron nano-computed tomography (47.4 nm/voxel, 7keV) of a Ryugu pyrrhotite crystal (C0002-FC012-from the second touch-down site) revealed probable fluid inclusions (Fig. 1A,B) [1]. The inclusions were completely encapsuled in pyrrhotite, suggesting the fluids were trapped in the early stages of crystal growth, and filled with low-Z material. We performed Time-of Flight-Secondary Ion Mass Spectrometry (TOF-SIMS) depth profiling and high-resolution map-ping at -120°C to exposure and measure the composition of the trapped fluids in a frozen state.
M Zolensky↗
Update on Measurement of the Composition of Ryugu Fluid Inclusions
Imaging using X-ray absorption contrast by synchrotron nano-computed tomography of a Ryugu pyrrhotite crystal (C0002-FC012 - from the second Hayabusa2 spacecraft touch-down site) revealed probable fluid inclusions in the center of a crystal of pyrrhotite, suggesting the parent fluids were trapped in the early stages of crystal growth on Ryugu’s parent asteroid. We previously described the performance of Time-of Flight-Secondary Ion Mass Spectrometry (TOF-SIMS) depth profiling and high-resolution mapping at -120°C to expose and measure the composition of the trapped fluids in a frozen state in two Ryugu inclusions [1,2]. Here we report results from follow-on measurements of additional inclusions in the same pyrrhotite crystal, and the initial results of measurement of standards. The ultimate goal is to reveal the quantitative composition of the fluids that caused aqueous alteration, in particular the H2O:CO2 ratio, which will also facilitate cosmochemical modeling of the alteration process.
M Zolensky↗
Direct Analyses of Aqueous Fluids from C-Class Asteroid 162173 Ryugu
Imaging using X-ray absorption contrast by synchrotron nano-computed tomography (47.4 nm/voxel, 7keV) of a Ryugu pyrrhotite crystal revealed probable fluid inclusions. The inclusions were completely encapsuled in pyrrhotite, suggesting the fluids were trapped in the early stages of crystal growth, and filled with low-Z material. We performed Time-of Flight-Secondary Ion Mass Spectrometry (TOF-SIMS) depth profiling and high-resolution mapping at -120°C to exposure and measure the composition of the trapped fluids in a frozen state. These measurements revealed that the ancient, trapped fluids on Ryugu’s parent asteroid were saline aqueous solutions containing H2O, CO2, sulfur species, and nitrogen- and chlorine-bearing organic compounds identified by representative secondary ion species including O(-), OH(-), CO(-), S(-), Cl(-), C2(-), C2H(-), and CN(-). The inferred presence of CO2 indicates formation of the sulfides, and by implication the Ryugu parent body, beyond the H2O and CO2 snow lines of the early solar system, i.e. > 3-4 au from the Sun.
M Zolensky↗
Real Time In Situ Observations of Equiaxed Dendrite Coherency in Al-Cu Alloys Using High-Brilliance, 3rd Generation Synchrotron Sources
In the last decade synchrotron X-ray sources have fast become the tool of choice for performing in-situ high resolution imaging during alloy solidification. This paper presents the results of an experimental campaign carried out at the European Synchrotron Radiation Facility, using a Bridgman furnace, to monitor phenomena during solidification of Al-Cu alloys - specifically the onset of equiaxed dendrite coherency. Conventional experimental methods for determining coherency involve measuring the change in viscosity or measuring the change in thermal conductivity across the solidifying melt Conflicts arise when comparing the results of these experimental techniques to find a relationship between cooling rate and coherency fraction. It has been shown that the ratio of average velocity to the average grain diameter has an inversely proportional relationship to coherency fraction. In-situ observation therefore makes it possible to measure these values directly from acquired images sequences and make comparisons with published results.
Murphy, Andrew G.↗
The synchrotron bays of the Crab Nebula - A magnetic structure associated with a presupernova circumstellar disk
We investigate the nature of two large conical indentations in the Crab Nebula's synchrotron emission, commonly known as the east and west 'bays'. Optical images spanning nearly nine decades (1899-1988) reveal the bays to be long-lasting remnant features. Proper motions of the bays away from the remnant's center of expansion are consistent with their locations near the SN progenitor site in A.D. 1054. Based on their morphologies and polarization properties, the bays appear to be portions of a torus encircling the remnant's center of expansion. The nebular magnetic field wrapped around this torus blocks the pulsar's relativistic particles, resulting in the observed lack of synchrotron emission. We propose that this torus is the result of a presupernova disklike ejection not less than 0.1 solar mass by the Crab progenitor, similar to the ring around SN 1987 A. A 0.5 solar mass disk of He-rich filaments along the equatorial plane is probably also related to presupernova mass loss, which might explain the wide range of abundances seen among filaments.
Fesen, Robert A.↗
From Tomography to Material Properties of Thermal Protection Systems
The X-ray micro-tomography technique provides non-destructive characterizations of three-dimensional material micro-structures at spatial resolutions from the sub-micron to the centimeter scale. High quality micro-tomography images of NASA Thermal Protection System (TPS) materials are obtained using one of the brightest synchrotron X-ray sources available. Leveraging on NASA supercomputing capabilities, material properties and response are computed from tomography-data. This talk highlights the process and challenges of going from 3D images of actual material structures to simulations of properties and phenomena relevant to TPS material response, such as thermal conductivity, permeability, mass transport and high temperature reactions. The talk is addressed to a broad audience including scientists, engineers, researchers, educators, programmers, managers, and members of the media.
tomography↗
In Situ Synchrotron Micro-CT of Microballoon-Filled RTV Silicone During Thermal Decomposition
This work investigates the thermal decomposition of microballoon-filled room-temperature-vulcanizing (RTV) silicone using time-resolved synchrotron micro-CT at the Advanced Light Source. In situ imaging of constrained and unconstrained samples captures the evolution of the internal microstructure during heating, including material expansion, microballoon and void growth, tearing, pyrolysis, shrinkage, and increasing porosity. The measurements provide new insight into the mechanisms governing RTV degradation and generate three-dimensional data for future quantitative analysis and material-response model development.
TPS↗
Properties and Spatial Distribution of Dust Emission in the Crab Nebula
The nature and quantity of dust produced in supernovae (SNe) is still poorly understood. Recent IR observations of freshly-formed dust in supernova remnants (SNRs) have yielded significantly lower dust masses than predicted by theoretical models and observations high-redshift galaxies. The Crab Nebula's pulsar wind is thought to be sweeping up freshly-formed SN dust along with the SN ejecta. The evidence for this dust was found in the form of an IR bump in the integrated spectrum of the Crab and in extinction against the synchrotron nebula that revealed the presence of dust in the filament cores. We present the first spatially-resolved emission spectra of dust in the Crab Nebula acquired with the Spitzer Space Telescope. The IR spectra are dominated by synchrotron emission and show forbidden line emission from both sides of the expanding nebula, including emission from [S III], [Si II], [Ne II], [Ne III], [Ne V], [Ar III], [Ar V], [Fe II], and [Ni II]. We extrapolated a synchrotron spectral data cube from the Spitzer 3.6 and 4.5 micron images, and subtracted this contribution from our 15-40 micron spectral data to produce a map of the residual continuum emission from dust. The emission appears to be concentrated along the ejecta filaments and is well described by astronomical silicates at an average temperature of 65 K. The estimated mass of dust in the Crab Nebula is 0.008 solar masses.
Sonneborn, G.↗
X-ray Observations of Cosmic Ray Acceleration
Since the discovery of cosmic rays, detection of their sources has remained elusive. A major breakthrough has come through the identification of synchrotron X-rays from the shocks of supernova remnants through imaging and spectroscopic observations by the most recent generation of X-ray observatories. This radiation is most likely produced by electrons accelerated to relativistic energy, and thus has offered the first, albeit indirect, observational evidence that diffusive shock acceleration in supernova remnants produces cosmic rays to TeV energies, possibly as high as the "knee" in the cosmic ray spectrum. X-ray observations have provided information about the maximum energy to which these shOCks accelerate electrons, as well as indirect evidence of proton acceleration. Shock morphologies measured in X-rays have indicated that a substantial fraction of the shock energy can be diverted into particle acceleration. This presentation will summarize what we have learned about cosmic ray acceleration from X-ray observations of supernova remnants over the past two decades.
Petre, Robert↗
Hubble Space Telescope Observations of Oxygen-rich Supernova Remnants in the Magellanic Clouds. III. WFPC2 Imaging of the Young, Crab-like Supernova Remnant SNRO540-69.3
Hubble Space Telescope images with the Wide Field Planetary Camera 2 of the young, oxygen-rich, Crab-like supernova remnant SNR0540-69.3 in the Large Magellanic Cloud (LMC) reveal details of the emission distribution and the relationship between the expanding ejecta and synchrotron nebula. The emission distributions appear very similar to those seen in the Crab nebula, with the ejecta located in a thin envelope surrounding the synchrotron nebula. The [O III] emission is more extended than other tracers, forming a faint "skin" around the denser filaments and synchrotron nebula, as also observed in the Crab. The [O III] exhibits somewhat different kinematic structure in long-slit spectra, including a more extended high-velocity emission halo not seen in images. Yet even the fastest expansion speeds in SNR 0540 s halo are slow when compared to most other young supernova remnants, though the Crab nebula has similar slow expansion speeds. We show a striking correspondence between the morphology of the synchrotron nebula observed in an optical continuum filter with that recently resolved in Chandra X-ray images. We argue that the multi-component kinematics and filamentary morphology of the optical emission-line features likely result from magnetic Rayleigh-Taylor instabilities that form as the synchrotron nebula expands and sweeps up ejecta, as seen in the Crab nebula. Our images and spectra help to refine our understanding of SNR 0540 in several more detailed respects: they confirm the identification of H(alpha)+[N II] in the red spectrum, they show that the systemic velocity of SNR 0540 is not significantly different from that of the LMC, and they hint at a lower Ne abundance than the Crab (potentially indicating a more massive progenitor star).
Morse, Jon A.↗