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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 37 records · Page 2
All sourcesNASA NTRSDOE OSTI
NASA NTRS1989

A study of microstructural characteristics and differential thermal analysis of Ni-based superalloys

The objective of this work is to correlate the mechanical properties of the Ni-based superalloy MAR M246(Hf) used in the Space Shuttle Main Engine with its structural characteristics by systematic study of optical photomicrographs and differential thermal analysis. The authors developed a method of predicting the liquidus and solidus temperature of various nickel based superalloys (MAR-M247, Waspaloy, Udimet-41, polycrystalline and single crystals of CMSX-2 and CMSX-3) and comparing the predictions with the experimental differential thermal analysis (DTA) curves using Perkin-Elmer DTA 1700. The method of predicting these temperatures is based on the additive effect of the components dissolved in nickel. The results were compared with the experimental values.

Aggarwal, M. D.↗
NASA NTRS1985

Theoretical interpretation of thermal arrest data from differential thermal analysis measurements

A theory was developed to interpret the thermal arrest data of HgCdTe system from differential thermal analysis measurements. A nonlinear regression program is used to model fit the data. The purpose is to obtain a set of parameters which will give the information about average radiation coefficient, latent heat of fussion, and specific heat of the HgCdTe system at various compositions. The liquidus and solidus at various compositions are also obtained. The heat radiation from the furnace, heat radiation from the system, heat capacity from both the system and the quartz tube and the heat of fusion of the system are considered, however, it neglects heat transfer through conduction and convection.

Wang, J. C.↗
NASA NTRS1990

Determining the nucleation rate curve for lithium disilicate glass by differential thermal analysis

The crystallization of lithium disilicate (Li2O+2SiO2) glass nucleated at various temperatures was studied by differential thermal analysis (DTA). A plot of the DTA crystallization peak height versus nucleation temperature closely resembles the classical nucleation rate curve for lithium disilicate glass whose maximum is at 453 C. The glass becomes saturated with internal nuclei when heated at 453 C for 10 h. The activation energy for crystallization and the heat of crystallization are independent of the concentration of nuclei and are 249 + or - 10 and 67 + or - 3 kJ/mol, respectively. The Avrami exponent, n, depends strongly on the concentration of nuclei in the glass.

Ray, Chandra S.↗
NASA NTRS1978

Analysis of differential absorption lidar from the Space Shuttle

A parametric analysis of the Shuttle-borne differential absorption lidar concept for the measurement of atmospheric trace constituent profiles in the nadir viewing mode is presented. The criterion of an optimum constituent optical depth is developed and applied to generate estimates of range resolved measurement errors. These errors emphasize the fundamental limitations for establishing the feasibility of range-resolved differential absorption lidar measurements from Shuttle. With current lidar system technology, atmospheric backscatter density profiles may be adequately determined up to about 60-km altitude at the doubled-ruby wavelength, 3472 A, for a 1-J/pulse laser and a 1-sq m receiver. Potential range-resolved measurements of stratospheric and mesospheric trace constituents by differential absorption from Shuttle altitudes are limited to H2O, CH4, N2O, O3, and CO, species which can be more easily measured by passive limb viewing techniques. Range-resolved water vapor data for the lower troposphere may be obtained with accuracies which would be competitive with those from passive sensors.

Remsberg, E. E.↗
NASA NTRS2005

Crystallization Kinetics of a Solid Oxide Fuel Cell Seal Glass by Differential Thermal Analysis

Crystallization kinetics of a barium calcium aluminosilicate glass (BCAS), a sealant material for planar solid oxide fuel cells, have been investigated by differential thermal analysis (DTA). From variation of DTA peak maximum temperature with heating rate, the activation energy for glass crystallization was calculated to be 259 kJ/mol. Development of crystalline phases on thermal treatments of the glass at various temperatures has been followed by powder x-ray diffraction. Microstructure and chemical composition of the crystalline phases were investigated by scanning electron microscopy and energy dispersive spectroscopic (EDS) analysis. BaSiO3 and hexacelsian (BaAl2Si2O8) were the primary crystalline phases whereas monoclinic celsian (BaAl2Si2O8) and (Ba(x), Ca(y))SiO4 were also detected as minor phases. Needle-shaped BaSiO3 crystals are formed first, followed by the formation of other phases at longer times of heat treatments. The glass does not fully crystallize even after long term heat treatments at 750 to 900 C.

Bansal, Narottam P.↗
NASA NTRS1983

Simulation and analysis of differential global positioning system for civil helicopter operations

A Differential Global Positioning System (DGPS) computer simulation was developed, to provide a versatile tool for assessing DGPS referenced civil helicopter navigation. The civil helicopter community will probably be an early user of the GPS capability because of the unique mission requirements which include offshore exploration and low altitude transport into remote areas not currently served by ground based Navaids. The Monte Carlo simulation provided a sufficiently high fidelity dynamic motion and propagation environment to enable accurate comparisons of alternative differential GPS implementations and navigation filter tradeoffs. The analyst has provided the capability to adjust most aspects of the system, the helicopter flight profile, the receiver Kalman filter, and the signal propagation environment to assess differential GPS performance and parameter sensitivities. Preliminary analysis was conducted to evaluate alternative implementations of the differential navigation algorithm in both the position and measurement domain. Results are presented to show that significant performance gains are achieved when compared with conventional GPS but that differences due to DGPS implementation techniques were small. System performance was relatively insensitive to the update rates of the error correction information.

Denaro, R. P.↗
NASA NTRS1971

Similarity analysis of differential equations by Lie group.

Methods for transforming partial differential equations into forms more suitable for analysis and solution are investigated. The idea of Lie's infinitesimal contact transformation group is introduced to develop a systematic method which involves mostly algebraic manipulations. A thorough presentation of the application of this general method to the problem of similarity analysis in a broader sense - namely, the similarity between partial and ordinary differential equations, boundary value and initial value problems, and nonlinear and linear equations - is given with new and very general methods evolved for deriving the possible groups of transformations.

Na, T. Y.↗
NASA NTRS1971

Differential thermal analysis and gas release studies of Apollo 11 samples.

The liquidus-solidus behavior of Apollo 11 lunar fines and the evolution characteristics of CO, nitrogen, He, Ne, and Ar were investigated by use of the combined techniques of high-vacuum differential thermal analysis (DTA) and mass spectrometry between 100 and 1500 C. The DTA thermogram has shown that the lunar fines undergo partial melting over a broad range of temperature from about 915 to 1300 C, with a significant initial melting of glassy and crystalline components within the fines at about 1140 C. The lunar material becomes a homogeneous melt at about 1300 C.

Wachi, F. M.↗
DOE OSTI2024

Lectures on Lie Group Analysis: Solving Differential Equations Using Symmetries

These notes are meant to be a supplemental reference for the beginner Lie Group Analyst. It is assumed that the reader has a basic concept of the fundamentals of Lie Group Theory (LGT), e.g. has seen the derivation of the infinitesimal generator and understands the mathematical meaning behind invariance. An excellent reference is Albright et al., “Symmetry Analysis of Differential Equations: A Primer,”. The reader is urged to read at least the first three chapters of that document to be able to follow the outset of Chapter 2 of this document. The reader should also have a general understanding of calculus, ordinary differential equations, and partial differential equations.

97 MATHEMATICS AND COMPUTING↗
NASA NTRS1982

Nonlinear zero-sum differential game analysis by singular perturbation methods

A class of nonlinear, zero-sum differential games, exhibiting time-scale separation properties, can be analyzed by singular-perturbation techniques. The merits of such an analysis, leading to an approximate game solution, as well as the 'well-posedness' of the formulation, are discussed. This approach is shown to be attractive for investigating pursuit-evasion problems; the original multidimensional differential game is decomposed to a 'simple pursuit' (free-stream) game and two independent (boundary-layer) optimal-control problems. Using multiple time-scale boundary-layer models results in a pair of uniformly valid zero-order composite feedback strategies. The dependence of suboptimal strategies on relative geometry and own-state measurements is demonstrated by a three dimensional, constant-speed example. For game analysis with realistic vehicle dynamics, the technique of forced singular perturbations and a variable modeling approach is proposed. Accuracy of the analysis is evaluated by comparison with the numerical solution of a time-optimal, variable-speed 'game of two cars' in the horizontal plane.

Sinar, J.↗
DOE OSTI2020

Hyper-Differential Sensitivity Analysis of Uncertain Parameters in PDE-Constrained Optimization

Many problems in engineering and sciences require the solution of large scale optimization constrained by partial differential equations (PDEs). Though PDE-constrained optimization is itself challenging, most applications pose additional complexity, namely, uncertain parameters in the PDEs. Uncertainty quantification (UQ) is necessary to characterize, prioritize, and study the influence of these uncertain parameters. Sensitivity analysis, a classical tool in UQ, is frequently used to study the sensitivity of a model to uncertain parameters. In this article, we introduce "hyper-differential sensitivity analysis" which considers the sensitivity of the solution of a PDE-constrained optimization problem to uncertain parameters. Our approach is a goal-oriented analysis which may be viewed as a tool to complement other UQ methods in the service of decision making and robust design. We formally define hyper-differential sensitivity indices and highlight their relationship to the existing optimization and sensitivity analysis literatures. Assuming the presence of low rank structure in the parameter space, computational efficiency is achieved by leveraging a generalized singular value decomposition in conjunction with a randomized solver which converts the computational bottleneck of the algorithm into an embarrassingly parallel loop. Two multi-physics examples, consisting of nonlinear steady state control and transient linear inversion, demonstrate efficient identification of the uncertain parameters which have the greatest influence on the optimal solution.

97 MATHEMATICS AND COMPUTING↗
NASA NTRS1998

Differential Thermal Analysis of Hg(1-x)Mn(x)Te Alloys in the X=0 to 0.3 Range

Understanding the experimental conditions necessary for the development of radial and axial compositional homogeneity in directionally solidified Hg(0.89)Mn(0.11)Te(MMT) crystals has been difficult due to the lack of segregation coefficient data on the Hg(1-x)Mn(x)Te alloy system in the X = 0 to 0.3 composition range. Determining segregation coefficient data from the available Hg(1-x)Mn(x)Te alloy phase equilibria data is not practical due to discrepancies in the shape of the reported solidus and liquidus curves in the X = 0 to 0.3 range. To resolve these discrepancies and to obtain segregation coefficient data which can be used to understand homogeneity in directionally solidified MMT crystals, the solidus and liquidus temperatures of seven Hg(1-x)Mn(x)Te alloys in the X = 0 to 0.3 range were determined using differential thermal analysis (DTA). The Hg(1-x)Mn(x)Te phase diagram constructed for the X = 0 to 0.3 range of this alloy system from the DTA measurements clarifies the shape of the solidus and liquidus curves in this range. The segregation coefficient for the Hg(1-x)Mn(x)Te system was found to vary from 5 to 4.4 as the solidus composition increased from 0-30 atomic percent MnTe. This information will be useful in the analysis of axial and radial homogeneity of directionally solidified MMT crystals.

Price, M. W.↗
NASA NTRS1983

An Evaluation of Techroll Seal Flexible Joint Material

This study evaluated the materials utilized in the flexible joint for possible failure modes. Studies undertaken included effect of temperature on the strength of the system, effect of fatigue on the strength of the system, thermogravimetric analysis, thermochemical analysis, differential scanning calorimeter analysis, dynamic mechanical analysis, and peel test. These studies indicate that if the joint failed due to a materials deficiency, the most likely mode was excessive temperature in the joint. In addition, the joint material is susceptible to fatigue damage which could have been a contributing factor.

Hall, W. B.↗
NASA NTRS1984

Materials testing of the IUS techroll seal material

As a part of the investigation of the control system failure Inertial Upper Stage on IUS-1 flight to position a Tracking and Data Relay Satellite (TDRS) in geosynchronous orbit, the materials utilized in the techroll seal are evaluated for possible failure models. Studies undertaken included effect of temperature on the strength of the system, effect of fatigue on the strength of the system, thermogravimetric analysis, thermomechanical analysis, differential scanning calorimeter analysis, dynamic mechanical analysis, and peel test. The most likely failure mode is excessive temperature in the seal. In addition, the seal material is susceptible to fatigue damage which could be a contributing factor.

Nichols, R. L.↗