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NASA NTRS1974

Effects of ultrasonic fields in the phosphoric acid process

A process of apatite decomposition with sulfuric acid was studied under the influence of ultrasound in the phosphoric acid production process. The studies were carried out with and without ultrasonic fields in the reaction mixture, which resembled the mixing ratio used in technical production processes. Ultrasound with a frequency of 20 kHz and an intensity of 1 W/sq cm was used in the studies. A very favorable ultrasonic effect upon the degree of apatite decomposition was observed. The ultrasonic field affects the shape of byproduct gypsum crystals. In the H3PO4 production process without ultrasound, the byproduct gypsum crystallizes as long, thin needles which cause problems in filtration. In the trials involving the application of wound, gypsum crystallized in the form of small platelets possessing a favorable ratio of length to width.

Kowalska, E.↗

NASA NTRS1998

JANNAF 17th Propulsion Systems Hazards Subcommittee Meeting

Volume 1, the first of two volumes is a compilation of 16 unclassified/unlimited technical papers presented at the 17th meeting of the Joint Army-Navy-NASA-Air Force (JANNAF) Propulsion Systems Hazards Subcommittee (PSHS) held jointly with the 35th Combustion Subcommittee (CS) and Airbreathing Propulsion Subcommittee (APS). The meeting was held on 7 - 11 December 1998 at Raytheon Systems Company and the Marriott Hotel, Tucson, AZ. Topics covered include projectile and shaped charge jet impact vulnerability of munitions; thermal decomposition and cookoff behavior of energetic materials; damage and hot spot initiation mechanisms with energetic materials; detonation phenomena of solid energetic materials; and hazard classification, insensitive munitions, and propulsion systems safety.

Cocchiaro, James E.↗

NASA NTRS1983

Algorithms for on-line parameter and mode shape estimation

Algorithms are presented for on-line parameter and mode-shape estimation. The approach used is based upon a modal decomposition of the dynamic response of the flexible structure and is designed to make use of the parallel processing features of modern minicomputers. Satisfactory performance of the parallel structure identification technique used can be achieved only when the approximation functions noted correspond to the natural modes of the flexible structure. The work summarized here presents a technique for estimating both mode shapes and modal parameters.

Thau, F. E.↗

NASA NTRS2010

Computational Analysis of Arc-Jet Wedge Tests Including Ablation and Shape Change

Coupled fluid-material response analyses of arc-jet wedge ablation tests conducted in a NASA Ames arc-jet facility are considered. These tests were conducted using blunt wedge models placed in a free jet downstream of the 6-inch diameter conical nozzle in the Ames 60-MW Interaction Heating Facility. The fluid analysis includes computational Navier-Stokes simulations of the nonequilibrium flowfield in the facility nozzle and test box as well as the flowfield over the models. The material response analysis includes simulation of two-dimensional surface ablation and internal heat conduction, thermal decomposition, and pyrolysis gas flow. For ablating test articles undergoing shape change, the material response and fluid analyses are coupled in order to calculate the time dependent surface heating and pressure distributions that result from shape change. The ablating material used in these arc-jet tests was Phenolic Impregnated Carbon Ablator. Effects of the test article shape change on fluid and material response simulations are demonstrated, and computational predictions of surface recession, shape change, and in-depth temperatures are compared with the experimental measurements.

Goekcen, Tahir↗

NASA NTRS1973

Development of a process for producing ribbon shaped boron filaments

A ribbon-shaped boron filament with a tensile strength of 138 KN/sq cm (200 ksi) was investigated. The investigation was carried out using both carbon and tungsten as substrate materials. No satisfactory results were obtained utilizing uncoated, copper-plated or silicon carbide coated tungsten ribbon substrates. Carbon ribbon substrates were prepared by pyrolysis of stretched polyimide tape. A severe deposition gradient occurred in all dc reactor experiments due to convective cooling at the edge of the substrate that resulted in a weak, nonuniform filament. RF heating, however, completely eliminated this gradient problem and a 90 cm (35.5 in.) long boron ribbon was produced at .85 cm/sec (100 ft/hr) using a frequency of 40.68 megahertz. This boron ribbon, however, exhibited a light-bulb effect during deposition to 59 KN/sq cm (85.7 ksi) were obtained from this ribbon. Several silicon carbide ribbon shaped filaments were also produced during this investigation by decomposition of CH3SiHCl2 onto carbon substrates. Contrary to the boron work, silicon carbide ribbon was readily prepared in dc static reactors. A very uniform and smooth deposition was obtained with strengths up to 71.1 KN/sq cm (103.5 ksi).

Basche, M.↗

NASA NTRSDate not supplied

Stability Analysis of the Flow Over a Swept Forward-Facing Step Using PIV Base Flows

Step excrescences are a type of surface imperfection encountered on swept wings of commercial aircraft, commonly because accessibility requirements prevent creating the wing’s surface from a single panel. If the step height is too large, super-critical, the flow can undergo an early transition to turbulence, which can be highly detrimental for the performance of the wing. In the case of a forward-facing step on a swept wing in a low-disturbance environment, stationary crossflow vortices can develop a significant amplitude upstream of the step and hence dominate the structure of the boundary-layer flow over the step. The main goal of the present investigation is to illuminate the path to transition supported by the fascinatingly complex flow field in the direct downstream vicinity of a step with a super critical height. The high-resolution, stereographic Particle Image Velocimetry (PIV) measurement dataset presently available for this flow field provides a complete description of the laminar flow for the execution of BiGlobal stability analysis in a plane parallel to the step. Although the notorious sensitivity of stability results to the description of the base flow demands a very careful uncertainty analysis of those results, it is argued that this very fact can be leveraged to produce new insight into the supported perturbation dynamics. In performing the analysis, several unsteady mode families are discovered that display the explosive perturbation expected for early transition to be induced. In considering domain widths equal to an integer-multiple of the incident crossflow-vortex wavelength and analyzing an extent of 5 crossflow-vortex wavelengths parallel to the step, it is found that the stability results converge while increasing the domain width. It is demonstrated, moreover, that the results for the wider domains can be approximated by appropriately averaging the results on neighboring single-crossflow-vortex-wavelength domains covering the same region. Besides being useful for computational purposes, this observed property suggests interpreting the instability mechanism as a distorted primary mechanism rather than a “proper” secondary mechanism. This follows in the context of the secondary in-stability analysis of three-dimensional boundary layers, because the secondary mechanism is usually characterized by being localized in a pocket of strong shear, while the distorted primary mechanism typically has an infinite support in the direction parallel to the step. Even though the growth rates are found to be sensitive to the interrogation-window size inherent to the PIV post-processing procedure, the spatial structure of the eigenfunctions is found to be relatively insensitive. Lastly, the spatial structure of the eigenfunctions corresponding to all velocity components are matched with the shape functions determined by computing the Spectral Proper Orthogonal Decomposition (SPOD) of a time-resolved measurement of the perturbation content.

forward-facing step↗

NASA NTRS2010

Validation of a Three-Dimensional Ablation and Thermal Response Simulation Code

The 3dFIAT code simulates pyrolysis, ablation, and shape change of thermal protection materials and systems in three dimensions. The governing equations, which include energy conservation, a three-component decomposition model, and a surface energy balance, are solved with a moving grid system to simulate the shape change due to surface recession. This work is the first part of a code validation study for new capabilities that were added to 3dFIAT. These expanded capabilities include a multi-block moving grid system and an orthotropic thermal conductivity model. This paper focuses on conditions with minimal shape change in which the fluid/solid coupling is not necessary. Two groups of test cases of 3dFIAT analyses of Phenolic Impregnated Carbon Ablator in an arc-jet are presented. In the first group, axisymmetric iso-q shaped models are studied to check the accuracy of three-dimensional multi-block grid system. In the second group, similar models with various through-the-thickness conductivity directions are examined. In this group, the material thermal response is three-dimensional, because of the carbon fiber orientation. Predictions from 3dFIAT are presented and compared with arcjet test data. The 3dFIAT predictions agree very well with thermocouple data for both groups of test cases.

Chen, Yih-Kanq↗

DOE OSTI2021

Parallel physics-informed neural networks via domain decomposition

Here we develop a distributed framework for the physics-informed neural networks (PINNs) based on two recent extensions, namely conservative PINNs (cPINNs) and extended PINNs (XPINNs), which employ domain decomposition in space and in time-space, respectively. This domain decomposition endows cPINNs and XPINNs with several advantages over the vanilla PINNs, such as parallelization capacity, large representation capacity, efficient hyperparameter tuning, and is particularly effective for multi-scale and multi-physics problems. Here, we present a parallel algorithm for cPINNs and XPINNs constructed with a hybrid programming model described by MPI + X, where X ∈ {CPUs, GPUs}. The main advantage of cPINN and XPINN over the more classical data and model parallel approaches is the flexibility of optimizing all hyperparameters of each neural network separately in each subdomain. We compare the performance of distributed cPINNs and XPINNs for various forward problems, using both weak and strong scalings. Our results indicate that for space domain decomposition, cPINNs are more efficient in terms of communication cost but XPINNs provide greater flexibility as they can also handle time-domain decomposition for any differential equations, and can deal with any arbitrarily shaped complex subdomains. To this end, we also present an application of the parallel XPINN method for solving an inverse diffusion problem with variable conductivity on the United States map, using ten regions as subdomains.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

DOE OSTI2024

Nanoscopic Imaging of Self-Propelled Ultrasmall Catalytic Nanomotors

Ultrasmall nanomotors (<100 nm) are highly desirable nanomachines for their size-specific advantages over their larger counterparts in applications spanning nanomedicine, directed assembly, active sensing, and environmental remediation. While there are extensive studies on motors larger than 100 nm, the design and understanding of ultrasmall nanomotors have been scant due to the lack of high-resolution imaging of their propelled motions with orientation and shape details resolved. Here, we report the imaging of the propelled motions of catalytically powered ultrasmall nanomotors─hundreds of them─at the nanometer resolution using liquid-phase transmission electron microscopy. These nanomotors are Pt nanoparticles of asymmetric shapes (“tadpoles” and “boomerangs”), which are colloidally synthesized and observed to be fueled by the catalyzed decomposition of NaBH4 in solution. Statistical analysis of the orientation and position trajectories of fueled and unfueled motors, coupled with finite element simulation, reveals that the shape asymmetry alone is sufficient to induce local chemical concentration gradient and self-diffusiophoresis to act against random Brownian motion. Our work elucidates the colloidal design and fundamental forces involved in the motions of ultrasmall nanomotors, which hold promise as active nanomachines to perform tasks in confined environments such as drug delivery and chemical sensing.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

NASA NTRS1986

A boundary element method for unsteady viscous flows

A potential vorticity method for the analysis of unsteady viscous incompressible flow past arbitrarily shaped objects is discussed which is based on the Helmholtz decomposition. It is found that the correct boundary condition to be imposed is on the normal component of the velocity for the cases of both inviscid and viscous flows. The no-slip condition is shown to be automatically satisfied for viscous flows. Numerical solutions for two-dimensional flow problems are given for attached flows in addition to those involving separation. The vorticity is confined, at least for the case of symmetric flows, to a small region in the immediate vicinity of the body, making possible the minimization of the number of node points in the field, and hence the computational time, without loss of accuracy.

Bharadvaj, B. K.↗

NASA NTRS1992

Approximation, abstraction and decomposition in search and optimization

In this paper, I discuss four different areas of my research. One portion of my research has focused on automatic synthesis of search control heuristics for constraint satisfaction problems (CSPs). I have developed techniques for automatically synthesizing two types of heuristics for CSPs: Filtering functions are used to remove portions of a search space from consideration. Another portion of my research is focused on automatic synthesis of hierarchic algorithms for solving constraint satisfaction problems (CSPs). I have developed a technique for constructing hierarchic problem solvers based on numeric interval algebra. Another portion of my research is focused on automatic decomposition of design optimization problems. We are using the design of racing yacht hulls as a testbed domain for this research. Decomposition is especially important in the design of complex physical shapes such as yacht hulls. Another portion of my research is focused on intelligent model selection in design optimization. The model selection problem results from the difficulty of using exact models to analyze the performance of candidate designs.

Ellman, Thomas↗

DOE OSTI2023

Solvent-free synthesis of lanthanide oxide and mixed lanthanide oxide nanoparticles

Lanthanide oxides and mixed lanthanide oxides can be produced using furnace or microwave assisted solid-state synthesis. The use of Ln-tri(methylsilyl)amide-based precursors yields spherical nanoparticles. The formation of spherical shaped nanoparticles is likely due to the preferential single-step decomposition of the Ln-TMS as well as the low activation energy to overcome decomposition. Reaction temperature, initial metal ion ratio, and reaction dwell time can be used to control the final nanoparticle size. The method enables solvent-free, high-yield synthesis of morphology-controlled lanthanide oxides.

Treadwell, LaRico Juan↗

NASA NTRS1982

Analytical electron microscope study of eight ataxites

Optical and electron optical (SEM, TEM, AEM) techniques were employed to investigate the fine structure of eight ataxite-iron meteorites. Structural studies indicated that the ataxites can be divided into two groups: a Widmanstaetten decomposition group and a martensite decomposition group. The Widmanstaetten decomposition group has a Type I plessite microstructure and the central taenite regions contain highly dislocated lath martensite. The steep M shaped Ni gradients in the taenite are consistent with the fast cooling rates, of not less than 500 C/my, observed for this group. The martensite decomposition group has a Type III plessite microstructure and contains all the chemical group IVB ataxites. The maximum taenite Ni contents vary from 47.5 to 52.7 wt % and are consistent with slow cooling to low temperatures of not greater than 350 C at cooling rates of not greater than 25 C/my.

Novotny, P. M.↗

DOE OSTI2021

Direct evidence for the role of microbial community composition in the formation of soil organic matter composition and persistence

The largest terrestrial carbon sink on earth is soil carbon stocks. As the climate changes, the rate at which the Earth’s climate warms depends in part on the persistence of soil organic carbon. Microbial turnover forms the backbone of soil organic matter (SOM) formation and it has been recently proposed that SOM molecular complexity is a key driver of stability. Despite this, the links between microbial diversity, chemical complexity and biogeochemical nature of SOM remain missing. Here we tested the hypotheses that distinct microbial communities shape the composition of SOM, and microbial-derived SOM has distinct decomposition potential depending on its community of origin. We inoculated microbial communities of varying diversities into a model soil matrix amended with simple carbon (cellobiose) and measured the thermal stability of the resultant SOM. Using a Rock-Eval ® ramped thermal analysis, we found that microbial community composition drives the chemical fingerprint of soil carbon. While diversity was not a driver of SOM composition, bacteria-only communities lead to more thermally labile soil C pools than communities with bacteria and fungi. Our results provide direct evidence for a link between microbial community structure, SOM composition, and thermal stability. This evidence demonstrates the relevance of soil microorganisms in building persistent SOM stocks.

Domeignoz-Horta, Luiz A. (ORCID:0000000346186253)↗

NASA NTRS1990

Rapid design of aerospace vehicle

This document presents in viewgraph form techniques for the optimal design of aerospace vehicles which take into account vehicle shape, aerodynamic performance, and weight minimization. Methods include multilevel optimization with linear decomposition, multi-constraint optimization, global sensitivity matrix, and calculation of sensitivity derivatives using both first and second order derivatives. The effects of including flexibility in the optimization is discussed.

Abdi, Frank↗

DOE OSTI2022

Diagnosis of the imploding shell asymmetry in polar-direct-drive deuterium–tritium cryogenic target implosions on OMEGA

We discuss the analyses of gated, x-ray imaging data from polar-direct-drive experiments with cryogenically layered deuterium–tritium targets on the OMEGA laser. The in-flight shell asymmetries were diagnosed at various times during the implosion, which was caused by the beam pointing geometry and preimposed variations in the energy partition between the different groups of laser beams. The shape of the ablation surface during the acceleration phase of the implosion was measured along two different lines of sight, and a Legendre mode (ℓ-mode) decomposition was applied for modes of up to ten to investigate shell asymmetries. A clear causal relationship between the imposed beam imbalance and the shape of the in-flight shell asymmetries was observed. The imploded shell with a balanced energy ratio shows smaller values of the amplitudes of ℓ-mode 2 compared to that from implosions with an imbalanced ring energy ratio. The amplitudes of ℓ-modes 4 and 6 are the same within the measurement uncertainty with respect to the change in beam energy ratio.

47 OTHER INSTRUMENTATION↗

NASA NTRS1989

Field structure of collapsing wave packets in 3D strong Langmuir turbulence

A simple model is constructed for the electric fields in the collapsing wave packets found in 3D simulations of driven and damped isotropic strong Langmuir turbulence. This model, based on a spherical-harmonic decomposition of the electrostatic potential, accounts for the distribution of wave-packet shapes observed in the simulations, particularly the predominance of oblate wave packets. In contrast with predictions for undamped and undriven subsonic collapse of scalar fields, oblate vector-field wave packets do not flatten during collapse but, instead, remain approximately self-similar and rigid.

Newman, D. L.↗

NASA NTRS1999

JANNAF 18th Propulsion Systems Hazards Subcommittee Meeting

This volume, the first of two volumes is a compilation of 18 unclassified/unlimited-distribution technical papers presented at the Joint Army-Navy-NASA-Air Force (JANNAF) 18th Propulsion Systems Hazards Subcommittee (PSHS) meeting held jointly with the 36th Combustion Subcommittee (CS) and 24th Airbreathing Propulsion Subcommittee (APS) meetings. The meeting was held 18-21 October 1999 at NASA Kennedy Space Center and The DoubleTree Oceanfront Hotel, Cocoa Beach, Florida. Topics covered at the PSHS meeting include: shaped charge jet and kinetic energy penetrator impact vulnerability of gun propellants; thermal decomposition and cookoff behavior of energetic materials; violent reaction; detonation phenomena of solid energetic materials subjected to shock and impact stimuli; and hazard classification, insensitive munitions, and propulsion systems safety.

Cocchiaro, James E.↗