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Preliminary Examination Process of Apollo Core 73002 - Insights and Lessons Learned From ANGSA for Future Sample Return Missions

Apollo Sample 73002 is part of a 2-foot long “drive tube” (73001/73002) of regolith that was collected from a landslide deposit near Lara Crater at the Apollo 17 site, Station 3. The double drive tube is believed to have penetrated a lunar landslide deposit that was transported from the slope of the South Massif into the TLV [1]. As part of the ANGSA (Apollo Next Generation Sample Analyses) initiative, preparing preliminary examination (PE) catalog of 73002 is a crucial first step for the early identification of material types such as rock fragments, and potential stratigraphy within the core. PE of Apollo core 73002 is distinct from science activities with the main goal to produces a sample catalog with a level of detail about sample characterization that is sufficient for the ANGSA PIs (and later on the lunar sample community) to select and request the samples to conduct their individual, scientific studies. Ultimately, the PE catalog of 73002 will help to establish a better understanding of the stratigraphy of the land slide deposit; the processes of the landslide including the trigger(s) and possibly number of landslide events, as well as the role of volatiles [1] and will aid in the careful preservation of the material for future studies [2].

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Exploring A Lunar Landslide Deposit In The Taurus-Littrow Valley (TLV). Variations In Mineralogy And Mineral Volatile Traps.

The double drive tube core sample (73001/73002), collected at Station 3 during the Apollo 17 mission, penetrated a lunar landslide deposit that was transported from the slope of the South Massif into the TLV (Figure 1). Orbital data suggest that this deposit represents multiple events that were triggered by movement along the Lee-Lincoln scarp [e.g., 1] or impact events [e.g., 2,3]. Although numerous core and trench samples were collected during the Apollo pro-gram and numerous landslide deposits have been identified on the lunar surface by orbital missions [e.g., 3], the Station 3 double drive tube is the only core that penetrated a landslide deposit. The intentions of our study are: to establish the stratigraphy of the deposit; to better understand the processes at work during the event(s), including the role of volatiles in the event(e.g., fluidization-enabled flow, escape of fluidizing volatiles) [1] and the capability of deposits for trapping indigenous volatiles; the number of landslide events; and the trigger(s) of such events. Here, we report some initial petrologic observations of the < 1mm fraction of the regolith. A companion abstract [4] emphasizes <1 mm lithic fragments, compares them to surface lithologies, and to > 4 mm lithic fragments.

M J Cato↗

Processing Frozen Apollo Samples in a Nitrogen Environment

A few weeks after their return to Earth, several Apollo 17 regolith sample splits and one Apollo 17 basalt were frozen at -20˚C (under dry gaseous N2 like all other pristine Apollo samples), and have remained essentially unstudied within the Apollo sample collection at NASA’s Johnson Space Center (JSC). As part of the Apollo Next Generation Sample Analysis (ANGSA) project, these frozen samples were selected for consortium study in 2019. Although the samples themselves were kept at -20˚C for nearly 50 years, the JSC Curation office has lacked a facility for processing frozen samples under pristine Apollo processing conditions. A temporary lab for this work was designed, built, and tested. Procedures were then developed for working in this unique environment, and the facility was sucessfully used to process the frozen Apollo samples for scientific allocation.

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From Apollo to Artemis: How Processing ANGSA Core Samples 73001/2 Can Help to Prepare for Future Sample Return Missions to the Moon and Beyond.

Introduction: Apollo Sample 73001/2 is a ~71cm long double drive tube consisting of an upper part (73002) and a lower part (73001) that contains regolith collected near Lara Crater at the Apollo 17 site, Station 3. The double drive tube is believed to have penetrated a lunar landslide deposit that was transported from the slope of the South Massif into the Taurus-Littrow Valley [1]. As part of the ANGSA (Apollo Next Generation Sample Analyses) initiative, preparing a preliminary examination (PE) catalog of 73001/2 is a crucial first step for the early identification of material types such as rock fragments and potential stratigraphy within the core. Many new curation and scientific tools such as X-ray computed tomography (XCT) [3], multi-spectral imaging [4], and gas extraction manifold with piercing tool [5-7], have been applied to the ANGSA core to benefit curation strategy, PE efforts, sample allocation to the planetary science community, and ultimately help to prepare for future sample return missions like Artemis. 73001/2 Preliminary Examination and Processing: Sample 73002 was successfully opened and extruded in Nov. 2019 and fully dissected at the end of 2021. Sample 73001 (Fig. 1) was successfully extruded in March 2022 after careful planning before opening the Core Sample Vacuum Container (CSVC) that was holding the drive tube of 73001. XCT, as part of PE, was used to scan the bottom and top part of the 73001 core tube within the CSVC prior to opening it to 1) facilitate non-destructive, rapid detection of any contamination potentials due to piercing of the CSVC during gas extraction [7]; and 2) to aid in the Artemis sample tool development and provide data on the knife edge seal of the CSVC. This knowledge will help us connect the mechanics of the implemented design (i.e., XCT data) to the performance of the seal (i.e., data on the gas samples will tell us how well the seal preserved the volatile record of lunar samples). Both type of information will feed forward into Artemis tool and storage strategies for future samples. Results and Lessons learned: The XCT data of the CSVC and core tube within showed that the bottom Teflon cap was not pierced during gas extraction (Fig. 1c) and thus, the sample integrity remained guaranteed during piercing and subsequent gas extraction. However, the XCT scan of the top of the core (Fig. 1b) revealed that the drive tube was overfilled with lunar soil and the tool that keeps the soil constrained within the drive tube was not fully deployed. These preliminary data allowed us to implement the necessary steps to prevent loss of sample integrity, including any potential stratigraphy shifts during extrusion. Processing Apollo core 73001/2, creating an informative PE catalog, and applying new and refined tools and technologies for sample analyses are invaluable activities that will assist in circumventing any potential pitfalls, aid in the characterization of samples, and help in the assessment of how well any lunar material has been collected and preserved in the past. This will aid in designing future sample collections and curation procedures and help to prepare for future human exploration and sampling missions such as Artemis. References: [1] Schmitt H. (2017) Icarus 298, 2-33. [3] Zeigler et al. (2021) LPSC 52nd, #2632; [4] Sun et al. (2021), LPSC 52nd, #1789; [5] Parai et al. (2021), LPSC 52nd #2665; [6] Schild et al. (2021) LPSC 52nd #1888; [7] McDonald (2022) ESL 2022.

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