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DOE OSTI2022

Acoustic focusing of microplastics in microfabricated and steel tube devices: An experimental study on the effects from particle size and medium density

The contamination of aquatic systems with microplastics is becoming a severe threat to living organisms. Microplastics found in the environment consist of a wide range of particle sizes thus give rise to several challenges to current purification methods. Acoustic focusing has been utilized as a particle concentrating method in biological and non-biological applications. In this study, we investigate the feasibility of using acoustic focusing technology to isolate microplastics in aqueous samples and find that a two-stage mechanism is essential to concentrate microplastics of wide size ranges of the same material. We demonstrate for the first time experimentally that when the particle size is comparable to the resonance wavelength, they deviate from typical pressure nodal focusing and show pressure antinodal focusing. Further, we have expanded microplastics isolation beyond microfluidic systems and demonstrate their extraction capabilities relatively at higher flow rates using microplastics of polystyrene, polyethylene, and polymethyl methacrylate ranging from 6 µm to 300 µm diameter and in devices fabricated with cylindrical steel tubes. We could extract 70% of microplastics smaller than 180 µm and 82% of microplastics greater than 180 µm in diameter from an aqueous sample at a flow rate of 12 mL/min. In conclusion, we demonstrate that small microplastics focus on acoustic pressure nodes regardless of the medium density. However, focusing of large microplastics of the same material depends on the medium density.

42 ENGINEERING↗

DOE OSTI2022

Super-strong magnetic field-dominated ion beam dynamics in focusing plasma devices

High energy density physics is the field of physics dedicated to the study of matter and plasmas in extreme conditions of temperature, densities and pressures. It encompasses multiple disciplines such as material science, planetary science, laboratory and astrophysical plasma science. For the latter, high energy density states can be accompanied by extreme radiation environments and super-strong magnetic fields. The creation of high energy density states in the laboratory consists in concentrating/depositing large amounts of energy in a reduced mass, typically solid material sample or dense plasma, over a time shorter than the typical timescales of heat conduction and hydrodynamic expansion. Laser-generated, high current–density ion beams constitute an important tool for the creation of high energy density states in the laboratory. Focusing plasma devices, such as cone-targets are necessary in order to focus and direct these intense beams towards the heating sample or dense plasma, while protecting the proton generation foil from the harsh environments typical of an integrated high-power laser experiment. A full understanding of the ion beam dynamics in focusing devices is therefore necessary in order to properly design and interpret the numerous experiments in the field. In this work, we report a detailed investigation of large-scale, kilojoule-class laser-generated ion beam dynamics in focusing devices and we demonstrate that high-brilliance ion beams compress magnetic fields to amplitudes exceeding tens of kilo-Tesla, which in turn play a dominant role in the focusing process, resulting either in a worsening or enhancement of focusing capabilities depending on the target geometry.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2021

The interplay between laser focusing conditions, expansion dynamics, ablation mechanisms, and emission intensity in ultrafast laser-produced plasmas

The interplay between ultrafast laser focusing conditions, emission intensity, expansion dynamics, and ablation mechanisms is critical to the detection of light isotopes relevant to nuclear energy, forensics, and geochemistry applications. Here, we study deuterium (2Hα) emission in plasmas generated from femtosecond laser ablation of a Zircaloy-4 target with a deuterium concentration of ≈37 at. %. Changes in emission intensity, plume morphology, crater dimensions, and surface modifications were investigated for varying focusing lens positions, where the laser was focused behind, at, and in front of the target. Spatially resolved optical emission spectroscopy and spectrally integrated plasma imaging were performed to investigate emission spectral features and plume morphology. Laser ablation crater dimensions and morphology were analyzed via optical profilometry and scanning electron microscopy. The 2Hα emission intensity showed significant reduction at the geometrical focal point or when the focal point is in front of the target. For all laser spot sizes, a two-component plume was observed but with different temporal histories. At the best focal point, the plume was spherical. When the laser was focused behind the target, the plume was elongated and propagated to farther distances than for the best focal position. In contrast, when the laser was focused in front of the target, filaments were generated in the beam path, and filament-plasma coupling occurred. By focusing the laser behind the target, the amount of material removal in the laser ablation process can be significantly reduced while still generating a plasma with a sufficient 2Hα emission signal for analysis.

Kautz, Elizabeth J. (ORCID:0000000263389223)↗

DOE OSTI2025

Enhanced quantum radiation with flying-focus laser pulses

The emission of a photon by an electron in an intense laser field is one of the most fundamental processes in electrodynamics and underlies the many applications that utilize high-energy photon beams. This process is typically studied for electrons colliding head-on with a stationary-focus laser pulse. Here, we show that the energy lost by electrons in the quantum regime and the yield of emitted photons can be substantially increased by replacing a stationary-focus pulse with an equal-energy flying-focus pulse whose focus co-propagates with the electrons. Furthermore, these advantages of the flying focus result from the energy loss and the photon yield scaling more favorably with the interaction time than the laser intensity in the quantum regime, with the latter also holding in the classical regime. Monte Carlo simulations of electrons colliding with equal-energy stationary and flying-focus laser pulses demonstrate these advantages.

Compton scattering↗

DOE OSTI2021

Relativistic flying laser focus by a laser-produced parabolic plasma mirror

Here, the question of electromagnetic field intensification towards the values typical for strong field quantum electrodynamics is of fundamental importance. One of the most promising intensification schemes is based on the relativistic-flying mirror concept, which shows that the electromagnetic radiation reflected by the mirror will be frequency upshifted by a factor of 4γ 2 (γ is the Lorentz factor of the mirror). In laser-plasma interactions, such a mirror travels with relativistic velocities through plasma and typically has a parabolic form, which is advantageous for light intensification. Thus, a relativistic-flying parabolic mirror reflects the counterpropagating radiation in the form of a focused and flying electromagnetic wave with a high frequency. The relativistic-flying motion of the laser focus makes the electric and magnetic field distributions of the focus complicated, and the mathematical expressions describing the field distributions of the focus become of fundamental interest. We present analytical expressions describing the field distribution formed by an ideal flying mirror which has a perfect reflectance over the entire surface and wavelength range. The peak field strength of an incident laser pulse with a center wavelength of λ 0 and an effective beam radius of w e is enhanced by a factor proportional to γ 3 (w e /λ 0 ) in the relativistic limit. Electron-positron pair production is investigated in the context of invariant fields based on the enhanced electromagnetic field. The pair production rate under the relativistic-flying laser focus is modified by the Lorentz γ-factor and the beam radius-wavelength ratio (w e /λ 0 ). We show that the electron-positron pairs can be created by colliding two counterpropagating relativistic-flying laser focuses in vacuum, each of which is formed when a 180 TW laser pulse is reflected by a relativistic-flying parabolic mirror with γ=12.2.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2023

Ultrabroadband flying-focus using an axiparabola-echelon pair

Flying-focus pulses promise to revolutionize laser-driven secondary sources by decoupling the trajectory of the peak intensity from the native group velocity of the medium over distances much longer than a Rayleigh range. Previous demonstrations of the flying focus have either produced an uncontrolled trajectory or a trajectory that is engineered using chromatic methods that limit the duration of the peak intensity to picosecond scales. Here we demonstrate a controllable ultrabroadband flying focus using a nearly achromatic axiparabola-echelon pair. Spectral interferometry using an ultrabroadband superluminescent diode was used to measure designed super- and subluminal flying-focus trajectories and the effective temporal pulse duration as inferred from the measured spectral phase. The measurements demonstrate that a nearly transform- and diffraction-limited moving focus can be created over a centimeter-scale—an extended focal region more than 50 Rayleigh ranges in length. This ultrabroadband flying-focus and the novel axiparabola-echelon configuration used to produce it are ideally suited for applications and scalable to >100 TW peak powers.

47 OTHER INSTRUMENTATION↗

DOE OSTI2021

Validation of simulated wave energy converter responses to focused waves

Focused waves are increasingly used as a design method to predict extreme loads for offshore structures, such as wave energy converters (WECs). However, the ability of computational methods to accurately simulate the prescribed focused waves and resulting wave structure interactions is not well validated. This study uses two computational fluid dynamic methods, WEC-Sim and STAR-CCM+, to evaluate the responses of two taut-moored WEC-like buoys to three different focused waves. WEC-Sim is a computationally efficient, mid-fidelity model, based on linearised potential flow theory. In contrast, STAR-CCM+ is a high-fidelity, three-dimensional, unsteady, Reynolds-averaged Navier–Stokes-based model. The two buoy geometries considered are a hemispherical-bottom cylinder and a truncated cylinder with a cylindrical moon pool. Three prescribed focused waves are generated in both codes, and the simulated displacements and mooring loads are obtained for each of the hydrodynamic bodies. The resulting STAR-CCM+ generated focused waves have approximately the same accuracy, in comparison with the analytic solution, as experimentally generated focused waves. The WEC-Sim simulated responses, when using viscous coefficients tuned to the measured displacements, are, on average, within 11.5% of experimentally measured values, whereas the STAR-CCM+ simulated responses are, on average, within 14.2% of the experimental values.

16 TIDAL AND WAVE POWER↗

NASA NTRS1986

An explanation for the plateau phenomenon in isoelectric focusing

Isoelectric focusing of mixtures of simple ampholytes occurs in two phases, an initial rapid separation phase and a second relatively slow stabilizing phase. Transient and steady-state computer simulation data are shown to predict the development of pH plateaus around neutrality during the stabilizing phase of the focusing of such mixtures. This occurs because a nonzero electrophoretic flux is present in a pure zone of focused ampholyte, which is a function of both its isolectric point (pI) and its Delta-pK value. For an ampholyte with a pI greater than 9 or less than 5, this flux causes the development of a significant concentration gradient within its focused zone which is accompanied by a contraction of this zone along the focusing axis. Acidic and basic ampholytes are thereby displayed toward the anode and cathode respectively, creating a pH plateau in the neutral region. Thus, there will be regions of the focusing column, closer to the electrodes and containing more acidic or basic pH values, within which the resolution of samples will reach a maximum and then decrease.

Mosher, Richard A.↗

NASA NTRS1991

Preliminary demonstrations of a focusing schlieren system for flow field diagnostics - Research in progress

A preliminary study to demonstrate the potential of the focusing schlieren technique to provide quantitative measurements of a three-dimensional flow field is described. The light intensity distribution in a focusing schlieren plane of view is shown to be related to the density gradients both in the focus plane and in the out of focus planes. The potential to implement digital filtering techniques to compensate for the out of focus features and to enhance the in focus features is discussed.

Doggett, G. P.↗

NASA NTRS1994

Axial focusing of impact energy in the Earth's interior: Proof-of-principle tests of a new hypothesis

A causal link between major impact events and global processes would probably require a significant change in the thermal state of the Earth's interior, presumably brought about by coupling of impact energy. One possible mechanism for such energy coupling from the surface to the deep interior would be through focusing due to axial symmetry. Antipodal focusing of surface and body waves from earthquakes is a well-known phenomenon which has previously been exploited by seismologists in studies of the Earth's deep interior. Antipodal focusing from impacts on the Moon, Mercury, and icy satellites has also been invoked by planetary scientists to explain unusual surface features opposite some of the large impact structures on these bodies. For example, 'disrupted' terrains have been observed antipodal to the Caloris impact basis on Mercury and Imbrium Basin on the Moon. Very recently there have been speculations that antipodal focusing of impact energy within the mantle may lead to flood basalt and hotspot activity, but there has not yet been an attempt at a rigorous model. A new hypothesis was proposed and preliminary proof-of-principle tests for the coupling of energy from major impacts to the mantle by axial focusing of seismic waves was performed. Because of the axial symmetry of the explosive source, the phases and amplitudes are dependent only on ray parameter (or takeoff angle) and are independent of azimuthal angle. For a symmetric and homogeneous Earth, all the seismic energy radiated by the impact at a given takeoff angle will be refocused (minus attenuation) on the axis of symmetry, regardless of the number of reflections and refractions it has experienced. Mantle material near the axis of symmetry will experience more strain cycles with much greater amplitude than elsewhere and will therefore experience more irreversible heating. The situation is very different than for a giant earthquake, which in addition to having less energy, has an asymmetric focal mechanism and a larger area. Two independent proof-of-principle approaches were used. The first makes use of seismic simulations, which are being performed with a realistic Earth model to determine the degree of focusing along the axis and to estimate the volume of material, if any, that experiences significant irreversible heating. The second involves two-dimensional hydrodynamic code simulations to determine the stress history, internal energy, and temperature rise as a function of radius along the axis.

Boslough, M. B.↗

NASA NTRS1994

AXAF VETA-I mirror ring focus measurements

The AXAF VETA-I mirror ring focus measurements were made with an HRI (microchannel plate) X-ray detector. The ring focus is a sharply focused ring formed by X-rays before they reach the VEAT-I focal plane. It is caused by spherical aberrations due to the finite source distance and the despace in the VETA-I test. The ring focus test reveals some aspects fo the test system distortions and the mirror surface figure which are difficult or impossible to detect at the focal plane. The test results show periodic modulations of the ring radius and width which could be caused by gravity, thermal, and/or epoxy shrinkage distortions. The strongest component of the modulation had a 12-fold symmetry, because these distortions were exerted on the mirror through 12 flexures of the VETA-I mount. Ring focus models were developed to simulate the ring image. The models were compared with the data to understand the test system distortions and the mirror glass imperfection. Further studies will be done to complete this work. The ring focus measurement is a very powerful test. We expect that a similar test for the finally assembled mirror of AXAD-I will be highly valuable.

Tananbaum, H. D.↗

NASA NTRS2000

Reflective Focused Schlieren System Improved for Use in 10- by 10-Foot Supersonic Wind Tunnel

The reflective focused schlieren system that was developed for use in the 10- by 10-Foot Supersonic Wind Tunnel (10x10 SWT) at the NASA Glenn Research Center at Lewis Field as part of the Unstart Test Program was improved this past year. In April 1999, the development and use of the system was presented at the Supersonic Tunnel Association International in Bedford, England. A focused schlieren system is similar to a standard schlieren system in that shock waves coming from an object in supersonic flow can be seen using a standard video camera. Unlike the standard schlieren system, which produces a two-dimensional schlieren image, a focused schlieren system can produce a threedimensional image. The preceding drawing shows the components of the reflective focused schlieren system being developed for use in the 10x10 SWT. Although the system worked well for the Unstart Test Program, it was not sensitive enough to be classified as a facility capability. Therefore, a program was implemented to improve the sensitivity of the reflective focused schlieren system so that it could be a facility capability for Glenn's 10x10 SWT. Several techniques were implemented to increase the sensitivity and to improve the overall operation of the system. These included refinement of the source grid, improvement in the cutoff grid production, improvement of the source grid and cutoff grid alignment, installation of an improved light source, and incorporation of an image-enhancing system. These changes are being implemented with the system set up in the laboratory. A checkout test of the system is planned in the 10x10 SWT in March 2000. Of these techniques, the most developed is the refinement of the source grid. The original system had a pattern of -in. by -in. squares on -in. centers (distance between the center points of adjacent squares). This gave a ratio of light to dark (reflective to nonreflective area) of 3:1. The recommended ratio is 1:1. In order to accomplish this, a pattern of -in.-diameter dots on 3/8-in. centers was developed. Preliminary tests with this pattern showed an increase in system sensitivity and image clarity. Further testing and refinement are scheduled. The former and improved dot patterns are shown. The use of glass plates to produce the cutoff grid improved the cutoff grid's quality and helped to align it with the source grid. The cutoff grid, which is the negative of the source grid, is made by exposing photography film (or glass plates) to the proper light while it is installed in the focused schlieren system. The exposed film or plate is removed from the system and then developed as a photograph negative. Because the glass plates are rigid, they eliminate the risk of distortion when the negative is reinstalled in the system and realigned with the source grid.

Williamson, Gary Scott↗

NASA NTRSDate not supplied

Recent Development Work with Self-Aligned Focusing Schlieren

A novel compact focusing schlieren instrument has recently been developed that eliminates the need for a separate source and cutoff grid. The technique works by projecting an image of a grid onto a retroreflective surface and then reimaging the projection back onto the original grid. By manipulating the polarization state of the light passing through the instrument, a single Rochon polarizing prism can be used to adjust the schlieren sensitivity by translating it along the instrument’s optical axis, which changes the in-plane offset between the reimaged projection and the original grid. This arrangement makes the instrument inherently self-aligned. Relative to conventional focusing schlieren instruments, which require alignment of a separate source grid and cutoff grid to achieve sensitivity, the setup time required in order to obtain high quality focusing schlieren images is significantly reduced. Further, the self-aligned nature of this instrument makes it insensitive to vibrations and allows for on-the-fly adjustments to field-of-view. In this paper we discuss recent work that has been performed to expand the capabilities of this self-aligned focusing schlieren instrument including: schlieren visualization at extreme angles for optically-restricted test facilities, 3D schlieren visualization using a light field camera, acquisition of high quality focusing schlieren images from facilities with low quality windows, and obtaining focusing schlieren images in full-scale ground test facilities.

Brett Bathel↗

DOE OSTI2022

Focusing ions at atmospheric pressure using nonlinear DC voltage sequences applied to a stacked ring ion guide

Many modern ion mobility (IM) and mass spectrometers (MS) operate under low pressure (= 10 Torr) and employ high voltage radiofrequencies (RF) to provide ion confinement. Unfortunately, RF effectiveness drastically decreases as pressure increases, and few techniques for focusing ions at elevated pressures exist. Here we demonstrate a new approach for focusing ions at atmospheric pressure (AP) by applying nonlinear DC voltage sequences following quadratic and power (exponential) functions to a stacked ring ion guide. In this work, we used ion trajectory simulations to rigorously explore how ions react to nonlinear electric fields and validate the simulations with a set of ion current measurements performed at AP. Ion trajectory simulations show that ions initially defocus near the entrance of the device but then become intensely focused as they travel through the device. Contour plots for both nonlinear voltage sequences show electric field lines that increasingly curve inwards as a function of distance, resulting in spatial ion focusing. Experimental ion current and spot size measurements were performed at AP using a 10-cm stacked ring ion guide and a segmented Faraday cup detector. Quadratic sequences produced ~5% smaller spot sizes (~22.8 mm) and ~25% higher ion current compared to a linear voltage sequence (~24.0 mm). Alternatively, power sequences produced ~64% smaller spot sizes (~8.7 mm), albeit with ~10x lower ion current. However, both nonlinear voltage sequences produced similar ion currents at the center of the Faraday cup detector, indicating that higher ion densities are achieved when using nonlinear voltage gradients. These results demonstrate a new way to focus ions at AP, and the capabilities demonstrated here provide fundamental insights on how to keep ions inside analytical devices at elevated pressures without RF.

47 OTHER INSTRUMENTATION↗

DOE OSTI2025

Beam focusing and consequences for Doppler backscattering measurements

The phenomenon of focusing of microwave beams in a plasma near a turning-point caustic is discussed by exploiting the analytical solution to the Gaussian beam-tracing equations in the two-dimensional (2-D) linear-layer problem. The location of maximum beam focusing and the beam width at that location are studied in terms of the beam initial conditions. This focusing must be taken into account to interpret Doppler backscattering (DBS) measurements. We find that the filter function that characterises the scattering intensity contribution along the beam path through the plasma is inversely proportional to the beam width, predicting enhanced scattering from the beam focusing region. We show that the DBS signal enhancement for decreasing incident angles between the beam path and the density gradient is due to beam focusing and not due to forward scattering, as was originally proposed by (Gusakov et al., (Plasma Phys. Contr. Fusion, vol. 56, 2014, p. 0250092014, 2017); Plasma Phys. Rep. vol. 43(6), 2017, pp. 605–613). The analytic beam model is used to predict the measurement of the k y density-fluctuation wavenumber power spectrum via DBS, showing that, in an NSTX-inspired example, the spectral exponent of the turbulent, intermediate-to-high k y density-fluctuation spectrum might be quantitatively measurable via DBS, but not the spectral peak corresponding to the driving scale of the turbulent cascade.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2026

Flying focus with arbitrary directionality for spatiotemporal control of laser intensity

Flying focus techniques produce laser pulses whose focal points travel at arbitrary, controllable velocities. While this flexibility can enhance a broad range of laser-based applications, existing techniques constrain the motion of the focal point to the propagation direction of the pulse. Here, we introduce a flying focus configuration that decouples the motion of the focus from the propagation direction. Here, a chirped laser pulse focused and diffracted by a diffractive lens and grating creates a focal point that can move both along and transverse to the propagation direction. The focal length of the lens, grating period, and chirp can be tuned to control the direction and velocity of the focus. Simulations demonstrate this control for a holographic configuration suited to high-power pulses, in which two off-axis pump beams with different focal lengths encode the equivalent phase of a chromatic lens and grating in a gas or plasma. For low-power pulses, conventional solid-state or adaptive optics can be used instead. Multi-dimensional control over the focal trajectory enables new configurations for applications, including laser wakefield acceleration of ions, nonlinear Thomson scattering, and surface-plasmon emission of THz radiation.

Classical optics↗

DOE OSTI2022

In-Situ Nanoscale Focusing of Extreme Ultraviolet Solid-State High Harmonics

Extreme ultraviolet light delivering radiation with a wavelength shorter than approximately 100 nm is now available from solid-state sources. However, despite exceptional progress, efficient focusing of extreme ultraviolet photons to their ultimate diffraction limit remains a formidable challenge because of the precision of the focusing by curved, optical surfaces. Here we integrate coherent short-wavelength high-order harmonics from a MgO crystal, with a high-numerical-aperture, nanostructured, focusing element etched onto the surface of the crystal itself. We focus extreme ultraviolet light, seventh harmonic of an 800-nm laser, with a zone plate of numerical aperture 0.35, down to a waist radius of 150 nm, with 18% focusing efficiency. The estimated intensity approaches 10 7 W/cm 2 . Future developments may demonstrate nanoscale laser ablation and miniaturization of extreme ultraviolet coherent sources on a chip.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

DOE OSTI2026

Rapidly tunable ultrabroadband flying focus using adaptive optics and an axiparabola

A programmable ultrabroadband flying focus was produced using adaptive optics and an axiparabola with a continuous wave superluminescent diode. A deformable mirror and spatial light modulator were used to add a programmable amount of radial group delay, and an axiparabola was used to create an extended focus by imparting spherical aberration. Three different flying focus trajectories were measured using spectral interferometry, two with uniform velocity and one with an accelerating velocity. Here, the temporal response function width of the flying focus optics alone was calculated to be 52 ± 6 fs, and the focal spot size was measured to be (1.2 ± 0.1) × larger than the diffraction-limited spot size through the extended focus.

Markland, H. S. [University of Rochester, NY (Unit↗