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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 37 records · Page 2
All sourcesNASA NTRSDOE OSTI
DOE OSTI2025

𝐵 → 𝜌⁢ℓ⁢$\bar{v}$ Resonance Form Factors from 𝐵→ 𝜋⁢𝜋⁢ℓ⁢$\bar{v}$ in Lattice QCD

The decay 𝐵 → 𝜌⁢ℓ⁢$\bar{v}$ is an attractive process for determining the magnitude of the smallest Cabibbo-Kobayashi-Maskawa matrix element, |𝑉 𝑢⁢𝑏 |, and can provide new insights into the origin of the long-standing exclusive-inclusive discrepancy in determinations of this standard-model parameter. This requires a nonperturbative QCD calculation of the 𝐵 → 𝜌 form factors 𝑉, 𝐴 0 , 𝐴 1 , and 𝐴 12 . The unstable nature of the 𝜌 resonance has prevented precise lattice QCD calculations of these form factors to date. Here, we present the first lattice QCD calculation of the 𝐵 → 𝜌 form factors in which the 𝜌 is treated properly as a resonance in 𝑃-wave 𝜋⁢𝜋 scattering. To this end, we use the Lellouch-Lüscher finite-volume formalism to compute the 𝐵 → 𝜋⁢𝜋 form factors as a function of both momentum transfer and 𝜋⁢𝜋 invariant mass, and then analytically continue to the 𝜌 resonance pole. This calculation is performed with 2 + 1 dynamical quark flavors at a pion mass of approximately 320 MeV, and demonstrates a clear path toward results at the physical point.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2026

Enabling Grid-Forming Control with Fault Ride-Through in Unbalanced Distribution Networks

Distribution networks are often unbalanced, causing oscillatory responses in inverter control designed for balanced conditions. Here, to address this problem, this paper proposes a novel time-domain transformation appropriate for inverter control and enables the decomposition of three-phase unbalanced signals into constant positive and negative components. Relations useful for calculating unbalanced active and reactive power are derived from first principle, providing insight into vector products of unbalanced three-phase signals. Furthermore, a grid-forming control effective under unbalanced conditions is developed, which delivers superior performance while meeting UNIFI1 specifications for grid-forming control under unbalanced conditions. specifications applicable to category 4 inverter-based resource, like setting and regulating frequency/voltage, providing voltage support, sharing active power, injecting negative sequence current, and riding through faults. A current limiter is proposed for safe fault ride-through and integrates with the grid-forming control featuring frequency/voltage droop controllers and current and voltage control loops. The transformation of interconnected inverters is formulated and stability of the proposed control analyzed to support robust parameter selections. The effectiveness of the proposed transformation and grid-forming control is demonstrated through analytical results and real-time simulation of a IEEE 123 distribution network on the Real-Time Digital Simulator. Comparison with existing methods shows that the proposed strategy satisfies the UNIFI specifications with a much better performance.

24 - POWER TRANSMISSION AND DISTRIBUTION↗
DOE OSTI2024

Digital Light Process 3D Printing of Magnetically Aligned Liquid Crystalline Elastomer Free–forms

Liquid crystalline elastomers (LCEs) are anisotropic soft materials capable of large dimensional changes when subjected to a stimulus. The magnitude and directionality of the stimuli-induced thermomechanical response is associated with the alignment of the LCE. Recent reports detail the preparation of LCEs by additive manufacturing (AM) techniques, predominately using direct ink write printing. Another AM technique, digital light process (DLP) 3D printing, has generated significant interest as it affords LCE free-forms with high fidelity and resolution. However, one challenge of printing LCEs using vat polymerization methods such as DLP is enforcing alignment. Here, we document the preparation of aligned, main-chain LCEs via DLP 3D printing using a 100 mT magnetic field. Systematic examination isolates the contribution of magnetic field strength, alignment time, and build layer thickness on the degree of orientation in 3D printed LCEs. Informed by this fundamental understanding, DLP is used to print complex LCE free-forms with through-thickness variation in both spatial orientations. Further, the hierarchical variation in spatial orientation within LCE free-forms is used to produce objects that exhibit mechanical instabilities upon heating. DLP printing of aligned LCEs opens new opportunities to fabricate stimuli-responsive materials in form factors optimized for functional use in soft robotics and energy absorption.

36 MATERIALS SCIENCE↗
DOE OSTI2025

Evaluation of a high-throughput method for processing sponge-stick samples to detect viable, non-spore-forming biothreat agents

After a bioterrorism incident, surface sampling is often used to determine the extent of contamination and exposure, guiding decontamination efforts and decisions for re-occupancy of affected sites. The sponge-stick (SS) is a preferred and commonly used device for sample collection to detect both spore-forming and non-spore-forming biothreat agents from non-porous surfaces. Here, in this study, a recently developed high-throughput method (HTM) for processing SS samples to detect viable Bacillus anthracis spores was adapted for detection of non-spore-forming biothreat agents, Yersinia pestis and Francisella tularensis. The scalable HTM was used to process up to 20 SS samples simultaneously, compared to the current stomacher-based method which processes one SS at a time. Comparisons of the HTM and the stomacher-based method were statistically indistinguishable for most experiments (P > 0.05) with HTM recoveries of 37–60 % for Y. pestis inoculated at 102–103 cells/SS and held 48 h at 4 °C to mimic sample transport/storage. The HTM was integrated with Rapid Viability-Polymerase Chain Reaction (RV-PCR) analysis to detect viable Y. pestis in the presence of particulate contamination (Arizona Test Dust, ATD). This approach detected Y. pestis inoculated at 20 cells/SS and ATD did not impact detection (P > 0.05). F. tularensis showed significantly lower recoveries between no-hold time and 48-h hold time (4 °C, P < 0.05) using the HTM, which further testing showed could be due to toxicity of the neutralizing buffer used for SS pre-wetting. With modifications, this method could enhance throughput capacity while maintaining similar recovery efficiencies to current methods for other non-spore-forming bacterial pathogens.

Biological and medical sciences↗
DOE OSTI2026

Multinuclear Solid-State NMR and NMR Crystallography of Solid Forms of Creatine and Creatinine

Creatine is a performance-enhancing supplement with two widely available commercial solid forms, namely, creatine monohydrate (creatine·H 2 O) and creatine HCl, the latter of which does not have a reported crystal structure. Moreover, commercial formulations of creatine may contain creatinine, an undesired impurity phase resulting from the self-cyclization of creatine during manufacturing. Therefore, reliable methods for characterizing the different solid forms of creatine and detecting the presence of creatinine are essential. Herein, we address these challenges using 13 C, 15 N, and 35 Cl solid-state NMR (SSNMR) spectroscopy to obtain distinct spectral fingerprints for creatine·H 2 O and creatine HCl, along with creatinine and creatinine HCl. The acquisition of these SSNMR spectra offers a robust approach for both the rapid characterization of each solid form and the detection of the impurity phases. Additionally, quadrupolar NMR crystallography-guided crystal structure prediction (QNMRX-CSP) was applied for the de novo crystal structure determination of creatine HCl, which was validated by the subsequently determined single-crystal X-ray diffraction (SCXRD) structure. Finally, to investigate the relationship between NMR parameters and structural features, 13 C and 15 N chemical shifts and 35 Cl electric field gradient (EFG) tensors were computed from geometry-optimized structures of the four solid forms by using dispersion-corrected DFT-D2* methods. Finally, this integrative approach offers a powerful framework for advancing the structural understanding and quality control of creatine-based supplements and next-generation formulations, as well as a wide range of other solid pharmaceuticals and nutraceuticals.

NMR↗
DOE OSTI2025

A family of tubular pili from harmful algal bloom forming cyanobacterium Microcystis aeruginosa

Cyanobacteria are vital photosynthetic prokaryotes, but some form harmful algal blooms (cyanoHABs) that disrupt ecosystems and produce toxins. The mechanisms by which these blooms form have yet to be fully understood, particularly the role of extracellular components. Here, we present a 2.4 Å cryo-EM structure of a pilus, termed the cyanobacterial tubular (CT) pilus, found in the cyanoHAB-forming Microcystis aeruginosa. The pilin exhibits a unique protein fold, forming a tubular pilus structure with tight, double-layer anti-parallel β-sheet interactions. We show that CT pili are essential for buoyancy by facilitating the formation of micro-colonies, which increases drag force and prevents sinking. The CT pilus surface is heavily glycosylated with ten monosaccharide modifications per pilin. Furthermore, CT pili can enrich microcystin, potentially enhancing cellular resilience, and co-localize with iron-enriched extracellular matrix components. Thus, we propose that this pilus plays an important role in the proliferation of cyanoHABs. This just discovered pilus family appears to be widely distributed across several cyanobacterial orders. Our structural and functional characterization of CT pili provide insights into cyanobacterial cell morphology, physiology, and toxin interactions, and identify potential targets for disrupting bloom formation.

Cryoelectron microscopy↗
DOE OSTI2025

Form-factor dependence of neutrino-nucleus cross sections using microscopic methods

To achieve its design goals, the next generation of neutrino-oscillation accelerator experiments requires percent-level predictions of neutrino-nucleus cross sections supplemented by robust estimates of the theoretical uncertainties involved. The latter arise from both approximations in solving the nuclear many-body problem and in the determination of the single- and few-nucleon quantities taken as input by many-body methods. To gauge the sensitivity of realistic nuclear many body methods to these few-nucleon quantities, we compute flux-averaged double-differential cross sections using the Green’s function Monte Carlo and spectral function methods as well as different parameterizations of the nucleon axial form factors based on either deuterium bubble-chamber data or lattice quantum chromodynamics calculations. The cross-section results are compared with available experimental data from the MiniBooNE and T2K collaborations. We also discuss the uncertainties associated with N → Δ transition form factors that enter the two-body current operator. We quantify the relations between neutrino-nucleus cross section and nucleon form factor uncertainties. These relations enable us to determine the form factor precision targets required to achieve a given cross-section precision.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2025

High-quality axions from higher-form symmetries in extra dimensions

The extradimensional axion solves the strong C P problem while largely circumventing the quality problem that plagues its four-dimensional counterparts. Such high quality can be clearly understood in terms of the generalized global symmetries of the higher-dimensional theory. We emphasize that an electric one-form symmetry is entirely responsible for protecting the potential of axions arising from 5D gauge theories and use this to systematically characterize the extradimensional axion quality problem. We identify three ways of breaking this one-form symmetry to generate an axion potential: adding electrically charged matter, gauging a magnetic higher-form symmetry, and turning on an Adler-Bell-Jackiw anomaly. In the latter case, we identify new ways of generating an axion potential via extradimensional magnetic monopoles. We also discuss how the axion is modified if the protective electric one-form symmetry is itself gauged. Finally, we relate these effects to gravitational expectations for the quality problem via generalized weak gravity conjectures. The clarity that generalized symmetries bring to the extradimensional axion quality problem highlights their relevance to particle phenomenology. Published by the American Physical Society 2025

Craig, Nathaniel↗
DOE OSTI2025

Microbial ecology of acidic, biogenic gypsum: community structure and distribution of extremophiles on freshly formed and relict sulfate deposits in a hydrogen sulfide-rich cave

Sulfate minerals are abundant on the Martian surface, and many of these evaporite deposits are thought to have precipitated from acidic fluids. On Earth, gypsum (CaSO 4 •2H 2 O) and other sulfates sometimes form under acidic conditions, so exploring the extremophilic life that occurs in these mineral environments can help evaluate the astrobiological potential of acid sulfate depositional settings. Here, we characterized the microbial communities associated with acidic gypsum deposits in a sulfuric acid cave, where sulfate precipitation is driven by sulfide-oxidizing bacteria and archaea. We used 16S rRNA gene sequencing and cell counts to characterize gypsum-associated microorganisms in freshly formed and relict deposits throughout the cave, to test how microbial community composition and abundance would vary with distance from the sulfidic water table and with the concentration of H 2 S(g) and other gases in the cave atmosphere. We found that actively forming gypsum in the lower cave levels was colonized by low-diversity communities that have few cells compared to other environments in the cave. The most abundant taxa were Acidithiobacillus, Metallibacterium, Mycobacteria, and three different Thermoplasmatales-group archaea, which occupied distinct niches based on proximity to sulfidic streams and the concentration of gases in the cave air. By contrast, deposits in older cave levels had more diverse communities that were distinct from those associated with freshly formed gypsum and likely represent a community reliant on different energy resources. These findings show that acidic sulfate deposits serve as habitats for extremophilic microorganisms and broaden our knowledge of the life associated with terrestrial sulfates.

58 GEOSCIENCES↗
DOE OSTI2025

Thermal properties and Thermodynamic Equilibrium Modeling of Cementitious Waste Forms

INTRODUCTION Cementitious matrices are used in the US DOE complex and worldwide to solidify aqueous radioactive, hazardous, mixed salt solutions, and sludges to meet low-level radioactive waste (LLW) disposal requirements. Blended formulations are used for most waste form mix designs. Substitution of pozzolans for Class F fly ash has the potential to alter the processing properties and stabilization properties of the resulting waste forms because they add chemical and mineralogical complexity to the final material. The Savannah River Site saltstone waste form was selected as the test case material. CemGEMS software was chosen as the model for predicting hydrated cementitious phases assemblages and phase evolution. Isothermal calorimetry was used as the method for evaluating processing and properties of fresh, uncured waste forms. The test cases consisted of reference case saltstone, and five natural pozzolan substituted saltstone mixes.

Bustamante, Michael E. [Savannah River National La↗
DOE OSTI2025

Optimal Control for Fast Frequency Response and Black-Start using Embedded Storages with Grid-Forming Control

The grid-forming inverter is regarded as the solution for integrating high levels of renewable resources into future power systems. Ensuring the stable operation of grids necessitates that grid-forming inverters offer fast frequency response. This report introduces an optimal control method that coordinates the embedded storage within the grid-forming control model with conventional synchronous generators. The optimized active power reference for the embedded storage is generated using receding horizon optimization control, aiming to keep the center of inertia frequency within acceptable limits. The effectiveness of the proposed control is verified through testing in the IEEE 39-bus system. In addition, with grid-forming capability, we will also investigate the application of using mobile embedded storages as black-start units to provide cranking power to energize non-blackstart generators in a black-start process.

24 POWER TRANSMISSION AND DISTRIBUTION↗
DOE OSTI2025

Small-scale Assessment of Simplified Ceramic Waste Form Processing

The feasibility of directly processing glass-bonded sodalite ceramic waste form materials by heating a mixture of Zeolite 4A, chloride salt, and sodium borosilicate binder glass was demonstrated by generating laboratory-scale materials. This direct processing method eliminates pre-setting the moisture content of the Zeolite 4A, eliminates the step of occluding salt in the prepared Zeolite 4A prior to processing, and can be conducted using larger particle sizes of crushed Zeolite 4A and crushed borosilicate glass than those called for in the current method. These simplifications are expected to facilitate material transfer and handling in a hot cell or controlled atmosphere environment and be more readily implemented at large scale than the current method. Most materials made to assess these simplifications were directly processed at 925 °C for two hours in an argon atmosphere glovebox, but one material was processed at 925 °C for four hours and one material was processed at 880 °C for two hours. Sodalite was generated and became microencapsulated by the binder glass in all materials. The microstructures were uniform throughout each product, were similar in all products, and were similar to the microstructures of materials made previously using the pressureless consolidation or hot isostatic pressing methods. Various formulations showed the efficiency of sodalite generation was not sensitive to the salt-to-Zeolite 4A ratio or salt-to-glass mass ratio, although a greater relative mass of glass is required to encapsulate sodalite generated from large particles of aggregated Zeolite 4A. The upper limit of salt loadings that can be effectively processed remains to be determined. The effectiveness of direct processing provided new insights into the conversion mechanism. The salt was likely dissolved into the glass that transported NaCl into the Zeolite 4A aggregates and sodalite was generated in situ as NaCl migrated from the outside of the aggregate inward. Other salt cations (e.g., potassium, strontium, cesium, and probably lithium) remain dissolved in the glass encapsulating the zeolite/sodalite domains. When the glass solidifies during cooling, small halite inclusion phases form in glass within sodalite domains and large mixed salt inclusions form in glass surrounding the sodalite due to the low solubility of chloride in the (solid) glass. Other salt cations were oxidized during processing and formed inclusions in the bulk glass (e.g., neodymium). Initial degradation tests show the dissolution behavior of directly processed CWF (SCWF) materials is similar to CWF materials made using different methods.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2026

Untangling the heavy-flavor mess: status of the Fermilab-MILC calculation of the $B_{(s)}\to D^{(\ast)}_{(s)}\ellν$ form factors

We present the status of calculations of the form factors of the most relevant heavy-to-heavy and heavy-to-light decay channels. Using seven $N_f = 2+1+1$ HISQ ensembles, with lattice spacings ranging from 0.15 fm down to 0.06 fm, we calculate the form factors of the decays, including correlations among them. More than half of our ensembles feature physical pion masses, and the heavy quarks are simulated at their physical masses using the Wilson-clover action with the Fermilab interpretation. Even though we have recently seen huge qualitative and quantitative leaps in the characterization of heavy-to-heavy decays, these advances have failed to translate into improvements for the inclusive vs exclusive question, or the matter of the Lepton Flavor Universality ratios. In particular, in the $B\to D^{\ast}\ellν$ channel, the current situation of the lattice-QCD form factors is far from clear. Further, the latest lattice-QCD results on the heavy-to-light form factors display unexplained tensions that must urgently be resolved. The work presented here is an attempt to address these issues.

Vaquero, Alejandro [Zaragoza U.]↗
DOE OSTI2025

Chemical interaction and compatibility of uranium mononitride and alumina forming austenitic stainless steel

Uranium mononitride (UN) and alumina forming austenitic (AFA) stainless steel are a potential fuel-cladding combination for the lead-cooled fast reactor (LFR). Chemical compatibility between UN and AFA steel needs to be verified before implementation in a nuclear reactor. Diffusion couple experiments at 823 K and 1023 K were conducted for nonirradiated UN samples in contact with as-cast (no thermally grown Al 2 O 3 ) and preoxidized (with thermally grown Al 2 O 3 ) AFA for 500 and 1000 h in an inert environment. Preoxidized AFA exhibited little to no interaction with all UN samples tested at both 823 K and 1023 K, displaying the stability and capability of the Al 2 O 3 layer to prevent chemical interaction and inter-diffusion with UN. Chemical interaction occurs between UN and as-cast AFA. At 1023 K, an aluminum and nitrogen rich phase (likely AlN) formed along the interface of as-cast AFA and UN samples. At 823 K the AlN phase was not prominently observed due to the reduced diffusivity of aluminum through AFA. The aluminum and nitrogen-enriched phase was also observed in a high temperature pressure-assisted test sample of UN and as-cast AFA thermally treated at 1373 K. Finally, in UN samples doped with a low weight percent of UO 2 (< 3 wt%), AlN was not detected along the interface at either temperatures, and an Al 2 O 3 layer likely formed along the interface and prevented further chemical interaction between UN and as-cast AFA.

36 MATERIALS SCIENCE↗
DOE OSTI2025

Synergy in Materials: Leveraging Phosphosilicate Waste Forms for Electrochemical Salt Waste

Here, waste forms containing glassy and crystalline phosphate and silicate phases were produced to immobilize salt waste simulants from pyroprocessing and characterized by using Raman spectroscopy, Mössbauer spectroscopy, X-ray diffraction, scanning electron microscopy, heat capacity, and chemical durability measurements. In this work, a phosphosilicate waste form is presented to leverage the benefits of both borosilicate glasses and iron phosphate glasses. To improve waste loading, prior to immobilization, salt simulants were successfully dechlorinated using ammonium dihydrogen phosphate, mixed with a borosilicate frit (5–30 wt %) and Fe 2 O 3 , and vitrified. Additions of 2.5–15 wt % borosilicate glass (NBS3) improved normalized release rates for Cs relative to iron-phosphates without NBS3, resulting in chemical durabilities similar to high-level waste borosilicate glass reference materials. The release rates of the alkalis (i.e., Li, Na, K, Cs) were the lowest with the addition of 5 wt % NBS3. Although Sr was not specifically targeted in this study, evidence exists that it preferentially partitioned with Si to form an amorphous droplet phase within the iron phosphate glass matrix.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2025

Exploring how urban form and demographics are linked with pedestrian and bicycle safety

With pedestrian and bicycle safety as the focus, this study investigates the role of urban form, burdened communities (BCs), and demographics at the national level. Urban form can contribute to segregation, limiting access to crucial resources such as safe infrastructure, essential services, and economic opportunities. Leveraging recent data, this research applies six key indicators to identify BCs based on various socioeconomic and environmental factors. Here, the study creates a unique database combining 10 years of pedestrian-bicycle-involved fatal crashes with data for the 71,729 census tracts with burden indicators and census data. The data are analyzed using descriptives and rigorous zero-hurdle negative binomial models, which account for excessive zeros observed in the data. The inference-based analysis results reveal a positive correlation between burden indicators and pedestrian-bicycle-involved fatal crash occurrences, alongside a heightened risk in areas with high-intensity development. Higher Black, American Indian, or Alaska Native populations are associated with more fatal crashes. The study offers novel insights into safety dynamics across different contexts characterized by urban forms, BCs, and demographics. The study underscores the importance of targeted interventions to enhance pedestrian and bicycle safety.

bicycle crashes↗
DOE OSTI2025

Virtual Self-Excited Induction Generator-Based Grid-Forming Inverter Control for Robust Voltage Regulation Under Nonideal Loading

This paper presents a generator-inspired control methodology for grid-forming (GFM) inverters that deliberately emulates a self-excited induction generator so that the inverter can hold its voltage and frequency under difficult loading and severe terminal disturbances across wide voltage and frequency ranges. The design integrates a Lyapunov energy function-based inner loop to provide high bandwidth and strong disturbance rejection, and it complements this with a passivity-based argument that furnishes a coherent large-signal stability guarantee beyond small-signal limits. Analytical insights are developed via the Krylov-Bogoliubov-Mitropolsky averaging method, which reveals an intrinsic resistive droop characteristic; these closed-form relations both explain the observed dynamics and yield simple, decentralized tuning rules. The methodology is validated on a controller-hardware-in-the-loop platform and exercised in real time across balanced, unbalanced, and nonlinear loads, as well as during parallel operation. Across these scenarios, the inverter maintains balanced three-phase voltages, limits harmonic content, settles quickly with well-damped transients, and remains resilient when multiple units operate in parallel. The contributions are a self-excited-machine-inspired GFM controller with enhanced dynamic performance and robustness, a single stability rationale grounded in passivity, closed-form expressions that guide tuning, and comprehensive hardware-in-the-loop validations demonstrating effectiveness and superiority under challenging operating conditions.

24 POWER TRANSMISSION AND DISTRIBUTION↗
DOE OSTI2026

Demonstration of Grid Services Using Mixed Grid-Forming and Grid-Following Technologies at the Wheatridge Renewable Energy Facility (Final Technical Report)

This Final Technical Report summarizes the analytical, modeling, and engineering work performed to evaluate grid-forming (GFM) inverter capabilities within a large hybrid renewable energy facility. The project focused on assessing the ability of advanced inverter-based resources to provide essential reliability services through coordinated operation of grid-forming (GFM) and grid-following (GFL) technologies. During Budget Period 1, the project developed a comprehensive framework of GFM performance metrics, including angle support, voltage regulation, frequency response, damping behavior, and current-limiting performance. Extensive electromagnetic transient (EMT) studies and hardware-in-the-loop (HIL) testing were conducted to validate GFM behavior under a range of operating conditions, including weak-grid scenarios, voltage disturbances, and multi-resource interactions. The project also established validated modeling approaches, plant-level control integration strategies, commissioning frameworks, and high-speed measurement infrastructure to support future field demonstration. Although the project concluded prior to field demonstration, the results provide a utility-scale foundation for evaluating, modeling, and deploying grid-forming technologies. The methodologies and tools developed contribute to industry understanding of inverter-based resource behavior and support future power system reliability under increasing renewable penetration.

14 SOLAR ENERGY↗