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At least 37 records · Page 2
All sourcesNASA NTRSDOE OSTI
DOE OSTI2015

Structural rearrangement and dispersion of functionalized graphene sheets in aqueous solutions

Surfactants are widely used for dispersing graphene and functionalized graphene sheets (FGS) in colloidal suspensions, but there have been few studies of the structure of the dispersed graphene-surfactant complexes in suspension and of their time evolution. Here, we combine experimental study of efficiencies of ionic surfactants/polymers in suspending FGS in water with characterization using atomic force microscopy, small angle neutron scattering, and molecular simulations to probe the detailed structures of FGSs. A systematic study of FGS dispersions using ionic surfactants with varying chain lengths revealed that the effective charge density of surfactant layer defines the concentration of dispersed FGS while the strength of interfacial binding defines the stability of graphene dispersion over long time aging. Ionic surfactants with strong interfacial binding and large molecular weight increase the dispersing power by over an order of magnitude.

36 MATERIALS SCIENCE↗
DOE OSTI2016

Ultra-sensitive magnetic microscopy with an optically pumped magnetometer

Optically pumped magnetometers (OPMs) based on lasers and alkali-metal vapor cells are currently the most sensitive non-cryogenic magnetic field sensors. Many applications in neuroscience and other fields require high-resolution, high-sensitivity magnetic microscopic measurements. In order to meet this demand we combined a cm-size spin-exchange relaxation-free (SERF) OPM and flux guides (FGs) to realize an ultra-sensitive FG-OPM magnetic microscope. The FGs serve to transmit the target magnetic flux to the OPM thus improving both the resolution and sensitivity to small magnetic objects. We investigated the performance of the FG-OPM device using experimental and numerical methods, and demonstrated that an optimized device can achieve a unique combination of high resolution (80 μm) and high sensitivity (8.1 pT/). Additionally, we also performed numerical calculations of the magnetic field distribution in the FGs to estimate the magnetic noise originating from the domain fluctuations in the material of the FGs. We anticipate many applications of the FG-OPM device such as the detection of micro-biological magnetic fields; the detection of magnetic nano-particles; and non-destructive testing. From our theoretical estimate, an FG-OPM could detect the magnetic field of a single neuron, which would be an important milestone in neuroscience.

47 OTHER INSTRUMENTATION↗
DOE OSTI2021

Ferromagnetic gyroscopes for tests of fundamental physics

Abstract A ferromagnetic gyroscope (FG) is a ferromagnet whose angular momentum is dominated by electron spin polarization and that will process under the action of an external torque, such as that due to a magnetic field. Here we model and analyze FG dynamics and sensitivity, focusing on practical schemes for experimental realization. In the case of a freely floating FG, we model the transition from dynamics dominated by libration in relatively high externally applied magnetic fields, to those dominated by precession at relatively low applied fields. Measurement of the libration frequency enables in situ determination of the magnetic field and a technique to reduce the field below the threshold for which precession dominates the FG dynamics. We note that evidence of gyroscopic behavior is present even at magnetic fields much larger than the threshold field below which precession dominates. We also model the dynamics of an FG levitated above a type-I superconductor via the Meissner effect, and find that for FGs with dimensions larger than about 100 nm the observed precession frequency is reduced compared to that of a freely floating FG. This is due to an effect akin to negative feedback that arises from the distortion of the field from the FG by the superconductor. Finally we assess the sensitivity of an FG levitated above a type-I superconductor to exotic spin-dependent interactions under practical experimental conditions, demonstrating the potential of FGs for tests of fundamental physics.

Physics↗
DOE OSTI2024

Species interactions amplify functional group responses to elevated CO 2 and N enrichment in a 24‐year grassland experiment

Abstract Plant functional groups (FGs) differ in their response to global changes, although species within those groups also vary in such responses. Both species and FG responses to global change are likely influenced by species interactions such as inter‐specific competition and facilitation, which are prevalent in species mixtures but not monocultures. As most studies focus on responses of plants growing in either monocultures or mixtures, but rarely both, it remains unclear how interspecific interactions in diverse ecological communities, especially among species in different FGs, modify FG responses to global changes. To address these issues, we leveraged data from a 16‐species, 24‐year perennial grassland experiment to examine plant FG biomass responses to atmospheric CO 2 , and N inputs at different planted diversity. FGs differed in their responses to N and CO 2 treatments in monocultures. Such differences were amplified in mixtures, where N enrichment strongly increased C3 grass success at ambient CO 2 and C4 grass success at elevated CO 2 . Legumes declined with N enrichment in mixtures at both CO 2 levels and increased with elevated CO 2 in the initial years of the experiment. Our results suggest that previous studies that considered responses to global changes in monocultures may underestimate biomass changes in diverse communities where interspecific interactions can amplify responses. Such effects of interspecific interactions on responses of FGs to global change may impact community composition over time and consequently influence ecosystem functions.

Mohanbabu, Neha↗
DOE OSTI2019

Methylmercury and Ethylmercury Analytical Performance in SRR Samples Measured by SRNL and Eurofins Frontier Global Sciences

Existing models and simulants of tank disposition media at the Savannah River Site (SRS) have presumed the presence of high concentrations of inorganic mercury. However, quarterly Tank 50 analyses have shown that mercury is present as organomercurial species at concentrations that may present challenges to its remediation and disposition and may challenge the Waste Acceptance Criteria (WAC) for Saltstone. Todate, methylmercury analyses for Savannah River Remediation (SRR) have been performed at an off-site laboratory by Eurofins Frontier Global Sciences (FGS) in Bothell, WA. Savannah River Remediation requested the development of methylmercury and ethylmercury determination capabilities at the Savannah River National Laboratory (SRNL) to support the Liquid Waste Operations at SRS. As part of that method development, SRR requested that SRNL Analytical Development (AD) compare their results with those obtained from their outside contract laboratory, Eurofins FGS. This document reports on this method development work as well as the comparative analyses conducted between the two laboratories. A series of optimization and validation experiments has been performed at SRNL, which has resulted in the development of on-site methylmercury and ethylmercury speciation capabilities using purge and trap (P&T) gas chromatography (GC) coupled with thermal desorption (TD) cold vapor – atomic fluorescence spectroscopy (CVAFS). Speciation has been achieved for both species, with a methylmercury method reporting limit (MRL) value of 1.13 pg and an overall uncertainty (1σ) of 5.1%. An ethylmercury MRL of 11.5 pg and an overall uncertainty (1σ) of 4.8% were obtained. These analytical parameters compare favorably with Eurofins FGS, which demonstrates uncertainties (1σ) for methylmercury and ethylmercury of 13% and 9.1%, respectively. Results obtained by SRNL from the routine analysis of Tanks 21, 40, 50, and 51 samples have provided statistically indistinguishable results compared with Eurofins FGS. Based upon the work performed by SRNL-AD and the data currently available, the following recommendations can be made: Further work should be performed to determine a “best practices” for sample holding time prior to analysis (both preserved and non-preserved samples), as well as any detrimental effects sample age may have on data quality. Analysis of ethylmercury is only recommended for tank samples that are reasonably expected to have significant quantities of ethylmercury, such as from the DWPF SMECT. Trace levels of ethylmercury in the presence of large quantities of methylmercury can be difficult or impossible to quantify. SRNL-AD development of methods for total mercury, purgeable mercury (which includes Hg(0) and dimethylmercury), inorganic mercury (Hg(I) and Hg(II)), dissolved mercury, and particulate mercury are underway and will be reported upon separately.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
NASA NTRS1983

A study into the loss of lock of the space telescope fine guidance sensor

The results of a study into the loss of lock phenomenon associated with the Space Telescope Fine Guidance Sensor (FGS) are documented. The primary cause of loss of lock has been found to be a combination of cosmic ray spikes and photon noise due to a 14.5 Mv star. The probability of maintaining lock versus time is estimated both for the baseline FGS design and with parameter changes in the FGS firmware which will improve the probability of maintaining lock. The parameters varied are changeable in-flight from the ground and hence do not impact the design of the FGS hardware.

Polites, M. E.↗
NASA NTRS1992

Astrometric performance characteristics of the Hubble Space Telescope fine guidance sensors

Each of the three fine guidance sensors for the Hubble Space Telescope constitutes a sixth science instrument to be used for astrometry. We detail the tests and results used in choosing one of the three sensors to be the prime astrometer. The Astrometry Science Team has chosen Fine Guidance Sensor (FGS) 3. FGS 3 produces position measurements on a star with V = 17 with a peraxis precision of 0.003 arcsec. The interferometer response function should permit double-star astrometry at least down to V = 16 for the central region of FGS 3. In a 10-h test of the stability of POS-mode astrometric measurements made in FGS 3, we found no scale or orientation variations greater than two parts in 100,000. During this same time period, we found no statistically significant systematic guide-star radial separation changes. Spacecraft jitter is found to be the prime determinant of astrometry success or failure.

Benedict, G. F.↗
NASA NTRS1994

The in-flight calibration of the Hubble Space Telescope fine guidance sensors, 2 (a success story)

The Hubble Space Telescope's fine guidance sensors (FGS's) are unique in the performance levels being attempted; spacecraft control and astrometric research with accuracies better than 3 milli-arcseconds (mas) are the ultimate goals. This paper presents a review of the in-flight calibration of the sensors, describing both the algorithms used and the results achieved to date. The work was done primarily in support of engineering operations related to spacecraft pointing and control and secondarily in support of the astrometric science calibration effort led by the Space Telescope Astrometry Team. Calibration items of principal interest are distortion, sensor magnification, and relative alignment. An initial in-flight calibration of the FGS's was performed in December 1990; this calibration has been used operationally over the past few years. Followup work demonstrated that significant, unexpected temporal variations in the calibration parameters are occurring; provided good characterization of the variation; and set the stage for a distortion calibration designed to achieve the full design accuracy for one of the FGS's. This full distortion calibration, using data acquired in January 1993, resulted in a solution having single-axis residuals with a standard deviation of 2.5 mas. Scale and alignment calibration results for all of the FGS's have been achieved commensurate with the best ground-based astrometric catalogs (root-mean-square error approximately 25 mas). A calibration monitoring program has been established to allow regular updates of the calibration parameters as needed.

Welter, Gary L.↗
NASA NTRS2004

Hubble Space Telescope Fine Guidance Sensor Post-Flight Bearing Inspection

Aerospace mechanism engineering success stories often, if not always, consist of overcoming developmental, test and flight anomalies. Many times it is these anomalies that stimulate technology growth and more reliable future systems. However, one must learn from these to achieve an ultimately successful mission. It is not often that a spacecraft engineer is able to inspect hardware that has flown in orbit for several years. However, in February 1997, the Fine Guidance Sensor-I (FGS-1) was removed from the Hubble Space Telescope (HST) and returned to NASA Goddard Space Flight Center (GSFC) during the second Servicing Mission (SM2). At the time of removal, FGS-1 had nearly 7 years of service and the bearings in the Star Selector Servos (SSS) had accumulated approximately 25 million Coarse Track (CT) cycles. The main reason for its replacement was due to a bearing torque anomaly leading to stalling of the B Star Selector Servo (SSS-B) when reversing direction during a vehicle offset maneuver, referred to herein as a Reversal Bump (RB). The returned HST FGS SSS bearings were disassembled for post-service condition assessment to better understand the actual cause of the torque spikes, identify potential process/design improvements, and provide information for remedial on-orbit operation modifications. The methods and technology utilized for this inspection are not unique to this system and can be adapted to most investigation ai varying stages of the mechanism life from development, through testing, io post night evaluation. The systematic methods used for the HST Fine Guidance Sensor (FGS) SSS and specific findings are the subjects presented in this paper. The lessons learned include the importance of cleanliness and handling for precision instrument bearings and the potential effects from contamination. The paper describes in detail, the analytical techniques used for the SSS and their importance in this investigation. Inspection analytical data and photographs are included throughout the paper.

Pellicciotti, Joseph↗
NASA NTRS2004

Hubble Space Telescope Fine Guidance Sensor Post-Flight Bearing Inspection

Aerospace mechanism engineering success stories often, if not always, consist of overcoming developmental, test and flight anomalies. Many times it is these anomalies that stimulate technology growth and more reliable future systems. However, one must learn from these to achieve an ultimately successful mission. It is not often that a spacecraft engineer is able to inspect hardware that has flown in orbit for several years. However, in February 1997, the Fine Guidance Sensor-1 (FGS-1) was removed from the Hubble Space Telescope (HST) and returned to NASA Goddard Space Flight Center (GSFC) during the second Servicing Mission (SM2). At the time of removal, FGS-1 had nearly 7 years of service and the bearings in the Star Selector Servos (SSS) had accumulated approximately 25 million Coarse Track (CT) cycles. The main reason for its replacement was due to a bearing torque anomaly leading to stalling of the B Star Selector Servo (SSS-B) when reversing direction during a vehicle offset maneuver, referred to herein as a Reversal Bump (RB). The returned HST FGS SSS bearings were disassembled for post-service condition assessment to better understand the actual cause of the torque spikes, identify potential process/design improvements, and provide information for remedial on-orbit operation modifications. The methods and technology utilized for this inspection are not unique to this system and can be adapted to most investigations at varying stages of the mechanism life from development, through testing, to post flight evaluation. The systematic methods used for the HST Fine Guidance Sensor (FGS) SSS and specific findings are the subjects presented in this paper. The lessons learned include the importance of cleanliness and handling for precision instrument bearings and the potential effects from contamination. The paper describes in detail, the analytical techniques used for the SSS and their importance in this investigation. Inspection analytical data and photographs are included throughout the paper.

Pellicciotti, J.↗
DOE OSTI2012

Functionalized Graphene Sheets as Molecular Templates for Controlled Nucleation and Self-Assembly of Metal Oxide-Graphene Nanocomposites

Graphene sheets have been extensively studied as a key functional component of graphene-based nanocomposites for electronics, energy, catalysis,and sensing applications. However, fundamental understanding of the interfacial binding and nucleation processes at graphene surfaces remains lacking, and the range of controlled structures that can be produced are limited. Here, by using a combination of theoretical and experimental approaches, we demonstrate that functionalized graphene sheets (FGS) can function as a new class of molecular templates to direct nucleation and self-assembly and produce novel, three-dimensional nanocomposite materials. Two key aspects are demonstrated: First, the functional groups on FGS surface determine the nucleation energy, and thus control the nucleation sites and nucleation density, as well as the preferred crystalline phases. Second, FGS can function as a template to direct the self-assembly of surfactant micelles and produce ordered, mesoporous arrays of crystalline metal oxides and composites.

Environmental Molecular Sciences Laboratory↗
DOE OSTI2015

The multiplicity of massive stars: A high angular resolution survey with the HST fine guidance sensor

We present the results of an all-sky survey made with the Fine Guidance Sensor on the Hubble Space Telescope to search for angularly resolved binary systems among massive stars. The sample of 224 stars is comprised mainly of Galactic O- and B-type stars and luminous blue variables, plus a few luminous stars in the Large Magellanic Cloud. The FGS TRANS mode observations are sensitive to the detection of companions with an angular separation between 0.″01 and 1.″0 and brighter than △m=5. The FGS observations resolved 52 binary and 6 triple star systems and detected partially resolved binaries in 7 additional targets (43 of these are new detections). These numbers yield a companion detection frequency of 29% for the FGS survey. We also gathered literature results on the numbers of close spectroscopic binaries and wider astrometric binaries among the sample, and we present estimates of the frequency of multiple systems and the companion frequency for subsets of stars residing in clusters and associations, field stars, and runaway stars. These results confirm the high multiplicity fraction, especially among massive stars in clusters and associations. We show that the period distribution is approximately flat in increments of logP. We identify a number of systems of potential interest for long-term orbital determinations, and we note the importance of some of these companions for the interpretation of the radial velocities and light curves of close binaries that have third companions.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2016

Mercury speciation comparison. BrooksApplied Laboratories and Eurofins Frontier Global Sciences

The Savannah River National Laboratory (SRNL) was tasked with preparing and shipping samples for Hg speciation by Eurofins Frontier Global Sciences (FGS), Inc. in Bothell, WA on behalf of the Savannah River Remediation (SRR) Mercury Program Team. These samples were analyzed for seven species including: total mercury, dissolved mercury, inorganic mercury ((Hg(I) and Hg(II)), elemental mercury, methylmercury, ethylmercury, and dimethylmercury, with an eighth species, particulate mercury, calculated from the difference between total and dissolved mercury after subtracting the elemental mercury. The species fraction of total mercury measured has ranged broadly from a low of 32% to a high of 146%, though the vast majority of samples have been <100%. This can be expected since one is summing multiple values that each have at least a ± 20% measurement uncertainty. Two liquid waste tanks particularly important to understanding the distribution of mercury species in the Savannah River Site (SRS) Tank Farm were selected for a round robin analysis by Eurofins FGS and BrooksApplied Laboratories (BAL). The analyses conducted by BAL on the Tank 22 and 38 samples and their agreement with those obtained from Eurofins FGS for total mercury, dissolved mercury, methylmercury, ethylmercury, and dimethylmercury provide a strong degree of confidence in these species measurements

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
NASA NTRS1979

Space Telescope fine guidance - A design for manufacturability

The NASA Space Telescope (ST) is a 2.4-m aperture, f/24 Ritchey-Chretien telescope coupled to five on-board astronomical scientific packages. The very accurate line-of-sight stability required by ST during operating periods of up to 24 hours is maintained by the Pointing Control System whose optical system, the Fine Guidance Subsystem (FGS), is described. The Pointing Control System includes three identical FGSs, any two of which provide line-of-sight stabilization by tracking guide stars while the third performs astrometry. The optical system for the ST FGS performs the field aberration correction within the FGS near a pupil plane measuring only 52.7 mm. The design is simple and easily corrected, and offers substantial advantages over the traditional approach in terms of manufacturability.

Friedman, I.↗
NASA NTRS1981

Guide star probabilities

Probabilities are calculated for acquiring suitable guide stars (GS) with the fine guidance system (FGS) of the space telescope. A number of the considerations and techniques described are also relevant for other space astronomy missions. The constraints of the FGS are reviewed. The available data on bright star densities are summarized and a previous error in the literature is corrected. Separate analytic and Monte Carlo calculations of the probabilities are described. A simulation of space telescope pointing is carried out using the Weistrop north galactic pole catalog of bright stars. Sufficient information is presented so that the probabilities of acquisition can be estimated as a function of position in the sky. The probability of acquiring suitable guide stars is greatly increased if the FGS can allow an appreciable difference between the (bright) primary GS limiting magnitude and the (fainter) secondary GS limiting magnitude.

Soneira, R. M.↗
NASA NTRS1988

The optical field angle distortion calibration feasibility study for the Hubble Space Telescope fine guidance sensors

The results of an analytical study to investigate the feasibility of calibrating the Hubble Space Telescope's (HST's) fine guidance sensors (FGSs) within HST mission accuracy limits are presented. The study has two purposes: (1) to determine the mathematical feasibility of the optical field angle distortion (OFAD) calibration algorithm and (2) to confirm that the OFAD, plate scale, and FGS-to-FGS alignment calibration algorithms produced a calibration of the FGSs that satisfied mission requirements. The study concluded that the mathematical specification of the OFAD algorithm is adequate and permits a determination of the FGS calibration parameters (accurate to better than 0.003 arc-second) sufficient to meet the mission requirements. The algorithms implemented, the characteristics of the simulated data and procedures for data analysis, and the study's results are discussed. In addition, several useful techniques for improving the stability and accuracy of the OFAD solution are outlined.

Luchetti, K.↗
NASA NTRS1990

Hubble Space Telescope: Fine guidance sensors instrument handbook. Version 2.1

The Fine Guidance Sensors (FGS) are a system of photomultiplier tubes and white light amplitude interferometers (Koester's prism) which are used for the fine guidance of the Hubble Space Telescope (HST). The purpose of the handbook is to provide information to a potential user of the FGS so that he may explore the feasibility of performing various observations. A brief overview is given of how the FGS works, along with an explanation of the instrument in some detail. The procedure for estimating exposure times is explained. The observing modes are described. Some details needed to specify the exposures and observation requirements on the proposal forms are explained. Data reduction procedures are outlined.

Taff, Larry↗
NASA NTRS1993

The Hubble Space Telescope fine guidance system operating in the coarse track pointing control mode

The Hubble Space Telescope (HST) Fine Guidance System has set new standards in pointing control capability for earth orbiting spacecraft. Two precision pointing control modes are implemented in the Fine Guidance System; one being a Coarse Track Mode which employs a pseudo-quadrature detector approach and the second being a Fine Mode which uses a two axis interferometer implementation. The Coarse Track Mode was designed to maintain FGS pointing error to within 20 milli-arc seconds (rms) when guiding on a 14.5 Mv star. The Fine Mode was designed to maintain FGS pointing error to less than 3 milli-arc seconds (rms). This paper addresses the HST FGS operating in the Coarse Track Mode. An overview of the implementation, the operation, and both the predicted and observed on orbit performance is presented. The discussion includes a review of the Fine Guidance System hardware which uses two beam steering Star Selector servos, four photon counting photomultiplier tube detectors, as well as a 24 bit microprocessor, which executes the control system firmware. Unanticipated spacecraft operational characteristics are discussed as they impact pointing performance. These include the influence of spherically aberrated star images as well as the mechanical shocks induced in the spacecraft during and following orbital day/night terminator crossings. Computer modeling of the Coarse Track Mode verifies the observed on orbit performance trends in the presence of these optical and mechanical disturbances. It is concluded that the coarse track pointing control function is performing as designed and is providing a robust pointing control capability for the Hubble Space Telescope.

Whittlesey, Richard↗