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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 37 records · Page 2
All sourcesNASA NTRSDOE OSTI
NASA NTRS1995

Confined-Pyrolysis as an Experimental Method for Hydrothermal Organic Synthesis

A closed pyrolysis system has been developed as a tool for studying the reactions of organic compounds under extreme hydrothermal conditions. Small high pressure stainless steel vessels in which the ratio of sediment or sample to water has been adjusted to eliminate the headspace at peak experimental conditions confines the organic components to the bulk solid matrix and eliminates the partitioning of the organic compounds away from the inorganic components during the experiment. Confined pyrolysis experiments were performed to simulate thermally driven catagenetic changes in sedimentary organic matter using a solids to water ratio of 3.4 to 1. The extent of alteration was measured by monitoring the steroid and triterpenoid biomarkers and polycyclic aromatic hydrocarbon distributions. These pyrolysis experiments duplicated the hydrothermal transformations observed in nature. Molecular probe experiments using alkadienes, alkenes and alkanes in H2O and D2O elucidated the isomerization and hydrogenation reactions of aliphatic and the competing oxidative reactions occurring under hydrothermal conditions. This confined pyrolysis technique is being applied to test experiments on organic synthesis of relevance to chemical evolution for the origin of life.

Leif, Roald N.↗
NASA NTRS2022

Design Optimization of Energized Composite Using Simulation and Experimental Methods

As electric vehicles (EVs) are evolving, innovative technologies like “energized composite” that can store energy in the car's body helps extend its range per charge. The composite's unique ability to function as both structural body panel and charge storage medium stems from its unique pattern design between “electrochemical areas (EcA)” and “epoxy area (EpA)”. Herein, a design optimization study is presented to obtain a balanced ratio between EcA versus EpA to maximize the charge storage ability of the composite while maintaining a decent tensile and bending strength. Simulations using ANSYS software and experimental confirmation using universal testing machines and electrochemical analyzers are used to derive optimum ratios between EcA and EpA. Uniaxial tension test and 3-point bend test have been performed to optimize the tensile and bend strengths, whereas cyclic voltammetry, galvanic charge–discharge, and electrochemical impedance spectroscopy are used to determine the electrochemical performance of various design configurations by modulating the ratios of EcA versus EpA. Overall, the highest achieved energy storage per lamina is 2531 mWh m−2 for a maximum of 81.6% EcA with a tensile strength of 417.73 MPa and bending strength of 263.13 MPa. This study is highly beneficial for EVs and aerospace applications.

energy storage↗
NASA NTRS1965

Ceramic materials purified by experimental method

Crystalline ceramic materials are purified for use as high-temperature electrical insulators. Any impurities migrate to the cathode when a dc voltage is applied across the material while it is heated in an inert gas atmosphere.

Source record↗
NASA NTRS1971

Concepts for a theoretical and experimental study of lifting rotor random loads and vibrations. Phase 5C: Development of experimental methods

Test equipment which was built and the calibration tests are described. The test equipment consists of a two-bladed rotor of 16-in. diameter, the blades of which are elastically hinged in flapping. The feathering shaft of the blades can be harmonically rotated with the help of a cam mechanism located inside the hollow rotor shaft. The frequency range measured in the rotating system can be adjusted between 0 and 80 cps and the rotor speed between 0 and 40 cps. The test equipment is for measuring the flapping response of the blades to harmonic feathering excitation.

Hohenemser, K. H.↗
NASA NTRS1972

Experimental methods for geological remote sensing

During the past year a two channel IR technique for discrimination among silicate rocks was tested for a second time, a three channel IR method was tested for the first time, and a new visible-reflective IR ratio method was hypothesized and qualitatively tested for iron oxide recognition. Both the two channel and three channel IR ratios methods were capable of discriminating felsic from mafic rock types. The three-channel ratio values measured by the scanner were found to agree, within reasonable limits, with the values of R calculated from laboratory data. The capability of the three channel method to obtain absolute ratios is accompanied by a costly processing routine. The two channel technique is superior for low thermal contrast scenes about which some ground truth is available because of its speed and economy.

Vincent, R. K.↗
NASA NTRS1972

Interferometric spectropolarimetry - Alternate experimental methods.

Three alternate methods of obtaining spectra of the intensity and state of polarization of light are proposed. The methods make use of a two-beam amplitude division interferometer using the technique of Fourier spectroscopy. They do not require the presence of polarizers in the arms of the instrument. In one method a single analyzer is used in front of the detector with three successive orientations of its transmission axis azimuth. In another method, a (linear) polarizer assuming the same set of orientations is placed in the incident beam. A third method, a hybrid of the former two methods, makes use of both a polarizer and analyzer in the locations indicated. The first method permits the determination of all four Stokes parameters of polarization, whereas the other two methods cannot yield the ellipticity parameter. All methods require the recording of three interferograms. However, two interferograms can provide the intensity and degree of polarization in any of the methods described.

Fymat, A. L.↗
NASA NTRS1974

Evaluation of experimental methods for determining dynamic stiffness and damping of composite materials

Various methods potentially usable for determining dynamic stiffness and damping of composite materials are reviewed. Of these, the following most widely used techniques are singled out for more detailed discussion: free vibration, pulse propagation, and forced vibration response. To illustrate the usefulness and validity of dynamic property data, their application in dynamic analyses and comparison with measured structural response are described for the following composite-material structures: free-free sandwich beam with glass-epoxy facings, clamped-edge sandwich plate with similar facings, free-end sandwich conical shell with similar facings, and boron-epoxy free plate with layers arranged at various orientations.

Bert, C. W.↗
NASA NTRS1976

An experimental method to obtain the elastic strain energy function from torsion-tension tests

It is shown that by employing a torsion-tension test, it is possible to have a complete mapping near the origin of the two principal strain invariants associated with the rate of change of the strain energy function. However, the mathematical representation of the twist moment and normal forces vs strain and the strain energy function are complex. This problem is solved by using a set of solid cylindrical bars with different diameters such that the difference in diameter of two successive bars is small. The stress-strain equations can be grossly oversimplified by considering differences in twist moment and normal force as a function of difference in radius.

Peng, S. T. J.↗
NASA NTRS1978

A new experimental method for the accelerated characterization of composite materials

A method which permits the prediction of long-term properties of graphite/epoxy laminates on the basis of short-term (15 min) laboratory tests is described. Demonstration of delayed viscoelastic fracture in one laminate configuration, and data on the time and temperature response of a matrix-dominated unidirectional laminate contributed to a characterization of the viscoelastic process in the graphite/epoxy composites. Master curves from short-term tests of certain laminate configurations can be employed to generate long-term master curves. In addition, analytical predictions from short-term results can be used to predict long-term (25-hour) laminate properties.

Brinson, H. F.↗
NASA NTRS1985

Experimental methods for quenching structures in lunar-analog silicate melts: Variations as a function of quench media and composition

Compositions analogous to lunar green, organge, and brown glasses were synthesized under consistent conditions, then quenched into a variety of different media when the samples were removed from the furnace. Iron valence and coordination are a direct function of quench media used, spanning the range from brine/ice (most effective quench), water, butyl phthalate, silicone oil, liquid nitrogen, highly reducing CO-CO2 gas, to air (least efficient quench). In the green and brown glasses, Fe(3+) in four-fold and six-fold coordination is observed in the slowest-quenched samples; Fe(2+) coordination varies directly with quench efficiency. Less pronounced changes were observed in the Ti-rich orange glass. Therefore the remote-sensed spectrum of a glass-bearing regolith on the Moon may be influenced by the process by which the glass cooled, and extreme caution must be used when comparing spectra of synthetic glass analogs with real lunar glasses.

Dyar, M. D.↗
NASA NTRS1984

Experimental methods for quenching structures in lunar-analog silicate melts - Variations as a function of quench media and composition

Compositions analogous to lunar green, orange, and brown glasses were synthesized under consistent conditions, then quenched into a variety of different media when the samples were removed from the furnace. Iron valence and coordination are a direct function of quench media used, spanning the range from brine/ice (most effective quench), water, butyl phthalate, silicone oil, liquid nitrogen, highly reducing CO-CO2 gas, to air (least efficient quench). In the green and brown glasses, Fe(3+) in four-fold and six-fold coordination is observed in the slowest-quenched samples; Fe(2+) coordination varies directly with quench efficiency. Less pronounced changes were observed in the Ti-rich orange glass. Therefore the remote-sensed spectrum of a glass-bearing regolith on the moon may be influenced by the process by which the glass cooled, and extreme caution must be used when comparing spectra of synthetic glass analogs with real lunar glasses.

Dyar, M. D.↗
NASA NTRS1986

An experimental method for measuring droplet impingement efficiency on two- and three-dimensional bodies

An efficient and accurate method is described for extracting water droplet impingement efficiency data from dye impregnated blotter paper samples obtained by employing a dye-tracer technique in wind tunnel spray tests. The method is based on laser reflectance spectroscopy. A brief description of the test method, instrumentation, and data reduction system is also presented. Preliminary test results and analyses are included for a cylinder and a 65(2)015 airfoil.

Papadakis, M.↗