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Design and Performance of the Hitomi/XRISM Adiabatic Demagnetization Refrigerator Controller

The Resolve instrument in the recently launched X-ray Imaging and Spectroscopy Mission (XRISM) is a rebuild of the Soft X-ray Spectrometer (SXS) in Hitomi (aka Astro-H which had an unfortunately brief mission life in 2016). It is a high-resolution non-dispersive soft x-ray spectrometer from nominally 0.3 keV to 12 keV based on a calorimeter detector array operating at 50 mK with a resolution better than 7 eV FWHM at 6 keV. For such sensitive cryogenic instruments, temperature stability has a strong impact on the detector’s performance. The Adiabatic Demagnetization Refrigerator Controller (ADRC) in the XRISM Resolve instrument is an electronics box responsible for high-precision sub-K temperature readout and control of the multi-stage adiabatic demagnetization refrigerator subsystem to achieve a thermal stability better than 2.5 uK RMS (over a 10-minute interval) for the calorimeter detectors in both cryogen (liquid helium) and cryo-free modes. It has direct telemetry/command and power interfaces with the spacecraft. It also provides sensor read-out and heater circuits for decontamination of the filters in the cold aperture. As a part of the discussion on the design and performance of the ADRC, this paper will also include an overall view of the 50 mK temperature control, plus monitor and control of the aperture filter temperature for de-contamination purpose.

ADRC

Design of the PIXIE Adiabatic Demagnetization Refrigerators

The Primordial Inflation Explorer (PIXIE) is a proposed mission to densely map the polarization of the cosmic microwave background. It will operate in a scanning mode from a sun-synchronous orbit, using low temperature detectors (at 0.1 K) and located inside a teslescope that is cooled to approximately 2.73 K - to match the background temperature. A mechanical cryocooler operating at 4.5 K establishes a low base temperature from which two adiabatic demagnetization refrigerator (ADR) assemblies will cool the telescope and detectors. To achieve continuous scanning capability, the ADRs must operate continuously. Complicating the design are two factors: 1) the need to systematically vary the temperature of various telescope components in order to separate the small polarization signal variations from those that may arise from temperature drifts and changing gradients within the telescope, and 2) the orbital and monthly variations in lunar irradiance into the telescope barrels. These factors require the telescope ADR to reject quasi-continuous heat loads of 2-3 millwatts, while maintaining a peak heat reject rate of less than 12 milliwatts. The detector heat load at 0.1 K is comparatively small at 1-2 microwatts. This paper will describe the 3-stage and 2-stage continuous ADRs that will be used to meet the cooling power and temperature stability requirements of the PIXIE detectors and telescope.

adiabatic demagnetization refrigerator

Salt Pill Design and Fabrication for Adiabatic Demagnetization Refrigerators

The performance of an adiabatic demagnetization refrigerator (ADR) is critically dependent on the design and construction of the salt pills that produce cooling. In most cases, the primary goal is to obtain the largest cooling capacity at the low temperature end of the operating range. The realizable cooling capacity depends on a number of factors, including refrigerant mass, and how efficiently it absorbs heat from the various instrument loads. The design and optimization of "salt pills" for ADR systems depend not only on the mechanical, chemical and thermal properties of the refrigerant, but also on the range of heat fluxes that the salt pill must accommodate. Despite the fairly wide variety of refrigerants available, those used at very low temperature tend to be hydrated salts that require a dedicated thermal bus and must be hermetically sealed, while those used at higher temperature - greater than about 0.5 K - tend to be single-­‐ or poly-­‐crystals that have much simpler requirements for thermal and mechanical packaging. This paper presents a summary of strategies and techniques for designing, optimizing and fabricating salt pills for both low-­‐ and mid-­‐temperature applications.

sub-kelvin cooling

On-Orbit Operation of the Adiabatic Demagnetization Refrigerator on the Astro-H/Hitomi Soft X-ray Spectrometer Instrument

The Soft X-ray Spectrometer instrument on the Astro-H observatory contains a 6x6 array of x-ray microcalorimeters, which is cooled to 50 mK by an adiabatic demagnetization refrigerator (ADR). The ADR consists of three stages in order to provide stable detector cooling using either a 1.2 K superfluid helium bath or a 4.5 K Joule-Thomson (JT) cryocooler as its heat sink. When liquid helium is present, two of the ADRs stages are used to single-shot cool the detectors while rejecting heat to the helium. After the helium is depleted, all three stages are used to cool both the helium tank (to about 1.5 K) and the detectors (to 50 mK) using the JT cryocooler as its heat sink. The Astro-H observatory, renamed Hitomi after its successful launch in February 2016, carried approximately 36 liters of helium into orbit. On day 5, the helium had cooled sufficiently (1.4 K) to allow operation of the ADR. This paper describes the design, operation and on-orbit performance of the ADR.

sub-kelvin refrigeration

Design and On-Orbit Operation of the Adiabatic Demagnetization Refrigerator on the Hitomi Soft X-Ray Spectrometer Instrument

The Soft X-ray Spectrometer instrument on the Astro-H observatory contains a 6x6 array of x-ray microcalorimeters that is cooled to 50 mK by an adiabatic demagnetization refrigerator (ADR). The ADR consists of three stages in order to provide stable detector cooling using either a 1.2 K superfluid helium bath or a 4.5 K Joule-Thomson (JT) cryocooler as its heat sink. When liquid helium is present, two of the ADR's stages are used to single-shot cool the detectors while rejecting heat to the helium. After the helium is depleted, all three stages are used to continuously cool the helium tank (to about 1.5 K) and single-shot cool the detectors (to 50 mK), using the JT cryocooler as its heat sink. The Astro-H observatory, renamed Hitomi after its successful launch in February 2016, carried approximately 36 liters of helium into orbit. On day 5, the helium had cooled sufficiently (<1.4 K) to allow operation of the ADR. This paper describes the design, operation and on-orbit performance of the ADR, and the use of the ADR's heat rejection as a tool for mass gauging the helium tank.

adiabatic demagnetization refrigerator

Development of a Flight-Worthy 10 to 4 K Continuous Adiabatic Demagnetization Refrigerator

The cryogenics and fluids branch at NASA's Goddard Space Flight Center is currently developing a high-efficiency, vibration-free, flight-worthy Continuous Adiabatic Demagnetization Refrigerator (CADR) that consist of two modular units: one that lifts ~6 microW at 50 mK while rejecting its heat to a 4 K thermal sink, and another unit that provides a constant 4 K cooling stage while rejecting its heat to a thermal sink at 10 K. The two units are linked together via a 4 K common platform. This paper discusses the status report on the thermodynamic performance of the 4 -10 K ADR. This ADR utilizes an Nb3Sn superconducting magnet and Gadolinium Gallium Garnet (GGG) as its refrigerant. Results show that an idealized cycle, one where its hold time at 4 K is equal to the recycle time, can lift 13 mW at 4 K with a hold time of 132 seconds.

CADR

An adiabatic demagnetization refrigerator for infrared bolometers

Adiabatic demagnetization refrigerators have been built and installed in small portable liquid helium cryostats to test the feasibility of this method of cooling infrared bolometric detectors to temperatures below 0.3 K. Performance has been achieved which suggests that bolometer temperatures of 0.2 K can be maintained for periods of approximately 60 hours. Applications to sensitive infrared detection from ground-based telescopes and space satellites are discussed. Design data are given which permit the evaluation of refrigerator performance for a variety of design parameters.

Britt, R. D.

Design of an adiabatic demagnetization refrigerator for studies in astrophysics

An adiabatic demagnetization refrigerator was designed for cooling infrared bolometers for studies in astrophysics and aeronomy. The design was tailored to the requirements of a Shuttle sortie experiment. The refrigerator should be capable of maintaining three bolometers at 0.1 K with a 90% cycle. The advantage are of operations the bolometer at 0.1K. greater sensitivity, faster response time, and the ability to use larger bolometer elements without compromising the response time. The design presented is the first complete design of an ADR intended for use in space. The most important of these specifications are to survive a Shuttle launch, to operate with 1.5 K - 2.0 K space-pumped liquid helium as a heat sink, to have a 90% duty cycle, and to be highly efficient.

Castles, S.

Bolometers operated at 0.1 K and 0.2 K cooled by adiabatic demagnetization

The construction of bolometers operating at temperatures of 0.1 K and 0.2 K and cooled by adiabatic demagnetization is reported. The electrical noise-equivalent power (NEP) of the bolometers was found to be 1.8 and 6.6 x 10 to the -16th W/sq rt Hz, respectively. These values are within a factor of two of the expected performance based upon bolometer theory. The thermistor material used was gallium-doped single-crystal germanium, for which a resistivity temperature dependence is found.

Lesyna, L.

A progress report on bolometers operating at 0.1 K using adiabatic demagnetization refrigeration

Bolometers are still the detectors of choice for low background infrared observations at wavelengths longer than 200 microns. In the low background limit, bolometers become more sensitive as their operating temperature decreases, due to fundamental thermodynamic laws. The adiabatic demagnetization technique was evaluated by building a bolometer detection system operating at a wavelength of 1 millimeter for use at a ground based telescope. The system was fit checked at the telescope and is expected to take its first data in November, 1985.

Roellig, T.

An adiabatic demagnetization cooled bolometer system

An adiabatic demagnetization refrigeration (ADR) system suitable for cooling bolometers for use at infrared and submillimeter wavelengths is constructed. Because it does not rely on a gravitational field for operation, this refrigeration method has been proposed to cool bolometers intended for NASA's Space Infrared Telescope Facility. To explore the use of ADR in this manner, a portable instrument that has been used successfully for ground-based astronomical observations was constructed. By employing chromic potassium sulfate as a paramagnetic cooling material, bolometers were cooled to temperatures of 0.1 K with a cryogenic hold time of greater than nine hours.

Lesyna, L.

An adiabatic demagnetization refrigerator for SIRTF

An adiabatic demagnetization refrigerator (ADR) has been proposed to cool bolometric infrared detectors on the multiband imaging photometer of the Space Infrared Telescope Facility (SIRTF). One such refrigerator has been built which uses a ferric ammonium alum salt pill suspended by nylon threads in a 3-T solenoid. The resonant modes of this suspension are above 100 Hz. The heat leak to the salt pill is less than 0.5 microW. The system has a hold time at 0.1K of more than 12 h. The cold stage temperature is regulated with a feedback loop that controls the magnetic field. A second, similar refrigerator is being built at a SIRTF prototype to fly on a ballon-borne telescope. It will use a ferromagnetic shield. The possibility of using a high-Tc solenoid-actuated heat switch is also discussed.

Timbie, P. T.

Adiabatic demagnetization refrigerator for space use

An Adiabatic Demagnetization Refrigerator (ADR) for space use is under development at NASA's Goddard Space Flight Center (GSFC). The breadboard ADR operated at 100 mK for 400 minutes. Some significant changes to that ADR, designed to eliminate shortcomings revealed during tests, are reported. To increase thermal contact, the ferric ammonium sulfate crystals were grown directly on gold-plated copper wires which serve as the thermal bus. The thermal link to the X-ray sensors was also markedly improved. To speed up the testing required to determine the best design parameters for the gas gap heat switch, the new heat switch has a modular design and is easy to disassemble.

Serlemitsos, A. T.

Salt materials testing for a spacecraft adiabatic demagnetization refrigerator

As part of a technology development effort to qualify adiabatic demagnetization refrigerators for use in a NASA spacecraft, such as the Space Infrared Telescope Facility, a study of low temperature characteristics, heat capacity and resistance to dehydration was conducted for different salt materials. This report includes results of testing with cerrous metaphosphate, several synthetic rubies, and chromic potassium alum (CPA). Preliminary results show that CPA may be suitable for long-term spacecraft use, provided that the salt is property encapsulated. Methods of salt pill construction and testing for all materials are discussed, as well as reliability tests. Also, the temperature regulation scheme and the test cryostat design are briefly discussed.

Savage, M. L.

Design of a spaceworthy adiabatic demagnetization refrigerator

A spaceworthy adiabatic demagnetization refrigerator (ADR) under development at NASA-Goddard is presented. A baseline model heat switch was tested extensively with an on/off ratio of about 10,000 and a parasitic heat leak of 10 micro-W. Data obtained from the breadboard models were used to design an ADR with improved structural integrity. The core of the ADR is the salt pill which consists of the paramagnetic salt crystal and the thermal bus. When a magnetic field is applied to the salt it forces the alignment of the magnetic moments, thereby decreasing the entropy of the salt. Preliminary tests results showed a net crystal mass of 680 g instead of the expected 740 g, which indicate that there are gaps in the salt pill. A partial fix was accomplished by sealing helium gas in the salt pill at a pressure of 2 bar, which improved the thermal contact during salt magnetization, at about 2 K.

Serlemitsos, A. T.

Magnetic shielding for a spaceborne adiabatic demagnetization refrigerator (ADR)

The Goddard Space Flight Center has studied magnetic shielding for an adiabatic demagnetization refrigerator. Four types of shielding were studied: active coils, passive ferromagnetic shells, passive superconducting coils, and passive superconducting shells. The passive superconducting shells failed by allowing flux penetration. The other three methods were successful, singly or together. Experimental studies of passive ferromagnetic shielding are compared with calculations made using the Poisson Group of programs, distributed by the Los Alamos Accelerator Code Group of the Los Alamos National Laboratory. Agreement between calculation and experiment is good. The ferromagnetic material is a silicon iron alloy.

Warner, Brent A.

A Multi-Stage Continuous-Duty Adiabatic Demagnetization Refrigerator

The design for a multi-stage adiabatic demagnetization refrigerator (ADR) that can provide continuous cooling at very low temperatures is presented. The ADR is being developed for use in x-ray, IR and sub-millimeter space astronomy missions which will employ large format detector arrays operating at 50 mK and lower and which may dissipate up to 10 microwatts. It is also being designed to reject heat slowly to a relatively warm heat sink (in the 6-10 K range), so that future missions may use mechanical cryocoolers instead of liquid helium for pre-cooling. The continuous nature of the device gives it a much higher cooling power per unit mass, allowing it to be much smaller and lighter than existing ADRs with comparable performance. Design details are discussed along with prototype test results.

Shirron, P. J.