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At least 37 records · Page 2

Growth of metal nanoparticles in hydrocarbon atmosphere of arc discharge

A direct current (DC) arc discharge is a widely used method for large-scale production of metal nanoparticles, core–shell particles, and carbon nanotubes. Here, the growth of iron nanoparticles is explored in a modified DC arc discharge. Iron particles are produced by the evaporation of an anode, made from low-carbon steel. Methane admixture into argon gas serves as a carbon source. Electron microscopy and elemental analysis suggest that methane and/or products of its decomposition adhere to iron clusters forming a carbon shell, which inhibits iron particle growth until its full encapsulation, at which point the iron core growth is ceased. Experimental observations are explained using an aerosol growth model. The results demonstrate the path to manipulate metal particle size in a hydrocarbon arc environment.

77 NANOSCIENCE AND NANOTECHNOLOGY↗

Control apparatus for spectral energy source

Automatic light-controlling system for dc arc emission spectrographs controls the vaporization rate of the sample and stabilizes the dc arc. The output energy is regulated such that advantage can be taken of the highly sensitive dc arc source without sacrificing the desired precision.

Gordon, W. A.↗

Enhanced Bottom Anode Monitoring in DC Electric Arc Furnaces Using Fiber-Optic Sensors

A pin style bottom anode employs conductive steel rods that serve as the pathway for the high electrical power through rammed refractory at the bottom of a DC Electric Arc Furnace (EAF). Anode wear during operation is important to monitor, as anode replacement is expensive and impacts EAF productivity. Liquid steel penetration into the un-sintered refractory layer can result from rapid electrical power ramp-up, dips in furnace temperature, or operating the anode for too long between EAF campaigns. In extreme cases, the liquid steel may penetrate the bottom of the furnace when anode wear progresses too close to the bottom shell, which is extremely dangerous and must be avoided. The current state of the art for monitoring bottom anode wear employs thermocouples imbedded in the anode pins at points in the anode. However, this approach is not sensitive enough to detect localized damage to the anode, especially when cracking occurs. Here, the present work utilizes fiber optic sensors to monitor the health of the anode, by creating a real-time spatially distributed temperature map of the anode. Unlike the traditional thermocouples, these sensors can be mounted at significantly greater depths, provide distributed temperature measurements, and can withstand temperatures of up to 900°C. Additionally, they are able to perform temperature measurements with a spatial resolution of 1.3 mm at a 5 Hz acquisition rate, providing unprecedented high-density real time monitoring of anode health and increasing the efficiency, and safety of EAF operation.

Bottom Anode↗

Electric arc heater is self starting

Remote method initiates an electric arc over a large range of gaps between two water-cooled electrodes of an arc-heated wind tunnel without disassembling the arc unit. This type of starting system can be used on both three-phase ac arc heaters and dc arc heaters.

Brown, R. D.↗

Magnetic Measurements of Arc Instabilities in Segmented Arc Heater Column

The Aerodynamic Heating Facility (AHF) at NASA Ames Research Center (ARC) generates high enthalpy, supersonic flow environments for ground testing of NASAheat shield materials. This arc jet heater operates by passing a DC arc (<3200A,<2500V) through a gas column (~10cm diameter, 2m length) and ejecting the heatedgas through a supersonic nozzle into a test chamber. The arc plasma is a partially ionized air mixture at low temperature (< 2eV) but needs to be stable for long test times (up to 30min) at high power (< 20MW). Currently, the operational envelope of the facility is limited by arc instabilities including the kink instability. Consequently, it is of interest to characterize these instabilities to better understand facility limits and inform methods to extend stable operational ranges. Due to the high enthalpy and long timescales (i.e., minutes) diagnostics must be non-invasive. This work will cover the development of two sets of magnetic sensors: differential B-dot sensors and tri-axial magnetic hall sensors and will describe initial measurements of arc motion usingthese sensors.

Kink instability↗

Magnetic Measurements of Arc Instabilities in Segmented Arc Heater Column

The Aerodynamic Heating Facility (AHF) at NASA Ames Research Center (ARC) generates high enthalpy, supersonic flow environments for ground testing of NASAheat shield materials. This arc jet heater operates by passing a DC arc (<3200 A,<2500 V) through a gas column (~6 cm diameter, 2 m length) and ejecting the heated gas through a supersonic nozzle into a test chamber. The arc plasma is a partially ionized air mixture at low temperature (< 2 eV) but needs to be stable for long test times (up to 30 min) at high power (< 20 MW). Currently, the operational envelope of the facility is limited by arc instabilities including the kink instability. Consequently, it is of interest to characterize these instabilities to better understand facility limits and inform methods to extend stable operational ranges. Due to the high enthalpy and long timescales (i.e., minutes) diagnostics must be non-invasive. This work will cover the development of two sets of magnetic sensors: differential B-dot sensors and tri-axial magnetic hall sensors and will describe initial measurements of arc motion using these sensors.

Kink instability↗

Arc-textured metal surfaces for high thermal emittance space radiators

Carbon arc electrical discharges struck across the surfaces of metals such as Nb-1 percent Zr, alter the morphology to produce a high thermal emittance surface. Metal from the surface and carbon from the arc electrode vaporize during arcing, and then condense on the metal surface to produce a microscopically rough surface having a high thermal emittance. Quantitative spectral reflectance measurements from 0.33 to 15 microns were made on metal surfaces which were carbon arc treated in an inert gas environment. The resulting spectral reflectance data were then used to calculate thermal emittance as a function of temperature for various methods of arc treatment. The results of arc treatment on various metals are presented for both ac and dc arcs. Surface characterization data, including thermal emittance as a function of temperature, scanning electron microscopy, and atomic oxygen durability, are also presented. The ac arc texturing was found to increase the thermal emittance at 800 K from 0.05 to 0.70.

Banks, Bruce A.↗

NASA/Ames Research Center DC-8 data system

In-flight facility data acquisition, distribution, and recording on the NASA Ames Research Center (ARC) DC-8 are performed by the Data Acquisition and Distribution System (DADS). Navigational and environmental data collected by the DADS are converted to engineering units and distributed real-time to investigator stations once per second. Selected engineering units data are printed and displayed on closed circuit television monitors throughout flights. An in-flight graphical display of the DC-8 flight track (with barbs indicating wind direction and magnitude) has recently been added to the DADS capabilities. Logging of data run starts/stops and commentary from the mission director are also provided. All data are recorded to hard disk in-flight and archived to tape medium post-flight. Post-flight, hard copies of the track map and mission director's log are created by the DADS. The DADS is a distributed system consisting of a data subsystem, an Avionic Serial Data-to-VMEbus (ASD2VME) subsystem, and a host subsystem. Each subsystem has a dedicated central processing unit (CPU) and is capable of stand-alone operation. All three subsystems are housed in a single 20-slot VME chassis and communicate with each other over the VMEbus. The data and host subsystems are briefly discussed, and the DC-8 DADS internal configuration and system block diagram are presented.

Cherniss, S. C.↗

A facility for the simulation of low orbit atmospheric oxygen bombardment

A molecular beam facility to simulate the space environment of a spacecraft at low orbit was designed with the intent of studying the effect on the properties of optical elements of oxygen atoms impacting at orbital velocity. The four-stage differentially pumped molecular beam facility includes a variety of oxygen atom beam sources which cover a wide range of velocities (1 km/sec to approximately 8 km/sec), in addition to the ultra-clean experimental environmental of an ultra-high vacuum chamber and an optical diagnostic set-up. The primary oxygen atom beam source used to obtain the 8 km/sec O atoms is an arc heated source. It consists of a modified commercially available plasma torch. The modifications include attachments which provide for a nozzle which is used to expand the atomic beam into the vacuum system, and exhaust channels to dispose of excess torch gas. The torch operates in the 'nontransferred' mode of operation, that is the electric arc is confined within the torch. A plasma is formed in helium by a dc arc. A small amount of O2 is injected downstream from the arc where it is thermally dissociated by the hot He into oxygen atoms. The high temperature and isentropic expansion give the oxygen atoms their velocity. Using seeded beam techniques, oxygen atom beams of approximately 3.5 and approximately 1.5 km/sec, respectively, are obtained.

Arnold, G. S.↗

Arcjet load characteristics

Experiments were conducted to define the interface characteristics and constraints of 1 kW class arcjets run on simulated decomposition products of hydrazine and power processors. The impacts of power supply output current ripple on arcjet performance were assessed by variation of the ripple frequency from 100 Hz to 100 kHz with 10 percent peak-to-peak ripple amplitude at 1.2 kW. Ripple had no significant effects on thrust, specific impulse or efficiency. The impact of output ripple on thruster lifetime was not assessed. The static and dynamic impedances of the arcjet were quantified with two thrusters of nearly identical configuration. Superposition of an AC component on the DC arc current was used to characterize the dynamic impedance as a function of flow rate and DC current level. A mathematical model was formulated from these data. Both the static and dynamic impedance magnitude were found to be dependent on mass flow rate. The amplitude of the AC component was found to have little effect on the dynamic impedance. Reducing the DC level from 10 to 8 amps led to a large change in the magnitude of the dynamic impedance with no observable phase change. The impedance data compared favorably between the two thrusters.

Hamley, John A.↗

Arcjet load characteristics

Experiments were conducted to define the interface characteristics and constraints of 1 kW class arcjets run on simulated decomposition products of hydrazine and power processors. The impacts of power supply output current ripple on arcjet performance were assessed by variation of the ripple frequency from 100 Hz to 100 kHz with 10 percent peak-to-peak ripple amplitude at 1.2 kW. Ripple had no significant effects on thrust, specific impulse or efficiency. The impact of output ripple on thruster lifetime was not assessed. The static and dynamic impedances of the arcjet were quantitied with two thrusters of nearly identical configuration. Superposition of an AC component on the DC arc current was used to characterize the dynamic impedance as a function of flow rate and DC current level. A mathematical model was formulated from these data. Both the static and dynamic impedance magnitude were found to be dependent on mass flow rate. The amplitude of the AC component was found to have little effect on the dynamic impedance. Reducing the DC level from 10 to 8 amps led to a large change in the magnitude of the dynamic impedance with no observable phase change. The impedance data compared favorably between the two thrusters.

Hamley, John A.↗

Orienting Arc Lamps for Longest Life

Temperature distribution strongly affects performance. Tests on floodlights for Space Shuttle payload bay show useful life of metal halide dc arc lamp prolonged by mounting "anode down" and wiring for maximum heat conduction away from electrodes. Anode-down configuration, anode and cathode temperatures stabilize at 333 degrees and 313 degrees C, respectively, after 1 hour of operation. Temperatures both below limit for quartz-to-metal seals, and lamps able to withstand a 2,000-hour life test with satisfactory light output at end.

Kiss, J.↗

Anode arc motion in high power arcjets

The long-term operational lifetime of most medium to high power arcjets is currently limited by the rapid deterioration of the arcjet electrodes. To a large extent, the rate of this deterioration is related to the motion of the arc discharge on the electrode surfaces. This paper details a series of experiments aimed at studying the temporal behavior of dc arcs on a water-cooled radially-segmented 30 kW class arcjet anode. The experimental anode used for these tests was made of copper, and was divided into four equivalent radial segments which were electrically isolated with aluminum oxide gaskets. The current carried by each segment was measured independently using four calibrated resistive shunts, and was analyzed by digital computer. The tests were limited to nitrogen propellant over a current range of 100-250 A dc. Results show that for the range of total currents considered here, the current distribution in the segmented arcjet anode is generally asymmetric, exhibiting random fluctuations over a wide range of frequencies.

Harris, W. J.↗

Optical Plasma Control During ARC Carbon Nanotube Growth

To improve nanotube production, we developed a novel optical control technique, based on the shape of the visible plasma zone created between the anode and the cathode in the direct current (DC) arc process. For a given inert gas, we adjust the anode to cathode distance (ACD) in order to obtain strong visible vortices around the cathode. This enhance anode vaporization, which improve nanotubes formation. In light of our experimental results, we focus our discussion on the relationship between plasma parameters and nanotube growth. Plasma temperature control during arc process is achieved using argon, helium, and their mixtures as a buffer gases. The variation of the gas mixture from pure argon to pure helium changes plasma temperature. As a consequence, the microscopic characteristics of nanotubes as diameter distribution is changed moving from smaller values for argon to higher diameters for helium. We also observe a dependence of the macroscopic characteristics of the final products as Brunauer-Emmett-Teller (BET) surface area.

Hinkov, I.↗

Pulsed metallic-plasma generators.

A pulsed metallic-plasma generator is described which utilizes a vacuum arc as the plasma source. The arc is initiated on the surface of a consumable cathode which can be any electrically conductive material. Ignition is accomplished by using a current pulse to vaporize a portion of a conductive film on the surface of an insulator separating the cathode from the ignition electrode. The film is regenerated during the ensuing arc. Over 100 million ignition cycles have been accomplished by using four 0.125-in. diameter zinc cathodes operating in parallel and high-density aluminum-oxide insulators. Among the applications being investigated for the generator are metal deposition, vacuum pumping, electric propulsion, and high-power dc arc interruption.

Gilmour, A. S., Jr.↗