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At least 37 records · Page 2

The magnetic effects of brecciation and shock in meteorites. II - The ureilites and evidence for strong nebular magnetic fields. III - The achondrites

Magnetic studies were conducted on samples of the ureilitic meteorites Goalpara, Havero, Novo Urei, and Kenna. Measurements included bulk magnetic susceptibility, natural remanent magnetization (NRM), saturation remanence, and the demagnetization behavior of NRM and saturation remanence. An approximate 'fossil' magnetic field intensity was determined by analysis of coercivity spectra of NRM and saturation remanence after reheating. It was found that the magnetic susceptibility of ureilites increased with severity of shock, and the NRM intensity decreases while its coercivity spectrum generally hardens with increasing shock. Goalpara and Kenna are distinguished by unexpectedly homogeneous, strong, stable, and directionally clustered NRM, indicative of a unique original magnetizing event. The results support the assertion that both ureilites and carbonaceous chondrites have formed from related nebular material and provide further evidence for a strong external magnetic field during the accretional stages and throughout an early bombardment stage.

Brecher, A.↗

Magnetic and metallurgical properties of directionally solidified eutectic Bi/MnBi composites - The effects of annealing

Eutectic Bi/MnBi (97.8 a/o Bi) samples have been plane-front directionally solidified. The resultant microstructures consist of elongated, aligned particles of MnBi dispersed in a Bi-matrix. Magnetization as a function of temperature (4.2 to 300 K) and applied field (up to 220 kG) has been used to evaluate solidification parameters and magnetic properties. At room temperature, in addition to the diamagnetic contribution of Bi, one finds a superposition of the ferromagnetic, low temperature (LTP) MnBi phase and paramagnetic phases. At cryogenic temperatures, one of the room temperature paramagnetic phases is ferromagnetic with an intrinsic coercivity of 120 kOe while the other remains paramagnetic for low fields and orders ferromagnetically at high fields in a complicated way. Annealing of as-grown samples was found to produce significant changes in magnetic properties. The origins of the paramagnetic phases and their relation to the mechanisms which control the coercive field of the hard magnetic LTP MnBi phase are discussed.

Pirich, R. G.↗

Magnetic cristobalite (?) - A possible new magnetic phase produced by the thermal decomposition of nontronite

The effect of heat treatment for 1 h or more at 900-1000 C on the magnetic properties of nontronite, an iron-rich smectite clay thought to be an important component of Martian regolith, is investigated experimentally, extending the findings of Moskowitz and Hargraves (1982). The results are presented in graphs and tables and discussed. A phase with Curie temperature 200-220 C, remanent coercivity greater than 800 mT, and a type-2 room-temperature-coercivity response to thermomagnetic cycling is observed and attributed to an iron-substituted cristobalite which may form by topotactic growth from a smectite precursor.

Moskowitz, B. M.↗

Plasma sprayed Fe(76)Nd(16)B(8) permanent magnets

Thin coatings (0.16 mm) and thick coatings (0.50 mm) of Fe(76)Nd(16)B(8) were deposited on stainless-steel substrates by low pressure plasma spraying. Microscopic examination of the coatings in a light microscope revealed excessive porosity, but good bonding to the substrate. Fracture cross sections examined in a scanning electron microscope showed the grains to be equiaxed and approximately 1 micron or less in diameter in the as-sprayed condition. The intrinsic coercivities of the as-sprayed coatings varied from 5.8 to 10.9 kOe. The effects of postspray heat treatments on the intrinsic coercivity are also given.

Overfelt, R. A.↗

The augmented Lagrangian method for parameter estimation in elliptic systems

In this paper a new technique for the estimation of parameters in elliptic partial differential equations is developed. It is a hybrid method combining the output-least-squares and the equation error method. The new method is realized by an augmented Lagrangian formulation, and convergence as well as rate of convergence proofs are provided. Technically the critical step is the verification of a coercivity estimate of an appropriately defined Lagrangian functional. To obtain this coercivity estimate a seminorm regularization technique is used.

Ito, Kazufumi↗

M-H characteristics and demagnetization resistance of samarium-cobalt permanent magnets to 300 C

The influence of temperature on the M-H demagnetization characteristics of permanent magnets is important information for the full utilization of the capabilities of samarium-cobalt magnets at high temperatures in demagnetization-resistant permanent magnet devices. In high temperature space power converters, such as free-piston Stirling engine driven linear alternators, magnet demagnetization can occur as a long-term consequence of thermal agitation of domains and of metallurgical change, and also as an immediate consequence of too large an applied field. Investigated here is the short-term demagnetization resistance to applied fields derived from basic M-H data. This quasistatic demagnetization data was obtained for commercial, high-intrinsic-coercivity, Sm2Co17-type magnets from 5 sources, in the temperature range 23 to 300 C. An electromagnet driven, electronic hysteresigraph was used to test the 1-cm cubic samples. The observed variation of the 2nd quadrant M-H characteristics was a typical rapid loss of M-coercivity and a relatively lesser loss of remanence with increasing temperature. The 2nd quadrant M-H curve knee point is used to define the limits of operation safe against irreversible demagnetization due to an excessive bucking field for a given flux density swing at temperature. Such safe operating area plots are shown to differentiate the high temperature capabilities of the samples from different sources. For most of the samples, their 2nd quadrant M-H loop squareness increased with temperature, reaching a peak or a plateau above 250 C.

Niedra, Janis M.↗

M-H characteristics and demagnetization resistance of samarium-cobalt permanent magnets to 300 C

The influence of temperature on the M-H demagnetization characteristics of permanent magnets is important information for the full utilization of the capabilities of samarium-cobalt magnets at high temperatures in demagnetization-resistant permanent magnet devices. In high temperature space power converters, such as free-piston Stirling engine driven linear alternators, magnet demagnetization can occur as long-term consequence of thermal agitation of domains and of metallurgical change, and also as an immediate consequence of too large an applied field. Investigated here is the short-term demagnetization resistance to applied fields derived from basic M-H data. These quasistatic demagnetization data were obtained for commercial, high-intrinsic-coercivity, Sm2Co17-type magnets from 5 sources, in the temperature range 23 to 300 C. An electromagnet driven, electronic hysteresigraph was used to test the 1-cm cubic samples. The observed variation of the 2nd quadrant M-H characteristics was a typical rapid loss of M-coercivity and a relatively lesser loss of remanence with increasing temperature.

Niedra, J. M.↗

Characterization facility for magneto-optic media and systems

Objectives of this research are: (1) to measure the hysteresis loop, Kerr rotation angle, anisotropy energy profile, Hall voltage, and magnetoresistance of thin-film magneto-optic media using our loop-tracer; (2) measure the wavelength-dependence of the Kerr rotation angle, Theta(sub k), and ellipticity, epsilon(sub k), for thin-film media using our magneto-optic Kerr spectrometer (MOKS); (3) measure the dielectric tensor of thin-film and multilayer samples using our variable-angle magneto-optic ellipsometer (VAMOE); (4) measure the hysteresis loop, coercivity, remanent magnetization, saturation magnetization, and anisotropy energy constant for thin film magnetic media using vibrating sample magnetometry; (5) observe small magnetic domains and investigate their interaction with defects using magnetic force microscopy; (6) perform static read/write/erase experiments on thin-film magneto-optic media using our static test station; (7) integrate the existing models of magnetization, magneto-optic effects, coercivity, and anisotropy in an interactive and user-friendly environment, and analyze the characterization data obtained in the various experiments, using this modeling package; (8) measure focusing- and tracking-error signals on a static testbed, determine the 'feedthrough' for various focusing schemes, investigate the effects of polarization and birefringence, and compare the results with diffraction-based calculations; and (9) measure the birefringence of optical disk substrates using two variable angle ellipsometers.

Mansuripur, M.↗

Short-Term Aging of NeFeB Magnets for Stirling Linear Alternator Applications

NeFeB type magnets have been proposed for use in free piston Stirling engine driven, linear alternators to generate electric power during long duration space missions. These type of materials provide the highest energy product commercial magnets, thus minimizing alternator size or mass, but do not provide the high temperature stability of magnetic properties found in the SmCo type magnets. Therefore, to apply the NeFeB type magnets at elevated temperatures to multiyear space missions, their long-term aging characteristics must be determined. This report presents 200 hr aging data for six types of NeFeB magnets selected from three manufacturers. Aging was performed under vacuum at 150 C, with a steady demagnetizing field of 5 kOe applied. From the data produced by this short-term aging run, candidate magnet types were selected for a planned 12,000 hr long-term run. Depending on the manufacturer's magnet type, remanence losses observed ranged from 0 to 7%, when measured at 120 C on an established recoil line. Also, intrinsic coercivity losses up to about 4% were observed for the M-H curve at 120 C. In some cases, these coercivity losses were not recoverable by recharge of the magnet, indicating a structural change of the material.

Niedra, Janis M.↗

Effect of Shock on the Magnetic Properties of Pyrrhotite, the Martian Crust, and Meteorites

We performed planar shock recovery experiments on natural pyrrhotite at pressures up to 6.9 GPa. We find that high-field isothermal remanent magnetization in pyrrhotite is demagnetized up to 90% by shock due to preferential removal of low coercivity components of magnetization. Contrary to static experiments, we do not observe complete demagnetization. Post shock permanent changes in magnetic properties include increasing saturation isothermal remanent magnetization, bulk coercivity and lowtemperature memory, and changes in squareness of hysteresis. These changes are consistent with an increase in the volume fraction of single domain grains. The lack of magnetic anomalies over large Martian impact basins is not expected to be solely due to shock demagnetization of the crust. We find that pyrrhotite-bearing rocks and meteorites can retain records of Martian magnetic fields even if shocked to pressures approaching 7 GPa. However, some paleointensity techniques may underestimate this field.

Louzad, Karin L.↗

Low frequency creep in CoNiFe films

The results of an investigation of domain wall motion excited by slow rise-time, bipolar, hard-axis pulses in vacuum deposited CoNiFe films 1500A to 2000A thick are presented. The results are consistent with those of comparable NiFe films in spite of large differences in film properties. The present low frequency creep data together with previously published results in this and other laboratories can be accounted for by a model which requires that the wall structure change usually associated with low frequency creep be predominately a gyromagnetic process. The correctness of this model is reinforced by the observation that the wall coercive force, the planar wall mobility, and the occurrence of an abrupt wall structure change are the only properties closely correlated to the creep displacement characteristics of a planar wall in low dispersion films.

Bartran, D. S.↗

Design and material selection for inverter transformer cores

Report is announced which studied magnetic properties of candidate materials for use in spacecraft transformers, static inverters, converters, and transformer-rectifier power supplies. Included are material characteristics for available alloy compositions in tabular form, including: trade names, saturated flux density, dc coercive force, loop squareness, material density, and watts per pound at 3 KHz.

Mclyman, W. T.↗

Low-frequency creep in CoNiFe films.

Domain wall motion excited by slow rise-time, bipolar, hard-axis pulses in vacuum deposited CoNiFe films from 1500 to 2000 A thick is studied. The results are consistent with those of comparable NiFe films. Furthermore, the wall coercivity is found to be the most significant sample property correlated to the low-frequency creep properties of all the samples.

Bartran, D. S.↗

A preliminary report on the magnetic measurements of samples 72275 and 72255

The direction and magnitude of natural remanent magnetization of five approximately 3-g subsamples of 72275 and 72255 and the high field saturation magnetization, coercive force, and isothermal remanent magnetization of 100-mg chip from each of these samples, were studied. Given an understanding of the magnetization processes, group 1 experiments provide information about the absolute direction of the ancient magnetizing field and a qualitative estimate of its size (paleointensity). The group 2 experiments yield a quantitative estimate of the iron content and a qualitative ideal of the grain sizes.

Banerjee, S. K.↗

Investigation of the growth of garnet films by liquid phase epitaxy

Liquid phase expitaxy was investigated to determine its applicability to fabricating magnetic rare earth garnet films for spacecraft data recording systems. Two mixed garnet systems were investigated in detail: (1) Gd-Y and (2) Eu-Yb-Y. All films were deposited on Gd3Ga5012 substrates. The uniaxial anisotropy of the Gd-Y garnets is primarily stress-induced. These garnets are characterized by high-domain wall mobility, low coercivity and modest anisotropy. Characteristic length was found to be relatively sensitive to temperature. The Eu-Yb-Y garnets exhibit acceptable mobilities, good temperature stability and reasonable quality factors. The uniaxial anisotropy of these garnets is primarily growth-induced. The system is well suited for compositional "tailoring" to optimize specific desirable properties. Liquid phase epitaxy can be used to deposit Gd3Ga5012 spacing layers on magnetic garnet films and this arrangement possesses certain advantages over more conventional magnetic filmspacing layer combinations. However, it cannot be used if the magnetic film is to be ion implanted.

Moody, J. W.↗

Remanent magnetization and structural effects due to shock in natural and man-made iron-nickel alloys

Explosive shock or meteorite impact are significant remagnetization processes. The mechanisms of remagnetization associated with the dynamic processes depend on the peak shock pressure, the nature of the shocked materials, and the behavior of the shock in the material. Magnetic measurements can be used to classify products formed during a shock process, and magnetic measurements can be used to investigate the process itself because of the special characteristics of the remanent magnetization vectors. The magnetic coercive force increases more rapidly in quenched and annealed iron-nickel alloys as nickel is added than it does in the alloys which have been shocked.

Wasilewski, P. J.↗