Investigation of resin systems for improved ablative materials
Resin systems for matrix material in ablative composite for liquid rocket combustion chambers using fluorine-containing propellants
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Resin systems for matrix material in ablative composite for liquid rocket combustion chambers using fluorine-containing propellants
Experimental efforts to develop a new procedure to measure char depth in carbon phenolic nozzle material are described. Using a Shor Type D Durometer, hardness profiles were mapped across post fired sample blocks and specimens from a fired rocket nozzle. Linear regression was used to estimate the char depth. Results are compared to those obtained from computed tomography in a comparative experiment. There was no significant difference in the depth estimates obtained by the two methods.
Internal temperatures of ablating material measured by thermocouple configurations
Comparisons of ablation calculations with the charring ablation computer code and ablation test data are presented over a wide range of environmental conditions in air for three materials: low-density nylon phenolic, Avcoat 5026-39HC/G, and a filled silicon elastomer. Heat fluxes considered range from over 500 Btu/sq ft-sec to less than 50 Btu/sq ft-sec. Pressures range from 0.5 atm to .004 atm. Enthalpies range from about 2000 Btu/lb to 18000 Btu/lb. Predictions of recession, pyrolysis penetration, and thermocouple responses are considered. Recession predictions for nylon phenolic are good as steady state is approached, but strongly transient cases are underpredicted. Pyrolysis penetrations and thermocouple responses are very well predicted. Recession amounts for Avcoat and silicone elastomer are less well predicted, although high heat flux cases near steady state are fairly satisfactory. Pyrolysis penetrations and thermocouple responses are very well predicted.
Ablative materials performance in high radiative heat flux environments produced by CW carbon dioxide laser
Spacecraft reentry flight tests for determining performance of heat shields made of charring ablating material
Asbestos free solid motor internal insulation samples were tested at the MSFC Hyperthermal Facility. Objectives of the test were to gather data for analog characterization of ablative and in-depth thermal performance of rubber materials subject to high enthalpy/pressure flow conditions. Tests were conducted over a range of convective heat fluxes for both inert and chemically reactive sub-sonic free stream gas flow. Instrumentation included use of total calorimeters, thermocouples, and a surface pyrometer for surface temperature measurement. Post-test sample forensics involved measurement of eroded depth, charred depth, total sample weight loss, and documentation of the general condition of the eroded profile. A complete Charring Material Ablator (CMA) style aero-thermal analysis was conducted for the test matrix and results compared to the measured data. In general, comparisons were possible for a number of the cases and the results show a limited predictive ability to model accurately both the ablative response and the in-depth temperature profiles. Lessons learned and modeling recommendations are made regarding future testing and modeling improvements that will increase understanding of the basic chemistry/physics associated with the complicated material ablation process of rubber materials.
Ablative material evaluation for nozzle sections of storable propellant rocket engine
Thermal analysis on pyrolysis of charring ablator materials
Ablative materials performance for solid rocket nozzle applications
Chemical equilibrium of ablation materials including condensed species
Ablative materials in hydrogen/oxygen thrust chamber using expansion nozzle to substitute regenerative thrust chamber assembly
A program to improve ablative materials for the Advanced Solid Rocket Motor (ASRM) is briefly discussed. The main concerns with the baseline material are summarized along with the measures being undertaken to obtain improvements. The materials involved in the program, all of which have been manufactured and are now being evaluated, are mentioned.
Asbestos free solid motor internal insulation samples were recently tested at the MSFC Hyperthermal Arc Jet Facility. Objectives of the test were to gather data for solid rocket motor analog characterization of ablative and in-depth thermal performance of rubber materials subject to high enthalpy/pressure flow conditions. Tests were conducted over a range of convective heat fluxes for both inert and chemically reactive sub-sonic free stream gas flow. Active instrumentation included use of total calorimeters, in-depth thermocouples, and a surface pyrometer for in-situ surface temperature measurement. Post-test sample forensics involved determination of eroded depth, charred depth, total sample weight loss, and documentation of the general condition of the eroded profile. A complete Charring Material Ablator (CMA) style aero thermal analysis was conducted for the test matrix and results compared to the measured data. In general, comparisons were possible for a number of the cases and the results show a limited predictive ability to model accurately both the ablative response and the in-depth temperature profiles. Lessons learned and modeling recommendations are made regarding future testing and modeling improvements that will increase understanding of the basic chemistry/physics associated with the complicated material ablation process of rubber materials.
Effect of enthalpy variation on ablating materials
Investigation in atmosphere entry simulator of nylon as ablative material for ballistic missiles
Techniques for rating performance of ablative materials in liquid-propellant rocket engines
Ability of several ablating materials to reduce surface heat transfer in electric arc heated airstream