Engineering Papers⌕ Search

SEARCH · Engineering Papers

Results for “Microwave heating”

Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

Quote a phrase for an exact phrase match. Source license links do not imply unrestricted reuse.

At least 343 records · Page 19
All sourcesNASA NTRSDOE OSTI
DOE OSTI2025

Technoeconomic Analysis of Microwave-Assisted Dry Reforming Integrated with Chemical Looping for Production of Methanol

Methanol is a key component in producing formaldehyde, acetic acid, and methyl tert -butyl ether (MTBE) and supports a wide array of industries, including plastics, textiles, and automotive. It also plays a growing role in renewable energy solutions. However, the conventional production of methanol involves steam reforming of methane, which is very energy-intensive and produces significant quantities of the greenhouse gas carbon dioxide. In this research, a chemical looping scheme is combined with dry reforming of natural gas in a novel microwave reactor to produce an industrial quantity of methanol. A heat exchanger network is developed to substantially reduce hot and cold utility usage. The effect of the cost of purchasing carbon dioxide from an external source for dry reforming, the capital cost of the microwave reactor, and the cost of electricity on the net present value is analyzed. Technoeconomic comparison with the conventional industrial process that produces methanol via steam reforming of methane indicates that the chemical looping generates a significant positive net present value along with a substantial reduction in carbon dioxide emissions while producing methanol significantly below the U.S. Department of Energy’s goal of $800/ton.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
NASA NTRS1991

In-situ sputtering of YBCO films for microwave applications

RF magnetron sputtering from a single YBCO target onto a heated substrate (700 C) was used to obtain c-axis-oriented 1-2-3 films that are superconducting without a subsequent annealing or oxygenation step, with Tc(R = 0) as high as 88 K on MgO and LaAlO3 substrates. This process uses an 8-in-diameter target in the sputter-up configuration, with a central grounded shield to eliminate negative ion bombardment. It can reproducibly and uniformly cover substrates as large as 3-in across at rates exceeding 1 A/s. Maintaining film composition very close to stoichiometry is essential for obtaining films with good superconducting properties and surface morphology. Optimum films have critical currents of 1 MA/sq cm at 77 K. Measurements of microwave surface resistance based on a stripline resonator indicate low surface resistance for unpatterned YBCO ground planes, but excess loss and a strong power dependence in a patterned center strip.

Ballentine, P. H.↗
NASA NTRS1973

Complex permittivity measurements during high temperature recycling of space shuttle antenna window and dielectric heat shield materials

The research performed and the data obtained on candidate space shuttle antenna window and heat shield materials are presented. The measurement technique employs a free-space focused beam microwave bridge for obtaining RF transmission data, and a device which rotates a sample holder which is heated on one side by natural gas-air flames. The surface temperature of each sample is monitored by IR pyrometry; embedded and rear surface thermocouples are also used in obtaining temperature data. The surface of the sample undergoing test is subjected to approximately the same temperature/time profile that occurs at a proposed antenna position on the space shuttle as it re-enters. The samples are cycled through ten of these temperature profiles to determine the recycling effects. Very little change was noted in the materials due to the recycling.

Bassett, H. L.↗
NASA NTRS1980

Joint microwave and infrared studies for soil moisture determination

The feasibility of using a combined microwave-thermal infrared system to determine soil moisture content is addressed. Of particular concern are bare soils. The theoretical basis for microwave emission from soils and the transport of heat and moisture in soils is presented. Also, a description is given of the results of two field experiments held during vernal months in the San Joaquin Valley of California.

Njoku, E. G.↗
NASA NTRS1991

Multispectral satellite data in the context of land surface heat balance

Multispectral satellite data are demonstrated to be an important potential contributor to the understanding and completeness of heat balance analysis. Satellite observations are presented, including visible, near-IR, IR, and microwave bands, which estimate surface characteristics and surface fluctuations. The relationship of the interannual variations of the satellite data and the land surface changes is discussed. It is shown that spatially representative values of global fluxes and parameters from multispectral data can consistently enhance the results of heat balance analysis. Daily net radiation can be estimated with a 10 percent error, while the error for albedo would be higher. Computations for all heat fluxes except the latent heat flux are shown. Soil moisture and surface temperature estimates can be derived from microwave and IR observations, respectively. Spectral reflectances in the visible and near-IR bands are suggested as important heat-balance indices for future consideration.

Choudhury, Bhaskar J.↗
DOE OSTI2020

Dark Photon Oscillations in Our Inhomogeneous Universe

A dark photon kinetically mixing with the ordinary photon represents one of the simplest viable extensions to the standard model, and would induce oscillations with observable imprints on cosmology. Oscillations are resonantly enhanced if the dark photon mass equals the ordinary photon plasma mass, which tracks the free electron number density. Previous studies have assumed a homogeneous Universe; in this Letter, we introduce for the first time an analytic formalism for treating resonant oscillations in the presence of inhomogeneities of the photon plasma mass. We apply our formalism to determine constraints from cosmic microwave background photons oscillating into dark photons, and from heating of the primordial plasma due to dark photon dark matter converting into low-energy photons. Including the effect of inhomogeneities demonstrates that prior homogeneous constraints are not conservative, and simultaneously extends current experimental limits into a vast new parameter space.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2022

Probing Temperature‐Induced Phase Transitions at Individual Ferroelectric Domain Walls

Abstract Ferroelectric domain walls have emerged as one of the most fascinating objects in condensed matter physics due to the broad variability of functional behaviors they exhibit. However, the vast majority of domain walls studies have been focused on bias‐induced dynamics and transport behaviors. Here, the scanning probe microscopy approach based on piezoresponse force microscopy (PFM) with a dynamically heated probe, combining local heating and local biasing of the material is introduced. This approach is used to explore the thermal polarization dynamics in soft Sn 2 P 2 S 6 ferroelectrics, and allows for the exploration of phase transitions at individual domain walls. The strong and weak modulation regimes for the thermal PFM are introduced. The future potential applications of heated probe approach for functional SPM measurements including piezoelectric, elastic, microwave, and transport measurements are discussed.

36 MATERIALS SCIENCE↗
NASA NTRS1995

Remote Sensing of Ocean Wind Using Polarimetric Microwave Radiometers

Winds over the ocean modulate the air-sea fluxes of heat, moisture, gases and particulates, regulating the crucial coupling between atmosphere and ocean that establishes and maintains global and regional climate. Global mapping (using spaceborne scatterometers) of ocean wind is crucial for many oceanographic and atmospheric studies. An overview of polarimetric wind radiometer (new) technology is given.

Ocean Ocean Wind Remote Sensing Radiometer Microwa↗
NASA NTRS1994

Transient microwave brightenings in solar active regions: Comparison between VLA and Yohkoh observations

We report observations of transient microwave (2 cm) brightenings and their relationship with brightenings in soft X-rays. The peak flux of the microwave brightenings observed by the Very Large Array (VLA) is smaller than the previously reported fluxes by two orders of magnitude. The microwave sources were highly polarized (up to 100%) and were situated on the periphery of a sunspot umbra. Among the many transients observed in X-rays by Yohkoh, two were observed simultaneously in microwaves. The microwave sources were found to be closer to the umbra of the sunspot than were the X-ray loops. It seems that the microwave sources are located at the footpoints of the looplike X-ray transients. Using the combined VLA, Yohkoh, and Mees data set, we determine the physical parameters of the loop in which the brightenings occur. We find that an increase in emission measure accompanied by small-scale heating can account for the X-ray brightening. The microwave emission can be interpreted as thermal gyroresonance or nonthermal gyrosynchrotron processes during the X-ray brightening. The magnetic field in the microwave-source region is found to be 1200-1800 G. The observations also provide evidence for temperature gradient in the coronal loops.

Gopalswamy, N.↗
NASA NTRS1989

Solid propellant combustion response to oscillatory radiant heat flux

A progress report is given on a research project to use the microwave Doppler velocimeter technique to measure the combustion response to an oscillating thermal radiation source (CO2 laser). The test technique and supporting analyses are described, and the results are presented for an initial test series on the nonmetallized, composite propellant, Naval Weapons Center formulation A-13. It is concluded that in-depth transmission of radiant heat flux is not a factor at the CO2 laser wave length.

Strand, L. D.↗
DOE OSTI2019

All-Optical Cryogenic Thermometry Based on Nitrogen-Vacancy Centers in Nanodiamonds

The nitrogen-vacancy (N-V) center in diamond has been viewed as a high-sensitivity nanometer-scale metrology platform. Thermometry has been a current focus, with attention largely confined to room-temperature applications. Temperature sensing at low temperatures, yet, remains challenging as the sensitivity decreases for many commonly used techniques, which rely on a temperature-dependent frequency shift of the N-V center's spin resonance and its control with microwaves. Here we use an alternative method that does not require microwaves, ratiometric all-optical thermometry, and demonstrate that it may be utilized to liquid-nitrogen temperatures without deterioration of the sensitivity. The use of an array of nanodiamonds embedded within a portable polydimethylsiloxane sheet provides a versatile temperature-sensing platform that can probe a wide variety of systems without the configurational restrictions needed for applying microwaves. With this device, we observe a temperature gradient over tens of microns in a ferromagnetic-insulator substrate (yttrium iron garnet) under local heating by a resistive heater. This thermometry technique provides a cryogenically compatible, microwave-free, minimally invasive approach capable of probing local temperatures with few restrictions on the substrate materials.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
NASA NTRS1990

Remote sensing of surface turbulence heat flux

The determination of latent heat-flux variability using spaceborne sensors is discussed. Particular attention is given to the microwave sensors which have all weather capability. The retrieval of surface layer humidity, of wind speed and interfacial humidity, and of sensible heat flux are discussed. Both the indirect retrieval and direct retrieval of latent heat flux are considered.

Liu, W. T.↗
DOE OSTI2023

Laser heating of ferroelectric cubes for tunable electromagnetic properties in metamaterials

In this experimental study, we demonstrate the feasibility of a thermally tunable, resonant dielectric microwave metasurface based on sub-wavelength Mie resonances of ferroelectric dielectric cubes (Calcium titanate, CaTiO 3 ) in which the temperature of the meta-atoms can be locally and dynamically controlled by heating with an optical laser beam over a large range of temperatures and, consequently, values of the dielectric constant of the cube and corresponding resonance frequency of the meta-atoms. Further, this avoids any interference of otherwise necessary heating elements or power supply wires with the propagation of the microwave signal and can be made spatially addressable. The concept scales at least to the THz domain. This contactless approach opens up an alternative avenue to tunability and active control of metamaterials.

36 MATERIALS SCIENCE↗
NASA NTRS1980

Solar Power Satellite Microwave Power Transmission System Description Executive Summary

The history of the concept of microwave power beaming to Earth is reviewed with emphasis on transmission frequency selection. Constraints on the system power level results from (1) required rejection of waste heat resulting from inefficiencies in the cover conversion of dc electric power to microwave power; (2) the rf power intensity in the ionosphere; and (3) the effect of sidelobe level on aperture illumination factors. Transmitter arrangement, the power distribution system, attitude control, subarrays, waveguides, and alignment are discussed.

Woodcock, G. R.↗
DOE OSTI2023

Energy-Efficient and Water-Saving Sorbent Regeneration at Near Room Temperature for Direct Air Capture

Here this study reports energy-efficient and water-saving microwave-accelerated regeneration of sorbent (MARS) for dilute carbon capture from the ambient air. The experimental studies indicated that the CO 2 desorption rate from the chemisorbents increased with microwave output under near-isothermal conditions at near room temperature. The reduced activation energy of MARS, i.e., 20–28 kJ/mol, indicated enhanced CO 2 desorption kinetics by microwave-induced rotational–vibrational (rovibrational) coupling transitions, primarily due to the highly polarized feature of the carbamate (CO 2 -PEI). The instant and selective delivery of microwave energy to the targeted polarized C–N bonds at room temperature is particularly advantageous for energy-efficient direct air capture. The experimental results also demonstrated a good working capacity of 0.6–1.4 mmol of CO 2 /g and a promising rapid MARS-DAC process with microwave swing. As it does not require steam regeneration and heat exchanger, a simple MARS process is attractive for CO 2 capture in water-stressed regions.

36 MATERIALS SCIENCE↗
DOE OSTI2024

Methods for Color Center Preserving Hydrogen‐Termination of Diamond

Abstract Chemical functionalization of diamond surfaces by hydrogen is an important method for controlling the charge state of near‐surface fluorescent color centers, an essential process in fabricating devices such as diamond field‐effect transistors and chemical sensors, and a required first step for realizing families of more complex terminations through subsequent chemical processing. In all these cases, termination is typically achieved using hydrogen plasma sources that can etch or damage the diamond, as well as deposited materials or embedded color centers. This work explores alternative methods for lower‐damage hydrogenation of diamond surfaces, specifically the annealing of diamond samples in high‐purity, non‐explosive mixtures of nitrogen and hydrogen gas, and the exposure of samples to microwave hydrogen plasmas in the absence of intentional stage heating. The effectiveness of these methods are characterized by x‐ray photoelectron spectroscopy (XPS), and comparison of the results to density‐functional modelling of the surface hydrogenation energetics implicates surface oxygen ligands as the primary factor limiting the termination quality of annealed samples. Finally, photoluminescence (PL) spectroscopy is used to verify that both the annealing and reduced sample temperature plasma methods are non‐destructive to near‐surface ensembles of nitrogen‐vacancy (NV) centers, in stark contrast to plasma treatments that use heated sample stages.

36 MATERIALS SCIENCE↗
DOE OSTI2021

Structural Analysis of the US ITER ECH Transmission Line System

The electron cyclotron heating (ECH) and current drive system is one of the main plasma heating systems for ITER. It uses high-power microwave beams with the power deposition location steerable across the plasma cross section. Microwave power is conveyed via transmission lines (TLs) that run from the gyrotrons in the radio frequency building through the assembly hall and tokamak building to the ECH launchers within the tokamak vacuum vessel. The ECH system includes a vast array of interconnected TL waveguides, in-line components, and support structures.Finite element (FE) modeling provides an essential means of simulating the system, applying loads and determining deflections, rotations, forces, moments, and stresses in order to evaluate various structural and microwave transmission performance metrics. A representative FE model of the overall ECH TL system is developed in ANSYS®. This top-level model defines the centerline of the waveguide system. Waveguide segments are represented by line elements (beams and pipes) with equivalent section properties, and support structures are represented by boundary conditions. A systematic approach is used to model each ECH component with lumped masses and structurally equivalent stiffness matrices or ANSYS superelements.The top-level TL FE model is used to evaluate the various loads (thermal, vacuum, seismic, etc.) and operating scenarios. The top-level model directly calculates stresses in the straight aluminum waveguide segments. The model provides the forces and moments acting on the in-line components for detailed submodel assessments. Displacement results from the top-level analysis feed into a separate microwave performance model to help determine operational efficiency. All TL performance and thermal-structural requirements are met, as specified by the applicable codes and standards, and successfully documented in numerous technical reports and demonstrated at the final design review.

Shanmugasundaram, Aravind↗
NASA NTRS1981

Tropical cyclone rainfall characteristics as determined from a satellite passive microwave radiometer

Data from the Nimbus 5 electrically scanning microwave radiometer (ESMR-5) were used to calculate latent heat release (LHR) and other rainfall parameters for over 70 satellite observations of 21 tropical cyclones during 1973, 1974, and 1975 in the tropical North Pacific Ocean. The results indicate that the ESMR-5 measurements can be useful in determining the rainfall characteristics of these storms and appear to be potentially useful in monitoring as well as predicting their intensity. The ESMR-5 derived total tropical cyclone rainfall estimates agree favorably with previous estimates for both the disturbance and typhoon stages. The mean typhoon rainfall rate (1.9 mm h/1) is approximately twice that of disturbances (1.1 mm h/1).

Rodgers, E. B.↗