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At least 343 records · Page 19

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DOE OSTI2022

Effects of Microbial-Mineral Interactions on Organic Carbon Stabilization in a Ponderosa Pine Root Zone: A Micro-Scale Approach

Soil microbial communities affect the formation of micro-scale mineral-associated organic matter (MAOM) where complex processes, including adhesion, aggregate formation, microbial mineral weathering and soil organic matter stabilization occur in a narrow zone of large biogeochemical gradients. Here we designed a field study to examine carbon stabilization mechanisms by using in-growth mesh bags containing biotite that were placed in a ponderosa pine root zone for 6 months and compared to the surrounding bulk soil. We sought to determine the composition of the microbial community in the mesh bags compared to the surrounding soils, analyze the direct interactions between microbes and biotite, and finally identify the nature of the newly formed MAOM within the mesh-bags. Our results revealed that minerals in the mesh bags were colonized by a microbial community that produced organic matter in situ. The 16S rRNA gene sequencing and ITS2 region characterization showed phylogenetic similarity between the mesh bag and bulk soil archaea/bacteria and fungi microbiomes, with significant differences in alpha- and beta-diversity and species abundances. Organic matter pools in the mesh bags, analyzed by Fourier transform ion cyclotron resonance mass spectrometry, contained protein- (peptides) and lipid-like compounds while the bulk soil OM was comprised of lignin-like and carboxyl-rich alicyclic molecules. These results support that the newly formed biotite associated organic compounds have a microbial signature in the mesh bags. High-resolution electron microscopy documented strongly adhered organic compounds to biotite surfaces, formation of microaggregates, elemental uptake at the microbe (organic matter)-mineral interface, and distortion of biotite layers. Overall, this study shows the direct and indirect involvement of soil microbial communities from the root zone of ponderosa pine in the formation of MAOM, soil organic carbon stabilization, microaggregation, and mineral weathering at micro- and nano-scales.

58 GEOSCIENCES↗

DOE OSTI2021

Ultra-Fast Laser Fabrication of Alumina Micro-Sample Array and High-Throughput Characterization of Microstructure and Hardness

In the light of recent advances in material informatics, there is a great demand for high-throughput approaches of sample fabrication and property characterization. Currently, no high-throughput approach has been demonstrated for the fast sampling of the microstructure and the correlated properties. In this paper, we demonstrate the ultra-fast fabrication of an alumina sample array and the high-throughput hardness characterization of these sample units. The alumina sample array was fabricated using picosecond (PS) laser micromachining and CO2 laser sintering within a short time (i.e., less than a few minutes). After laser sintering, the hardness of these sample units was characterized using micro-indentation, and the microstructure was observed using scanning electron microscopy (SEM). In each sample unit, the microstructure was uniform for the entire top surface and within about 20 µm depth from the top surface. The relative density (RD) and corresponding micro-hardness of the sample units was found to continuously vary over a wide range from 89% RD with 600 kgf/mm2 hardness to 99% RD with 1609 kgf/mm2 hardness. For these laser-sintered samples, the correlation of hardness and relative density of the alumina matched well with the literature reports on sintered alumina obtained using conventional low-throughput furnace sintering experiments.

36 MATERIALS SCIENCE↗

DOE OSTI2023

Milone eTape Liquid Level Sensor Laboratory Calibration with a Commercial 12.2 cm HS-Flume and 3D Printed 4 cm Micro-HS-Flumes

The NGEE Arctic Rainfall Simulator (NARS) is a variable intensity rainfall simulator (RFS) with a frame design based on the Humphry et al. (2002) RFS and a water delivery system based on the Walnut Gulch (Paige et al., 2004) RFS. The NARS uses an aluminum frame that is fully deconstructable for transportation to field locations and a water system that enables variable rain intensity. Prior to field deployment, H-flume discharge and the corresponding Milone eTape Liquid Level Sensor (eTape) resistance values were measured in the laboratory so that discharge measurements from the NGEE Arctic Rainfall Simulator could be automated. eTape resistance was measured with increasing fluid heights for the full range of the eTape to calculate sensor detection limits and resolution. The eTape was calibrated to both a commercially available 12.2 cm HS-flume and a 3D printed 4 cm Micro-HS-flume. This data package contains two .csv files, one for the eTape calibration and the other for the flume calibrations, and two .stl files to 3D print the 4 cm Micro-HS-Flume design with a 1 cm x 3.6 cm stilling well opening. The .stl files can be opened in most 3D printing or CAD programs/software. Two .kml files of the laboratory location and broader area where testing was conducted are also included in this data package.The Next-Generation Ecosystem Experiments: Arctic (NGEE Arctic), was a research effort to reduce uncertainty in Earth System Models by developing a predictive understanding of carbon-rich Arctic ecosystems and feedbacks to climate. NGEE Arctic was supported by the Department of Energy's Office of Biological and Environmental Research.The NGEE Arctic project had two field research sites: 1) located within the Arctic polygonal tundra coastal region on the Barrow Environmental Observatory (BEO) and the North Slope near Utqiagvik (Barrow), Alaska and 2) multiple areas on the discontinuous permafrost region of the Seward Peninsula north of Nome, Alaska.Through observations, experiments, and synthesis with existing datasets, NGEE Arctic provided an enhanced knowledge base for multi-scale modeling and contributed to improved process representation at global pan-Arctic scales within the Department of Energy's Earth system Model (the Energy Exascale Earth System Model, or E3SM), and specifically within the E3SM Land Model component (ELM).

54 ENVIRONMENTAL SCIENCES↗

NASA NTRS1973

Solar cosmic ray micro-events

To study small discrete solar particle events, it has proven useful to define a special class such that the proton flux at energies greater than 20 MeV exceed 0.0001 protons/sq cm-sec-sr-MeV. These increases are termed microevents. An arbitrary upper limit is placed at 2 X 0.02 protons/sq cm-sec-sr-MeV. By demanding a measurable flux above 20 MeV, a better separation from corotating events is achieved and onset times can in general be determined more precisely. Over an observing period extending from May 1967 through December 1971, approximately 105 events were observed. There are several different sources of these small events. Some are produced by moderate to large solar flares near the east limb or by solar flares on the nonvisible disk of the sun. Others are produced by generally minor solar activity: typically in 1N flare, a group of type 3 radio bursts and a well defined X-ray burst. A significant number of this latter type are accompanied by type 2 radio emission. A small sample of the micro-events can be classified as scatter-free events. For these the distance traveled by the particles before their initial detection at earth is on the order of 1.5 AU and observed rise and decay times are much less than normal. Examples of these general types of micro-events and their solar association are discussed.

Mcdonald, F. B.↗

NASA NTRS1974

Vapor growth of GeTe single crystals in micro-gravity

The positive effects of micro-gravity on crystal growth and fundamental properties of the vapor transport reaction were established by analyzing the results of GeSe and GeTe vapor transport experiments performed on board Skylab. The analysis was based on a direct comparison of GeSe and GeTe crystals and of mass transport rate data obtained on earth and in space. For this purpose, a total of six transport experiments employing different concentrations of transport agent (GeI4) and two temperature gradients were performed during the Skylab 3 and 4 missions. Extensive ground-based studies demonstrated that the crystal morphology and the mass transport rates of the above systems are affected by the transport conditions, in particular by gravity-driven convection. The results demonstrate unambiguously a considerable improvement of the space crystals in terms of surface perfection, crystalline homogeneity and defect density. The observation of greater mass transport rates than expected in micro-gravity environment is of basic scientific and technological significance. This indicates that conventional transport models are incomplete and demonstrates that crystals of improved quality can be grown at reasonable rates by this technique in space. Results are of practical importance for the modification of crystal growth techniques on earth.

Wiedemeier, H.↗

NASA NTRS1977

Surface micro-discharges on spacecraft dielectrics

Extensive measurements on Teflon and Kapton in a scanning electron microscope indicate the existence of a well-defined family of surface micro-discharges characteristic of the dielectric material. For a given small region exposed to the 16-20 kV electron beam, the strongest discharge pulses are similar in shape and amplitude. For Teflon, typical pulse durations are 2-3 ns, rise and fall times are sometimes as low as 0.2 ns, current amplitudes are approximately 100 mA flowing down to the pedestal and the pulses are unidirectional with no ringing. The use of a rapid-scan electron microscope with a secondary-electron imaging system reveals complex charge distributions resembling Lichtenberg figures on a supposedly flat homogeneous dielectric surface. These patterns undergo extensive alteration at each micro-discharge pulse and indicate that both the charging and discharging processes are highly nonuniform over the dielectric surface. The use of floodbeam causes the occurrence of a large-scale macro-discharges, in which a typical peak current is 40 A with a duration of 120 ns.

Balmain, K. G.↗

NASA NTRS1980

Rectenna session: Micro aspects

Two micro aspects of the rectenna design are addressed: evaluation of the degradation in net rectenna RF to DC conversion efficiency due to power density variations across the rectenna (power combining analysis) and design of Yagi-Uda receiving elements to reduce rectenna cost by decreasing the number of conversion circuits (directional receiving elements). The first of these micro aspects involves resolving a fundamental question of efficiency potential with a rectenna, while the second involves a design modification with a large potential cost saving.

Gutmann, R. J.↗

NASA NTRS1985

Micro-Raman spectroscopy: The analysis of micrometer and submicrometer atmospheric aerosols

A nondestructive method of molecular analysis which is required to fully utilize the information contained within a collected particle is discussed. Upper atmosphere reaction mechanisms are assessed when the chemical compounds, the use of micro-Raman spectrometric techniques to perform micron and submicron particle analysis was evaluated. The results are favorable and it is concluded that micron and submicron particles can be analyzed by the micron-Raman approach. Completely automatic analysis should be possible to 0.3 micro m. No problems are anticipated with photo or thermal decomposition. Sample and impurity fluorescence are the key source of background as they cannot be completely eliminated.

Klainer, S. M.↗

NASA NTRS1986

A three-mass tethered system for micro-g/variable-g applications

This paper describes a Space-Station attached tethered system for micro-g/variable-g applications. The system consists of three platforms: the Space Station, an end mass anchored at the end of a 10 km long kevlar tether and a micro-g/variable-g laboratory with the capability of crawling along the tether. Control strategies are devised for performing both the deployment and the station-keeping maneuvers of the system. Effective algorithms are identified for damping out the major vibrational modes.

Lorenzini, E. C.↗

NASA NTRS1987

Structural/control interaction (payload pointing and micro-g)

A 203rd order simulation model was developed to evaluate the space station customer accommodation payload pointing and micro-g requirements. The simulation shows the pointing errors on the telescope are significantly smaller than at the base of the telescope. The pointing results could change when the parametric studies are performed. The results show the micro-g requirement is met with an active isolation system.

Larson, C. R.↗

NASA NTRS1988

Steady state micro-g environment on Space Station

In circular earth orbit, the Space Station (SS) will sense acceleration from external environmental forces due to the gravitational gradient, rotational accelerations, and atmospheric drag. This paper discusses these forces and how they will affect the SS micro-g environment. The effect of SS attitude on the micro-g profile is addressed. Sources for nonsteady state acceleration levels for which disturbance models are currently being developed are briefly considered.

Waters, L.↗

NASA NTRS1988

Measurement of micro-roughness and effects of detector bandwidth and finite width

Surface micro-roughness of grazing incidence optics has long been recognized as a critical parameter in the control of the scattered X-ray intensity and its effects on the point spread function half-energy width. Accurate knowledge of the amplitude of surface micro-roughness is vital to assess optic predicted performance during the final stages of fabrication. This requires not only a knowledge of the spatial bandwidth over which surface features must be measured, but also knowledge of the bandwidth of the measurement instrument. We show that the standard assumption that instruments respond up to their Nyquist limit is an oversimplification which neglects the finite detector size and its bandwidth limiting effects when sampling a real (i.e., two-dimensional) surface.

Reid, P. B.↗

NASA NTRS1988

Redundant manipulators for momentum compensation in a micro-gravity environment

This paper is concerned with the implementation and assessment of joint motion management strategies for kinematically redundant robotic manipulators operating in the micro-gravity environment of Space Station. These robots must be capable of conducting experiments and manufacturing processes without disturbing the micro-gravity environment through base reactions/motions. The redundant degrees of freedom of the manipulator permit the inverse kinematic problem to be solved simultaneously with the minimization of a cost function. The cost function in this case is the weighted sum of the squares of the base forces and moments and is minimized over discrete time segments. The Generalized Inverse Method and Rayleigh Ritz technique are used to solve the combined optimization/inverse kinematics problem. Numerical examples include various robotic configurations and degrees of manipulator redundancy.

Quinn, R. D.↗

NASA NTRS1988

Robots for manipulation in a micro-gravity environment

This paper is concerned with the development of control strategies and mechanisms for robots operating in the micro-gravity environment of Space Station. These robots must be capable of conducting experiments and manufacturing processes without disturbing the micro-gravity environment through base reactions/motions. Approaches discussed for controlling the robot base reactions/motions include strategies making use of manipulators with redundant degrees of freedon, actuators at the robot base, and a redundant (balancing) arm. Two degree-of-freedom, traction-drive joints are discussed as well as the conceptual design for a traction-driven manipulator.

Quinn, R. D.↗

NASA NTRS1988

Acceleration levels on board the Space Station and a tethered elevator for micro and variable-gravity applications

This paper investigates the dynamics and acceleration levels of a new tethered system for micro and variable-gravity applications. The system consists of two platforms tethered on opposite sides to the Space Station. A fourth platform, the elevator, is placed in between the Space Station and the upper platform. Variable-g levels on board the elevator are obtained by moving this facility along the upper tether, while micro-g experiments are carried out on board the Space Station. By controlling the length of the lower tether the position of the system CM can be maintained on board the Space Station despite variations of the station's distribution of mass. The paper illustrates the mathematical model, the environmental perturbations and the control techniques which have been adopted for the simulation and control of the system dynamics. Two sets of results from two different simulation runs are shown. The first set shows the system dynamics and the acceleration spectra on board the Space Station and the elevator during station-keeping. The second set of results demonstrates the capability of the elevator to attain a preselected g-level.

Lorenzini, E. C.↗

NASA NTRS1990

High-performance fault-tolerant VLSI systems using micro rollback

A technique called micro rollback, which allows most of the performance penalty for concurrent error detection to be eliminated, is presented. Detection is performed in parallel with the transmission of information between modules, thus removing the delay for detection from the critical path. Erroneous information may thus reach its destination module several clock cycles before an error indication. Operations performed on this erroneous information are undone using a hardware mechanism for fast rollback of a few cycles. The implementation of a VLSI processor capable of micro rollback is discussed, as well as several critical issues related to its use in a complete system.

Tamir, Yuval↗

NASA NTRS1990

The development of physically based micro-mechanics - Based on the characteristic tip field of dislocation pileup

Based on the analytical solution by Eshelby et al. (1951) and the numerical calculations by Chou and Li (1969) and Armstrong et al. (1962), it is shown that the force, F, on the locked leading dislocation of a discrete dislocation pileup is capable of characterizing uniquely the stress, strain, and displacement field at the tip of the pileup, including the positions of the discrete mobile dislocations next to the leading dislocation. Conversely, the positions of the mobile dislocations can be used to measure F. The F thus measured can be used to study micro-plastic deformation and micro-fractures at grain boundaries or any other dislocation barriers.

Gao, Q.↗

NASA NTRS1992

Rotary Apparatus Concentrates And Separates Micro-Organisms

Apparatus concentrates and separates swimming micro-organisms of different species into concentric rings in fluid. Fluid containing high concentration of desired species removed by use of small scoop placed into fluid at radius of one of rings formed by that species. Micro-organisms concentrated into concentric rings by combined dynamic effects of upward and horizontal components of swimming, rotation of dish, gravitation, and viscosity.

Noever, David A.↗