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At least 343 records · Page 19

Using an Absolute Cavity Pyrgeometer to Validate the Calibration of a Transfer Standard Pyrgeometer Outdoors, Independent from the Reference Value of the Atmospheric Longwave Irradiance

A unique method of pyrgeometer calibration has been developed to improve the measurement uncertainty [1]. The results of this method yielded irradiance values within ±3 W/m2 of those traceable to the World InfraRed Standard Group (WISG). The ACPs and pyrgeometer model PIR were deployed outdoors, and the irradiance measured by the PIR was compared against the irradiance measured by ACP95F3. Based on the results it is possible to achieve an uncertainty of ± 3.51 W/m2. These results suggest that the PIR calibration method might be useful in addressing the international need for a secondary standard pyrgeometer traceable to SI.

absolute cavity pyrgeometer↗

SeaWiFS Postlaunch Technical Report Series: The Fifth Sea-WiFS Intercalibration Round-Robin Experiment (SIRREX-5), July 1996 - Volume 7

This report documents the fifth Sea-viewing Wide Field-of-view Sensor (SeaWiFS) Intercalibration Round-Robin Experiment (SIRREX-5), which was held at the National Institute of Standards and Technology (NIST) on 23-30 July 1996. The agenda for SIRREX-5 was established based on recommendations made during SIRREX-4. For the first time in a SIRREX activity, instrument intercomparisons were performed at field sites, which were near NIST. The goals of SIRREX-5 were to continue the emphasis on training and the implementation of standard measurement practices, investigate the calibration methods and measurement chains in use by the oceanographic community, provide opportunities for discussion, and intercompare selected instruments. As at SIRREX-4, the day was divided between morning lectures and afternoon laboratory exercises. A set of core laboratory sessions were performed: 1) in-water radiant flux measurements; 2) in-air radiant flux measurements; 3) spectral radiance responsivity measurements using the plaque method; 4) device calibration or stability monitoring with portable field sources; and 5) various ancillary exercises designed to illustrate radiometric concepts. Before, during, and after SIRREX-5, NIST calibrated the SIRREX-5 participating radiometers for radiance and irradiance responsivity. The Facility for Automated Spectroradiometric Calibrations (FASCAL) was scheduled for spectral irradiance calibrations for standard lamps during SIRREX-5. Three lamps from the SeaWiFS community were submitted and two were calibrated.

Hooker, Stanford B.↗

Tables for calibrating altimeters and computing altitudes based on the standard atmosphere

During 1925 the assumption of an isothermal atmosphere which was in general use as the standard for the calibration of altimeters in the United States was replaced by a standard atmosphere which assumes an altitude-temperature relation closely corresponding to the average of upper air observations at latitude 40 degrees in this country. The same standard atmosphere had already been adopted somewhat earlier in the United States as the aircraft performance standard. National Advisory Committee for Aeronautics Technical Reports nos. 147 and 218 give necessary constants, tables, and information. However, neither of these reports includes all of the tables required for the computation of actual altitudes nor those readily suitable for use in calibrating altimeters, since the altitude intervals for which data are given are not sufficiently small. The present report has been prepared specifically for these purposes. The formulas which define the standard atmosphere are given in this report, together with other formulas giving the corrections to be applied to the standard altitude in order to obtain the actual altitude when the necessary observations of pressure and temperature are available. The tables necessary for the use of this standard atmosphere in calibrating altimeters and in computing altitudes form the principal part of this report. An example of the computation of actual altitudes from observed pressures and temperatures are given in table IV.

Brombacher, W G↗

Calibration source maintenance, characterization and development

The Standards and Calibration Office maintains visible and near infrared calibration sources for the use of various GSFC organizations instrument calibration needs and related field activities. These are large aperture spherical and hemispherical integrating sources designed to provide a spatially uniform absolute spectral radiance with a well-defined angular uniformity characteristic. In essence, the calibration and characterization efforts involve monitoring and documenting the stability and the absolute radiance of these calibration sources. These sources are recalibrated on a regular basis to both document any changes that might occur in the output of the sources and to provide the most up-to-date calibration data for the source users. Efforts included comparing the calibration numbers with those of a commercial calibration laboratory that was engaged to do independent calibrations. However, the most recent calibrations done by the independent laboratory and those done by GSFC personnel show a rather large discrepancy (10 to 15 percent). Efforts are underway to resolve these differences.

Mclean, J. T.↗

Using an Absolute Cavity Pyrgeometer to Validate the Calibration of a Secondary Standard Pyrgeometer Outdoors, Independent from the Reference Value of the Atmospheric Longwave Irradiance

Accurate measurements of broadband outdoor longwave irradiance are important for renewable energy applications and the study of the atmosphere and climate change. A unique method of pyrgeometer calibration has been developed to improve the measurement uncertainty [1]. The results of this method yielded irradiance values within ±3 W/m 2 of those traceable to the World InfraRed Standard Group (WISG). This article describes a technique for validating this pyrgeometer calibration method using two Absolute Cavity Pyrgeometers (ACPs). The ACPs and pyrgeometer model PIR were deployed outdoors and the irradiance measured by the PIR was compared against the average irradiance measured by the two ACPs. The irradiance measured by the PIR was calculated using two equations, NREL equation and the Physikalisch Meteorologisches Observatorium Davos (PMOD) equation. The uncertainty with 95% confidence level ( U 95 ) of the irradiance measured by the PIR using NREL equation equaled ±3.51 W/m 2 with respect to SI and using PMOD equation U 95 equaled ±2.99 W/m 2 with respect to SI. These results suggest that the PIR calibration method might be useful in addressing the international need for a secondary standard pyrgeometer traceable to SI.

54 ENVIRONMENTAL SCIENCES↗

On Calibrations Using the Crab Nebula as a Standard Candle

Inspired by a recent paper (Kirsch et al. 2005) on possible use of the Crab Nebula as a standard candle for calibrating X-ray response func tions, we examine possible consequences of intrinsic departures from a single (absorbed) power law upon such calibrations. We limited our analyses to three more modern X-ray instruments -- the ROSAT/PSPC, th e RXTE/PCA, and the XMM-Newton/EPIC-pn. The results are unexpected an d indicate a need to refine two of the three response functions studi ed. The implications for Chandra will be discussed.

Weisskopf, Martin↗

Apollo experience report: Flight instrumentation calibration

Three types of instrumentation-calibration data were used in the Apollo Program to provide the correct engineering data for tests and mission support. The command and service module instrumentation-component procurement specifications required individual-component calibration, and calibration data for these individual components (conventional-calibration data) were always used for mission data support. A mean standard type of calibration data derived from a statistical sampling of conventional-calibration data was used for test and checkout during the latter part of the Apollo Program. The lunar module instrumentation procurement specification permitted the use of standard-calibration data. These data were applicable to similarly instrumented measurements. The definition, merit, and application of each type of data are discussed.

Demoss, J. F.↗

Evaluating Statistical Process Control (SPC) techniques and computing the uncertainty of force calibrations

In recent years there has been a push within NASA to use statistical techniques to improve the quality of production. Two areas where statistics are used are in establishing product and process quality control of flight hardware and in evaluating the uncertainty of calibration of instruments. The Flight Systems Quality Engineering branch is responsible for developing and assuring the quality of all flight hardware; the statistical process control methods employed are reviewed and evaluated. The Measurement Standards and Calibration Laboratory performs the calibration of all instruments used on-site at JSC as well as those used by all off-site contractors. These calibrations must be performed in such a way as to be traceable to national standards maintained by the National Institute of Standards and Technology, and they must meet a four-to-one ratio of the instrument specifications to calibrating standard uncertainty. In some instances this ratio is not met, and in these cases it is desirable to compute the exact uncertainty of the calibration and determine ways of reducing it. A particular example where this problem is encountered is with a machine which does automatic calibrations of force. The process of force calibration using the United Force Machine is described in detail. The sources of error are identified and quantified when possible. Suggestions for improvement are made.

Navard, Sharon E.↗

Standardization work for the calibration of intensities of celestial objects

Observations of celestial phenomena need to be calibrated, to be related, to some measurable quantity. There continues to be a long-term need for accurate photometric standard stars, those with known intensities and colors, so that brightness and color measurements made of various celestial phenomena by different observers can be integrated and compared with one another. Toward this end, the author has been emphasizing data collection in recent years for stars of 'intermediate' brightness, those approximately in the magnitude range 11.5 is less than V is less than 16.0. Photoelectric data were obtained at the Cerro Tololo InterAmerican Observatory's (CTIO) telescopes for stars in certain selected areas near the celestial equator. Stars of extreme color outside the selected areas, but near the equator, also were selected to provide a more broad and complete range in color index. It was proposed to complete the photoelectric phase of the program. The author proposed developing extremely faint sequences of photometric standard stars useful for both large space-based detectors and for land-based detectors. These data were to be collected via charge-coupled devices (CCD's) at telescopes located at CTIO and at the Las Campanas Observatory (LCO), both observatories being located in Chile. It was hoped that accurate data could be collected down to the 21st or 22nd magnitude.

Landolt, Arlo U.↗

Multipurpose Spectroradiometer for Satellite Instrument Calibration and Zenith Sky Remote Sensing Measurements

In the early 1990s a series of surface-based direct sun and zenith sky measurements of total column ozone were made with SBUV/2 flight models and the SSBUV Space Shuttle instrument in Boulder, Colorado which were compared with NOAA Dobson Instrument direct sun observations and TOMS instrument overpass observations of column ozone. These early measurements led to the investigation of the accuracy of derived total column ozone amounts and aerosol optical depths from zenith sky observations. Following the development and availability of radiometrically stable IAD narrow band interference filter and nitrided silicon photodiodes a simple compact multifilter spectroradiometer was developed which can be used as a calibration transfer standard spectroradiometer (CTSS) or as a surface based instrument remote sensing instruments for measurements of total column ozone and aerosol optical depths. The total column ozone derived from zenith sky observations agrees with Dobson direct sun AD double wavelength pair measurements and with TOMS overpass ozone amounts within uncertainties of about 1%. When used as a calibration transfer standard spectroradiometer the multifilter spectroradiometer appears to be capable of establishing instrument radiometric calibration uncertainties of the order of 1% or less relative to national standards laboratory radiometric standards.

Heath, Donald F.↗

Comparison of Analytical Methods for the Determination of Uranium in Seawater Using Inductively Coupled Plasma Mass Spectrometry

Trace element determinations in seawater by inductively coupled plasma mass spectrometry are analytically challenging due to the typically very low concentrations of the trace elements and the potential interference of the salt matrix. In this study, we did a comparison for uranium analysis using inductively coupled plasma mass spectrometry (ICP-MS) of Sequim Bay seawater samples and three seawater certified reference materials (SLEW-3, CASS-5 and NASS-6) using seven different analytical approaches. The methods evaluated include: direct analysis, Fe/Pd reductive precipitation, standard addition calibration, online automated dilution using an external calibration with and without matrix matching, and online automated pre-concentration. The method which produced the most accurate results was the method of standard addition calibration, recovering uranium from a Sequim Bay seawater sample at 101 ± 1.2%. The on-line preconcentration method and the automated dilution with matrix-matched calibration method also performed well. The two least effective methods were the direct analysis and the Fe/Pd reductive precipitation using sodium borohydride

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Solar cell measurements

The measurement of the electrical performance characteristics of individual solar cells is discussed. One of the reasons is determination of the output power, measurement of the effect of various degradation mechanisms, and separation of cells by current and voltage for eventual use in series and parallel combinations. Major problem areas in making accurate performance measurements are the determination of the irradiance level during measurement, the measurement and control of cell junction temperature, and the contacting of the separate current and potential leads to the cell under test. Solar cells respond to only part of the solar spectrum, irradiance measurement made with blackbody detectors lead to spectral mismatch errors. The use of reference cells with a spectral response similar to that of the test cell reduces this error. Reference cells are calibrated at standard atmospheric conditions with all cells calibrated at the same conditions.

Curtis, H. B.↗

Binary pseudo-random array standard for extreme ultraviolet lithography tool characterization

Extreme ultraviolet (EUV) imaging tools play a crucial role in EUV lithography. Achieving high accuracy in EUV metrology is essential for advanced semiconductor manufacturing. A thorough characterization of the instrumentation in use is required. Binary pseudo-random arrays (BPRAs) are an established standard for calibrating and characterizing optical instruments in the frequency domain. Here, we expand the BPRA standard to applications in EUV imaging. To extend the technology to the EUV spectral range, a high-resolution BPRA target with the smallest feature size of 40 nm is developed. The EUV BPRA target establishes an in situ and portable calibration and alignment standard for EUV imaging. The target is patterned by means of electron-beam lithography, using a nickel absorber with a thickness of 39 nm. The substrate is a 4″ silicon wafer with a molybdenum/silicon multilayer coating. To demonstrate the efficacy of the target and develop the instrument calibration protocol, the target is imaged on the Sharp Hyper-NA Actinic Reticle Review Project EUV mask microscope. Power spectral density (PSD) data are presented. The characteristics of the imaging system are imprinted on the PSD. The modulation transfer function is extracted from the PSD data. A partially coherent imaging model is used as a reference to the experimental results.

BPRA↗

Absolute flux calibration of optical spectrophotometric standard stars

A method based on Landolt photometry in B and V is developed to correct for a wavelength independent offset of the absolute flux level of optical spectrophotometric standards. The method is based on synthetic photometry techniques in B and V and is accurate to approximately 1%. The correction method is verified by Hubble Space Telescope Faint Object Spectrograph absolute fluxes for five calibration stars, which agree with Landolt photometry to 0.5% in B and V.

Colina, Luis↗

STANDARD STARS AND EMPIRICAL CALIBRATIONS FOR Hα AND Hβ PHOTOMETRY

We define an Hα photometric system that is designed as a companion to the well established Hβ index. The new system is built on spectrophotometric observations of field stars as well as stars in benchmark open clusters. We present data for 75 field stars, 12 stars from the Coma star cluster, 24 stars from the Hyades, 17 stars from the Pleiades, and 8 stars from NGC 752 to be used as primary standard stars in the new systems. We show that the system transformations are relatively insensitive to the shape of the filter functions. We make comparisons of the Hα index to the Hβ index and illustrate the relationship between the two systems. In addition, we present relations that relate both hydrogen indices to equivalent width and effective temperature. We derive equations to calibrate both systems for Main Sequence stars with spectral types in the range O9 to K2 for equivalent width and A2 to K2 for effective temperature.

79 ASTRONOMY AND ASTROPHYSICS↗

A round-robin gamma stereotactic radiosurgery dosimetry interinstitution comparison of calibration protocols

Purpose: Absorbed dose calibration for gamma stereotactic radiosurgery is challenging due to the unique geometric conditions, dosimetry characteristics, and nonstandard field size of these devices. Members of the American Association of Physicists in Medicine (AAPM) Task Group 178 on Gamma Stereotactic Radiosurgery Dosimetry and Quality Assurance have participated in a round-robin exchange of calibrated measurement instrumentation and phantoms exploring two approved and two proposed calibration protocols or formalisms on ten gamma radiosurgery units. The objectives of this study were to benchmark and compare new formalisms to existing calibration methods, while maintaining traceability to U.S. primary dosimetry calibration laboratory standards. Methods: Nine institutions made measurements using ten gamma stereotactic radiosurgery units in three different 160 mm diameter spherical phantoms [acrylonitrile butadiene styrene (ABS) plastic, Solid Water, and liquid water] and in air using a positioning jig. Two calibrated miniature ionization chambers and one calibrated electrometer were circulated for all measurements. Reference dose-rates at the phantom center were determined using the well-established AAPM TG-21 or TG-51 dose calibration protocols and using two proposed dose calibration protocols/formalisms: an in-air protocol and a formalism proposed by the International Atomic Energy Agency (IAEA) working group for small and nonstandard radiation fields. Each institution’s results were normalized to the dose-rate determined at that institution using the TG-21 protocol in the ABS phantom. Results: Percentages of dose-rates within 1.5% of the reference dose-rate (TG-21 + ABS phantom) for the eight chamber-protocol-phantom combinations were the following: 88% for TG-21, 70% for TG-51, 93% for the new IAEA nonstandard-field formalism, and 65% for the new in-air protocol. Averages and standard deviations for dose-rates over all measurements relative to the TG-21 + ABS dose-rate were 0.999 ± 0.009 (TG-21), 0.991 ± 0.013 (TG-51), 1.000 ± 0.009 (IAEA), and 1.009 ± 0.012 (in-air). There were no statistically significant differences (i.e., p > 0.05) between the two ionization chambers for the TG-21 protocol applied to all dosimetry phantoms. The mean results using the TG-51 protocol were notably lower than those for the other dosimetry protocols, with a standard deviation 2–3 times larger. The in-air protocol was not statistically different from TG-21 for the A16 chamber in the liquid water or ABS phantoms (p = 0.300 and p = 0.135) but was statistically different from TG-21 for the PTW chamber in all phantoms (p = 0.006 for Solid Water, 0.014 for liquid water, and 0.020 for ABS). Results of IAEA formalism were statistically different from TG-21 results only for the combination of the A16 chamber with the liquid water phantom (p = 0.017). In the latter case, dose-rates measured with the two protocols differed by only 0.4%. For other phantom-ionization-chamber combinations, the new IAEA formalism was not statistically different from TG-21. Conclusions: Although further investigation is needed to validate the new protocols for other ionization chambers, these results can serve as a reference to quantitatively compare different calibration protocols and ionization chambers if a particular method is chosen by a professional society to serve as a standardized calibration protocol.

07 ISOTOPE AND RADIATION SOURCES↗

Atmospheric analysis for airdata calibration on research aircraft

In-flight airdata calibrations are used to determine the aerodynamic influence of an airplane on pitot-static pressure measurements of altitude and speed. Conventional flight-test calibration techniques are briefly reviewed and meteorological analysis methods for estimating calibration reference values of atmospheric conditions are described. There are cases where some conventional in-flight techniques are not entirely satisfactory for research aircraft because of added equipment requirements or flight envelope and location limitations. In these cases, atmospheric wind and pressure information can be used to complement conventional techniques. Accuracy of the atmospheric measurements and the variability of upper-air winds and pressure values are discussed. Results from several flight research aircraft show that wind reference calibration is generally less accurate than calibration accuracy standards for civil and research aircraft. Examples of pressure reference altimetry derived from meteorological analyses are also presented for a variety of flight research programs. These flight data show that the reference pressure accuracy provided by meteorological analyses is usually within civil aircraft and flight research airdata calibration accuracy standards. Meteorological analyses altimetry is particularly useful when it is not feasible to restrict the test airplane altitude, location, or maneuver envelope.

Ehernberger, L. J.↗