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At least 343 records · Page 19

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NASA NTRS2024

Reversionary Control Modes for the Mitigation of Failures in a Partially Turboelectric Aircraft Propulsion System

In support of emission and fuel burn reduction goals, the aviation industry is actively pursuing the advancement of electrified aircraft propulsion (EAP) technology. This includes turboelectric and hybrid electric propulsion designs that combine gas turbine engine and electrical system hardware. Such architectures exhibit a high degree of coupling between subsystems. This drives the need for system-level control strategies to ensure the safe, coordinated, and efficient operation of all subsystems. The design and certification of any aircraft propulsion system requires that all potential subsystem failures are identified, and the hazards posed by these failures are appropriately mitigated. This requirement is particularly challenging for EAP systems due to their integrated nature. One approach to assist in EAP failure mitigation is the inclusion of automated reconfiguration capabilities within the propulsion control system. Such control modes, referred to as reversionary control modes, are designed to automatically detect failures and activate backup control modes upon failure detection. This paper covers the design and evaluation of reversionary control mode logic developed for a partially turboelectric propulsion concept. Test results from a real-time hardware-in-the-loop evaluation of the concept are also presented and discussed. The results show that the developed reversionary control logic can successfully detect and mitigate subsystem failures in a representative environment that includes actual electrical system hardware.

Electrified Aircraft Propulsion↗

DOE OSTI2022

Improving Unit Flexibility Utilizing Plasma Ignitors

Coal fired steam generation operators face increasing market challenges, including competition from low cost generation, renewables, and regulatory pressure. These market conditions are forcing utilities to operate their coal assets in a more flexible mode, including more frequent starts and stops, faster ramp rates, frequent cycling, and extended operation at the lowest possible loads. Without upgrades to firing and control systems, pressure parts, and auxiliary systems, CAPEX and OPEX costs will increase significantly. Typically, expensive support fuels (Oil or Gas) are required to maintain safe, stable coal ignition when operating below 25% to 35% MCR (Maximum Continuous Rating). The exact minimum load without support fuel differs depending upon unit design specifications and fuel being burned. Frequent starts also increase the use of support fuels. The firing and burner control systems must be designed to allow for proper operation over the unit’s load range, ensuring that all mechanical components operate properly, and proper control of air and fuel streams can be maintained. To address the need for frequent starts and the need for stable low load operation on coal fired steam generators, this paper discusses options available, including, Firing Systems upgrades, Digital solutions, and pressure part upgrades. Several case studies are included that highlight options available allowing units to stay in operation and reduce CAPEX and OPEX costs.

01 COAL, LIGNITE, AND PEAT↗

NASA NTRS1984

Transportable Pumps Could Save Oil Cargoes

Transportable pumps designed for firefighting used to salvage crude oil from tankships leaking, burning, or grounded. Pump incorporated into self-contained transportable module along with engine and controls. Module carried by helicopter, boat, or van to site of fire provides large quantities of water at high pressure in firefighting mode or pump oil into barge in salvage mode.

Burns, R.↗

DOE OSTI2023

Implementation of AI/DEEP learning disruption predictor into a plasma control system

Abstract This paper reports on advances in the state‐of‐the‐art deep learning disruption prediction models based on the Fusion Recurrent Neural Network (FRNN) originally introduced in a 2019 NATURE publication [ https://doi.org/10.1038/s41586‐019‐1116‐4 ]. In particular, the predictor now features not only the “disruption score,” as an indicator of the probability of an imminent disruption, but also a “sensitivity score” in real time to indicate the underlying reasons for the imminent disruption. This adds valuable physics interpretability for the deep learning model and can provide helpful guidance for control actuators now implemented into a modern plasma control system (PCS). The advance is a significant step forward in moving from modern deep learning disruption prediction to real‐time control and brings novel AI‐enabled capabilities relevant for application to the future burning plasma ITER system. Our analyses use large amounts of data from JET and DIII‐D vetted in the earlier NATURE publication. In addition to “when” a shot is predicted to disrupt, this paper addresses reasons “why” by carrying out sensitivity studies. FRNN is accordingly extended to use more channels of information, including measured DIII‐D signals such as (i) the “n1rms” signal that is correlated with the n = 1 modes with finite frequency, including neoclassical tearing mode and sawtooth dynamics; (ii) the bolometer data indicative of plasma impurity control; and (iii) “q‐min”—the minimum value of the safety factor relevant to the key physics of kink modes. The additional channels and interpretability features expand the ability of the deep learning FRNN software to provide information about disruption subcategories as well as more precise and direct guidance for the actuators in a PCS.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

NASA NTRS1998

Buoyancy and Pressure Effects on Bulk Metal-Oxygen Reactions

The combustion behavior of metal-oxygen reactions if a weakly buoyant environment is studied to understand the rate-controlling mechanisms in the homogeneous and heterogeneous combustion of bulk metals. Cylindrical titanium and magnesium specimens are ignited in pure-oxygen at pressures ranging from 0.1 to 4.0 atm. Reduced gravity is obtained from an aircraft flying parabolic trajectories. A weakly buoyant environment is generated at low pressures under normal gravity and also at 1 atm under reduced gravity (0.01g). The similarity between these two experimental conditions comes from the p(exp 2)g buoyancy scale extracted from the Grashof number. Lower propagation rates of the molten interface on titanium samples are found at progressively lower pressures at 1 g. These rates are compared to theoretical results from heat conduction analyses with a diffusion/convection controlled reaction. The close agreement found between experimental and theoretical values indicate the importance values indicate the importance of natural convection enhanced oxygen transport on combustion rates. For magnesium, progressively longer burning times are experienced at lower pressures and 1 g. Under reduced gravity conditions at 1 atm, a burning time twice as long as in 1 g is exhibited. However, in this case, the validity of the p(exp 2)g buoyancy scale remains untested due to the inability to obtain steady gas-phase burning of the magnesium sample at 0.1 atm. Nevertheless, longer burning times and larger flame standoff distance at low pressures and at low gravity points to a diffusion/convection controlled reaction.

Abbud-Madrid, A.↗

NASA NTRS1987

The use of electrical discharge for ignition and control of combustion of solid propellants

As the first step of the study of the combustion control of solid propellants by electrical discharges, the effects of an arc discharge, which flows along the burning surface, on the burning rate and on the increase of enthalpy of the combustion product were investigated. For specially devised composite propellants, which are composed of Al and Teflon powders, it was shown that the combination can be controlled by an arc discharge; the combustion continues when the arc discharge is applied and is interrupted when the arc discharge breaks. In the present investigation, it was also shown that an arc discharge coupled with a high-frequency electrical discharge has potential as an effective ignition method for solid propellants. For the application of this type of combustion control to an ignitor for a solid propellant rocket motor or to a control rocket motor, this method lacks flexibility in the configuration scale and needs relatively high electric power at the present stage.

Tachibana, Takeshi↗

NASA NTRS2012

Peak Seeking Control for Reduced Fuel Consumption with Preliminary Flight Test Results

The Environmentally Responsible Aviation project seeks to accomplish the simultaneous reduction of fuel burn, noise, and emissions. A project at NASA Dryden Flight Research Center is contributing to ERAs goals by exploring the practical application of real-time trim configuration optimization for enhanced performance and reduced fuel consumption. This peak-seeking control approach is based on Newton-Raphson algorithm using a time-varying Kalman filter to estimate the gradient of the performance function. In real-time operation, deflection of symmetric ailerons, trailing-edge flaps, and leading-edge flaps of a modified F-18 are directly optimized, and the horizontal stabilators and angle of attack are indirectly optimized. Preliminary results from three research flights are presented herein. The optimization system found a trim configuration that required approximately 3.5% less fuel flow than the baseline trim at the given flight condition. The algorithm consistently rediscovered the solution from several initial conditions. These preliminary results show the algorithm has good performance and is expected to show similar results at other flight conditions and aircraft configurations.

Brown, Nelson↗

DOE OSTI2024

Investigation of Ammonia Carrier Materials for Next Generation Ammonia Dosing System - CRADA 334 (Abstract)

Lean-burn gasoline and diesel engines can offer substantially higher fuel efficiency, good driving performance, and reduced carbon dioxide emission compared to stoichiometric gasoline engines. Various catalyst technologies have been developed to remove the pollutants from these engines. For example, a three-way catalyst (TWC) is used to remove hydrocarbons (HC), carbon monoxide (CO), and nitrogen oxides (NOx) from gasoline engines during the stoichiometric conditions. During the lean-burn conditions, a TWC or a diesel oxidation catalyst (DOC) is used to control HC and CO emissions. NOx is removed by either lean NOx trap catalyst (LNT) that can store NOx under lean conditions and reduce NOx under rich conditions, or selective catalytic reduction catalyst (SCR) that can selectively remove NOx with a reducing agent. Among the NOx reduction catalyst technologies, SCR offers a number of advantages, including excellent NOx reduction efficiency over a wide range of temperatures and overall lower system cost. In fact, the SCR technology using ammonia (NH3) as reductant has been proven effective and used commercially for the removal of NOx emissions from stationary sources since the 1970s. Currently, SCR is being used to meet the NOx emission standards for diesel engines in Europe and North America, and also being considered for meeting the future NOx emission standards for lean-burn gasoline engines. Because of the challenges associated with storage, handling and transportation of ammonia on a vehicle, aqueous urea solution (e.g., Diesel Exhaust Fluid, AdBlue) has been developed as ammonia storage compound for mobile applications. When the aqueous urea solution is sprayed into exhaust gas stream, urea is decomposed to release ammonia, which then reduces NOx over the downstream SCR catalyst. Although aqueous urea solution technology has enabled automakers and engine manufacturers to meet the current NOx emission standards, this process of releasing ammonia requires a hot exhaust gas and sufficient mixing, creating challenges for low temperature NOx emission control and aftertreatment system packaging. For these reasons, alternative technologies have been developed as ammonia sources (e.g., solid urea, ammonium carbamate, metal ammine chloride) during the past few years. These technologies promise more convenient handling and distribution of ammonia sources, and help maximize the low-temperature performance of SCR catalysts and reduce the overall system volume and weight. However, none of these alternative technologies can be successfully implemented without the industry consensus. Therefore, the USCAR SCR work group, which is comprised of representatives from GM, Ford, and Chrysler, has decided to investigate the potential alternative ammonia carriers, define common standard vehicle interfaces, and address personal and environmental safety concerns with part suppliers and chemical companies. Under this CRADA Project, USCAR and Battelle will investigate alternative ammonia carrier materials that are currently under development. Based on the data and information derived under the CRADA project, the USCAR SCR work group plans to build the consensus and make recommendations for the industry.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗

DOE OSTI2024

Investigation of Ammonia Carrier Materials for Next Generation Ammonia Dosing System - CRADA 334 (Abstract)

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗

NASA NTRS2010

The Successful Implementation of NASA Orbital Debris Requirements for the Retirement of TDRS-1

TDRS-1 was decommissioned on October 28th 2009 following more than 26 years of operation. The Grand Old Dame of the TDRSS constellation wa s launched aboard the maiden voyage of the Space Shuttle Challenger ( STS-6) in April 1983. TDRS-1 survived a malfunction of the Inertial Upper Stage eventually utilizing its own propulsion system to success fully reach its assigned station in geosynchronous orbit. The anomalo us beginning of the TDRS-1 mission was not without lasting consequenc es as the primary reaction control system (A-side) was completely di sabled with an apparent propellant leak and the secondary system (B-s ide) suffered damage to its negative roll thruster rendering the thru ster inoperable. Following decommissioning the challenge to completin g a successful TDRS-1 end-of-mission (EOM) was the implementation of the stringent orbital debris requirements of NPR 8715.6 with a parti ally functioning spacecraft not originally designed to meet those req uirements. The TDRS-1 EOM had three key goals: 1) removal of the spac ecraft from geosynchronous orbit; 2) depletion of the remaining prope llant; and 3) passivation of all other sources of energy storage or generation. The TDRS-1 EOM approach was one of minimizing risks while accomplishing the goals above. The orbit raising portion of EOM was accomplished using deltavelocity operations already proven during pre vious stationchanging maneuvers. The propellant depletion approach wa s necessarily more aggressive as over 20 hours of burn time was requ ired to deplete the remaining fuel. A novel approach utilizing a spin ning, thrusting, passively controlled spacecraft configuration was ut ilized to achieve reasonable burn durations that met schedule constra ints. This nonstandard configuration required careful analysis of ele ctrical, thermal, and communication subsystems. The configuration wa s thoroughly simulated prior to the start of operations and carefully characterized during the initial spin period and first burn. Passiva tion was by definition a unique operation not previously performed wi thin the TDRS 1-7 constellation. Use was made of a TDRS spacecraft si mulator to verify the operational procedure to mitigate risks and pro vide crew training. TDRS-1 orbit raising maneuvers commenced on June 5th 2010 and completed on June 14th with an apogee 370 km and a peri gee 352 km above geosynchronous altitude. 127 kg of propellant were e stimated to be remaining in the tanks at the completion of orbit rais ing. TDRS-1 was placed in its spinning orientation on June 16th and the first fuel depletion burn was performed the following day. A seri es of 10 depletion burns were performed ending on June 26th when both propellant tank pressures experienced dramatic drops. Final passivat ion was performed on June 27 th deactivating electronics, removing t he batteries from the bus and solar arrays, and disabling the space-t o-ground communications equipment. The Second TDRS Ground Terminal (S TGT) continued to open loop track TDRS-1 for several days attempting command reacquisition several times a day. All attempts were unsucce ssful confirming passivation was achieved. The TDRS-1 orbit at passiv ation was an orbital debris compliant 36,319 x 36,128 km in height. W hile differing spacecraft designs may preclude mimicking the exact TD RS-1 EOM approach, the TDRS-1 campaign serves to demonstrate that pr e-NPR 8715.6 designs can be made to meet the requirements resulting i n a reduced orbit debris environment for future missions

Mirczak, Walter↗

NASA NTRS2013

Elastically Shaped Wing Optimization and Aircraft Concept for Improved Cruise Efficiency

This paper presents the findings of a study conducted tn 2010 by the NASA Innovation Fund Award project entitled "Elastically Shaped Future Air Vehicle Concept". The study presents three themes in support of meeting national and global aviation challenges of reducing fuel burn for present and future aviation systems. The first theme addresses the drag reduction goal through innovative vehicle configurations via non-planar wing optimization. Two wing candidate concepts have been identified from the wing optimization: a drooped wing shape and an inflected wing shape. The drooped wing shape is a truly biologically inspired wing concept that mimics a seagull wing and could achieve about 5% to 6% drag reduction, which is aerodynamically significant. From a practical perspective, this concept would require new radical changes to the current aircraft development capabilities for new vehicles with futuristic-looking wings such as this concept. The inflected wing concepts could achieve between 3% to 4% drag reduction. While the drag reduction benefit may be less, the inflected-wing concept could have a near-term impact since this concept could be developed within the current aircraft development capabilities. The second theme addresses the drag reduction goal through a new concept of elastic wing shaping control. By aeroelastically tailoring the wing shape with active control to maintain optimal aerodynamics, a significant drag reduction benefit could be realized. A significant reduction in fuel burn for long-range cruise from elastic wing shaping control could be realized. To realize the potential of the elastic wing shaping control concept, the third theme emerges that addresses the drag reduction goal through a new aerodynamic control effector called a variable camber continuous trailing edge flap. Conventional aerodynamic control surfaces are discrete independent surfaces that cause geometric discontinuities at the trailing edge region. These discontinuities promote vorticities which result in drag rises as well as noise sources. The variable camber trailing edge flap concept could provide a substantial drag reduction benefit over a conventional discrete flap system. Aerodynamic simulations show a drag reduction of over 50% could be achieved with the flap concept over a conventional discrete flap system.

Nguyen, Nhan↗

NASA NTRS2010

Lunar Reconnaissance Orbiter (LRO) Guidance, Navigation and Control (GN&C) Overview

The National Aeronautics and Space Administration s (NASA) Lunar Reconnaissance Orbiter (LRO) launched on June 18, 2009 from the Cape Canaveral Air Force Station aboard an Atlas V launch vehicle and into a direct insertion trajectory to the oon. LRO, which was designed, built, and operated by the NASA Goddard Space Flight Center in Greenbelt, MD, is gathering crucial data on the lunar environment that will help astronauts prepare for long-duration lunar expeditions. The mission has a nominal life of 1 year as its seven instruments find safe landing sites, locate potential resources, characterize the radiation environment, and test new technology. To date, LRO has been operating well within the bounds of its requirements and has been collecting excellent science data images taken from the LRO Camera Narrow Angle Camera of the Apollo landing sites appeared on cable news networks. A significant amount of information on LRO s science instruments is provided at the LRO mission webpage. LRO s Guidance, Navigation and Control (GN&C) subsystem is made up of an onboard attitude control system (ACS) and a hardware suite of sensors and actuators. The LRO onboard ACS is a collection of algorithms based on high level and derived requirements, and reflect the science and operational events throughout the mission lifetime. The primary control mode is the Observing mode, which maintains the lunar pointing orientation and any offset pointing from this baseline. It is within this mode that all science instrument calibrations, slews and science data is collected. Because of a high accuracy requirement for knowledge and pointing, the Observing mode makes use of star tracker (ST) measurement data to determine an instantaneous attitude pointing. But even the star trackers alone do not meet the tight requirements, so a six-state Kalman Filter is employed to improve the noisy measurement data. The Observing mode obtains its rate information from an inertial reference unit (IRU) and in the event of an IRU failure, the rate data is be derived from the star tracker, but with degraded pointing performance. The Delta-V control mode responsibility is to maintain attitude pointing during the cruise trajectory, insertion burns and lunar orbit maintenance by adjustments made to the spacecraft s velocity magnitude and vector direction. The ACS also provides for a thruster based system momentum management algorithm (known as Delta-H) to maintain the system and wheel momentum to within acceptable levels. In the event an anomaly causes the LRO spacecraft to lose the ability to maintain its current attitude pointing, a Sun Safe mode is included in the ACS for the purpose of providing a known power and thermally safe coarse inertial sun attitude for an indefinite period of time, within the manageable limits of the reaction wheels. The Sun Safe mode is also the initial spacecraft control mode off of the launch vehicle and provides for a means to null tip-off rates immediately after separation. The nominal configuration is to use the IRU for rate information in the controller. In the event of a gyro failure a gyroless control mode was developed that computes rate information from the CSS data.

Garrick, Joseph↗

DOE OSTI2020

Development of the Marble experimental platform at the National Ignition Facility

The Marble experimental platform at the National Ignition Facility (NIF) was developed to quantify the influence of heterogeneous mix on fusion burn. The platform utilizes a plastic capsule filled with a deuterated plastic foam of controlled coarseness, with tritium gas filling the voids in the foam. The capsule implosion is driven with x rays generated in an NIF Hohlraum in which the time-dependent symmetry of the implosion can be controlled via dynamic beam phasing. Importantly, the Hohlraum drive conditions can be understood via integrated 2D radiation-hydrodynamic simulations, and capsule implosions can be reliably calculated. After several years of development and experimentation, the NIF Marble platform has become successful and has produced important experimental results. Here, the experimental results, which will be presented in a future publication by the LANL Marble team, provide the first definitive examination of the influence of heterogeneous mix on thermonuclear burn.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

NASA NTRS2017

Seasonal Impact of Regional Outdoor Biomass Burning on Air Pollution in Three Indian Cities: Delhi, Bengaluru, and Pune

Air pollution in many of India's cities exceeds national and international standards, and effective pollution control strategies require knowledge of the sources that contribute to air pollution and their spatiotemporal variability. In this study, we examine the influence of a single pollution source, outdoor biomass burning, on particulate matter (PM) concentrations, surface visibility, and aerosol optical depth (AOD) from 2007 to 2013 in three of the most populous Indian cities. We define the upwind regions, or "airsheds," for the cities by using atmospheric back trajectories from the HYSPLIT model. Using satellite fire radiative power (FRP) observations as a measure of fire activity, we target pre-monsoon and post-monsoon fires upwind of the Delhi National Capital Region and pre-monsoon fires surrounding Bengaluru and Pune. We find varying contributions of outdoor fires to different air quality metrics. For the post-monsoon burning season, we find that a subset of local meteorological variables (air temperature, humidity, sea level pressure, wind speed and direction) and FRP as the only pollution source explained 39% of variance in Delhi station PM(sub 10) anomalies, 77% in visibility, and 30% in satellite AOD; additionally, per unit increase in FRP within the daily airshed (1000 MW), PM(sub 10) increases by 16.34 micrograms per cubic meter, visibility decreases by 0.097 km, and satellite AOD increases by 0.07. In contrast, for the pre-monsoon burning season, we find less significant contributions from FRP to air quality in all three cities. Further, we attribute 99% of FRP from post-monsoon outdoor fires within Delhi's average airshed to agricultural burning. Our work suggests that although outdoor fires are not the dominant air pollution source in India throughout the year, post-monsoon fires contribute substantially to regional air pollution and high levels of population exposure around Delhi. During 3-day blocks of extreme PM(sub 2.5) in the 2013 post-monsoon burning season, which coincided with statistically significant high fire activity, concentrations in Delhi averaged 304 micrograms per cubic meter, or more than 1000% above the 24-h PM(sub 2.5) guideline (25 micrograms per cubic meter) of the World Health Organization. These results suggest that providing viable alternatives to agricultural residue burning could help improve post-monsoon air quality for a growing population of 63 million (39% in urban areas) within Delhi's airshed.

Air quality; Outdoor fires; Crop residue burning; ↗

NASA NTRS1994

Biomass Burning and the Production of Greenhouse Gases

Biomass burning is a source of greenhouse gases, carbon dioxide, methane, and nitrous oxide. In addition, biomass burning is a source of chemically active gases, including carbon monoxide, nonmethane hydrocarbons, and nitric oxide. These gases, along with methane, lead to the chemical production of tropospheric ozone (another greenhouse gas) as well as control the concentration of the hydroxyl radical, which regulates the lifetime of almost every atmospheric gas. Following biomass burning, biogenic emissions of nitrous oxide, nitric oxide, and methane are significantly enhanced. It is hypothesized that enhanced postburn biogenic emissions of these gases are related to fire-induced changes in soil chemistry and/or microbial ecology. Biomass burning, once believed to be a tropical phenomenon, has been demonstrated by satellite imagery to also be a regular feature of the world's boreal forests. One example of biomass burning is the extensive 1987 fire that destroyed more than 12 million acres of boreal forest in the People's Republic of China and across its border in the Soviet Union. Recent estimates indicate that almost all biomass burning is human-initiated and that it is increasing with time. With the formation of greenhouse and chemically active gases as direct combustion products and a longer-term enhancement of biogenic emissions of gases, biomass burning may be a significant driver for global change.

Levine, Joel S.↗

NASA NTRS2007

Zero-Propellant Maneuver[TM] Flight Results for 180 deg ISS Rotation

This paper presents results for the Zero Propellant Maneuver (ZPM) TradeMark attitude control concept flight demonstration. On March 3, 2007, a ZPM was used to reorient the International Space Station 180 degrees without using any propellant. The identical reorientation performed with thrusters would have burned 110lbs of propellant. The ZPM was a pre-planned trajectory used to command the CMG attitude hold controller to perform the maneuver between specified initial and final states while maintaining the CMGs within their operational limits. The trajectory was obtained from a PseudoSpectral solution to a new optimal attitude control problem. The flight test established the breakthrough capability to simultaneously perform a large angle attitude maneuver and momentum desaturation without the need to use thrusters. The flight implementation did not require any modifications to flight software. This approach is applicable to any spacecraft that are controlled by momentum storage devices.

Bedrossian, Nazareth↗

DOE OSTI2022

Regulation of the central safety factor and normalized beta under low NBI torque in DIII-D

An algorithm has been designed to simultaneously control the central safety factor (q 0 ) and normalized beta (β N ) while ensuring near-zero torque from the neutral beam injection in DIII-D. Feedback control of q 0 and β N in tokamaks can be beneficial due to the close relationship that these variables have with plasma performance and magneto-hydrodynamic stability. In addition, low neutral-beam-torque conditions are of special interest in present devices because future burning-plasma tokamaks such as ITER will most likely operate at very low plasma rotation. The control synthesis of the algorithm presented in this work is based on a linearized, one-dimensional (1D) model of the current-profile dynamics coupled with a zero-dimensional (0D) plasma-energy balance. The actuators considered are neutral beam injection and electron-cyclotron heating and current drive, and discrete logic determines the neutral-beam injection powers that deliver near-zero torque. Here, the algorithm has been tested in nonlinear, 1D simulations using COTSIM (Control-Oriented Transport SIMulator) and in DIII-D experiments, demonstrating satisfactory performance.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2023

Self-Organization and Nitrogen Incorporation in Diamond-Like Carbon Microstructures Synthesized by Nonthermal Plasma

Nonthermal plasma activation of light alkanes is an encouraging decarbonization strategy to produce chemicals or fuels from abundant and/or flared carbon sources. However, prolific carbon growth on both the catalyst and electrode has limited its practicality, requiring additional knowledge of the carbon structure and growth mechanism before breakthroughs are realized. Furthermore, visual evidence is provided for nonuniform diamond-like carbon (DLC) microstructures that materialize in a coaxial dielectric barrier discharge (DBD) reactor flowing ethane and He at 278 K. Through a connection to known behaviors of DBD microdischarge patterns, the microstructure spacing was controlled by altering the applied voltage (ΔV) of the plasma or the burning voltage (U b ). Additionally, carbon valorization through nitrogen incorporation from N 2 was explored as an orthogonal solution to carbon mitigation, with N/C values >0.25 achieved and both sp 2 and sp 3 C–N bonding observed in the microstructures.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗