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At least 325 records · Page 18
All sourcesNASA NTRSDOE OSTI
NASA NTRS1973

Mass spectrometry and inhomogeneous ion optics

Work done in several areas to advance the state of the art of magnetic mass spectrometers is described. The calculations and data necessary for the design of inhomogeneous field mass spectrometers, and the calculation of ion trajectories through such fields are presented. The development and testing of solid state ion detection devices providing the capability of counting single ions is discussed. New techniques in the preparation and operation of thermal-ionization ion sources are described. Data obtained on the concentrations of copper in rainfall and uranium in air samples using the improved thermal ionization techniques are presented. The design of a closed system static mass spectrometer for isotopic analyses is discussed. A summary of instrumental aspects of a four-stage mass spectrometer comprising two electrostatic and two 90 deg. magnetic lenses with a 122-cm radius used to study the interaction of ions with solids is presented.

White, F. A.↗
NASA NTRS1974

Flight test of a pressurization system used to measure minor atmospheric constituents from an aircraft

A flight evaluation of an ambient air sample pressurization system was conducted at altitudes between 6 and 12 km. The system regulated the sample pressure to 10.15 + or - 0.1 N/sq n and provided sample flow to three gas analysis instruments included in the system. Ozone concentrations measured by two instruments employing different techniques varied from about 30 parts per billion by volume (ppbv) to over 350 ppbv, and the two ozone monitors agreed to within 20 ppbv. A carbon dioxide analyzer indicated modifications required for future installations.

Reck, G. M.↗
NASA NTRS1974

Aerodynamic size distribution of suspended particulate matter in the ambient air in the city of Cleveland, Ohio

The City of Cleveland Division of Air Pollution Control and NASA jointly investigated the chemical and physical characteristics of the suspended particulate matter in Cleveland, and as part of the program, measurements of the particle size distribution of ambient air samples at five urban locations during August and September 1972 were made using high-volume cascade impactions. The distributions were evaluated for lognormality, and the mass median diameters were compared between locations and as a function of resultant wind direction. Junge-type distributions were consistent with dirty continental aerosols. About two-thirds of the suspended particulate matter observed in Cleveland is less than 7 microns in diameter.

Leibecki, H. F.↗
NASA NTRS1975

Upper atmosphere pollution measurements (GASP)

The environmental effects are discussed of engine effluents of future large fleets of aircraft operating in the stratosphere. Topics discussed include: atmospheric properties, aircraft engine effluents, upper atmospheric measurements, global air sampling, and data reduction and analysis

Rudey, R. A.↗
NASA NTRS1975

Development and testing of a portable wind sensitive directional air sampler

A portable wind-sensitive directional air sampler has been developed as part of an air pollution source identification system. The system is designed to identify sources of air pollution based on the directional collection of field air samples and their analysis for TSP and trace element characteristics. Sources can be identified by analyzing the data on the basis of pattern recognition concepts. Functional testing of a prototype sampler is described; all items exhibited performance and life sufficient to carry out field performance test operations. Life testing of the wind direction sensor and the directional porting valves, which are critical to reliable operation, was emphasized with successful results.

Deyo, J.↗
NASA NTRS1975

Concentrations of CH4, CO, CO2, H2, H2O and N2O in the upper stratosphere

On 23 May 1973 a cryogenic air sampler was flown on an Aerobee rocket from White Sands Missile Range. A large air sample was collected between 40 and 50 km altitude and successfully recovered for water vapor and trace gas analysis. The results were as follows: water vapor, 4.0 (+1.3 or - 0.9) ppmV; methane, 0.37 + or - 0.01 ppmV; molecular hydrogen, 0.47 + or - 0.02 ppmV; carbon monoxide, 0.05 + or - 0.01 ppmV; carbon dioxide, 316.2 + or - 2.8 ppmV; and nitrous oxide, 3 + or - 7 ppb.

Ehhalt, D. H.↗
NASA NTRS1975

Space Shuttle Trace Gas Analyzer

A Trace Gas Analyzer (TGA) with the ability to detect the presence of toxic contaminants in the Space Shuttle atmosphere within the subparts-per-million range is under development. The design is a modification of the miniaturized Gas Chromatograph-Mass Spectrometer (GCMS) developed for the Viking Mars Lander. An ambient air sample is injected onto the GC column from a constant volume sample loop and separated into individual compounds for identification by the MS. The GC-MS interface consists of an effluent divider and a silver-paladium separator, an electrochemical cell which removes more than 99.99% of the hydrogen carrier gas. The hydrogen is reclaimed and repressurized without affecting the separator efficiency, a feature which enables a considerable weight reduction in the carrier gas supply system.

Dencker, W.↗
NASA NTRS1976

Measurements of atmospheric ozone made from a GASP-equipped 747 airliner Mid-March, 1975

This paper presents data on the ozone mixing ratio, static air temperature, wind speed, and wind direction obtained at altitudes from 8 to 12 km during several flights of a commercial airliner equipped with a fully automated air-sampling system developed for the NASA Global Atmospheric Sampling Program (GASP). The objectives of GASP are reviewed, and the data-gathering techniques are described. Two data sets are discussed which illustrate variations of the upper-tropospheric and lower-stratospheric ozone mixing ratios as a function of geographical location and aircraft altitude. Good agreement is found between the GASP data and the tropopause height obtained from National Meteorological Center gridded data.

Falconer, P. D.↗
NASA NTRS1976

Status of NASA aircraft engine emission reduction and upper atmosphere measurement programs

Advanced emission reduction techniques for five existing aircraft gas turbine engines are evaluated. Progress made toward meeting the 1979 EPA standards in rig tests of combustors for the five engines is reported. Results of fundamental combustion studies suggest the possibility of a new generation of jet engine combustor technology that would reduce oxides-of-nitrogen (NOx) emissions far below levels currently demonstrated in the engine-related programs. The Global Air Sampling Program (GAS) is now in full operation and is providing data on constituent measurements of ozone and other minor upper-atmosphere species related to aircraft emissions.

Rudey, R. A.↗
NASA NTRS1977

Ion chromatographic determination of anions collected on filters at altitudes between 9.6 and 13.7 kilometers

The investigation of atmospheric pollution to determine the anion-containing particulates in the atmosphere at altitudes between 9.6 and 13.7 km is discussed. Air samples collected on cellulose fiber discs impregnated with dibutoxyethylphthalate require very sensitive methods of analysis. It is concluded that ion chromatography is suited for the determination of anions collected on the filters. Methods to control contamination and interfering side reactions are described.

Otterson, D. A.↗
NASA NTRS1977

Evaluation of a hydrogen chloride detector for environmental monitoring

The paper describes a hydrogen chloride detector designed to monitor concentrations of hydrogen chloride gas in the ambient environment. The detector was developed for NASA for use in launch vehicle effluent monitoring. The detector operates on chemiluminescence principles with a lower detection limit of less than 5 x 10 to the -3rd ppm (by volume). The hydrogen chloride in the air sample reacts with a bromide-bromate coating in the inlet tube of the instrument producing bromine. Bromine is then quantitated by chemiluminescent oxidation of luminol. The visible light generated in the chemiluminescent reaction is proportional to the hydrogen chloride concentration of the sampled airstream. The detector is most suited to laboratory or field studies where hydrogen chloride is the dominant pollutant, as compared to the interfering species. Interferences include strong acids, acid-forming gases, and halogen gases. Of the interferences investigated the most serious in these groups are hydrochloric and sulfuric acid, sulfur dioxide, and chlorine, respectively. The detector has been in use since 1974 and has been found to be highly portable, rugged, and stable under extreme environmental conditions.

Gregory, G. L.↗
NASA NTRS1978

High-flying Mini-Sniffer RPV - Mars bound

The Mini-Sniffer is a small unmanned survey aircraft developed by NASA to conduct turbulence and atmospheric pollution measurements from ground level to an altitude of 90,000 ft. Carrying a 25-lb air sampling apparatus, the Mini-Sniffer typically cruises for one hour at 70,000 ft before being remotely piloted back to earth. A hydrazine monopropellant engine powers the craft, while a PCM telemetering system and a radar transponder provide control functions. Development of a high-performance low-Reynolds-number airfoil could make the research craft suitable for a low-altitude terrain-following mission on Mars.

Reed, R. D.↗
NASA NTRS1979

Recommendations of the panels: Panel on in-flight measurements

The attenuation factor for aircraft other than the B-747 in reducing the ambient ozone concentrations which enter the cabin is obtained. The need to continue NASA Global Air Sampling Program measurements was expressed for three main purposes; testing new filters, correlation of complaints with ozone levels, and ambient ozone data. The need to continue cooperation between NASA and industry is indicated. Concern with regard to the correlation of ozone levels and complaints was given. The need to measure the variability of ozone within the aircraft cabin was investigated. The requirement for an onboard ozone monitor on all aircraft is discussed.

Rogers, J.↗
NASA NTRS1979

Measurement of NO and O3 from aircraft: 1977 tropical convergence zone experiment

As part of the Ames Research Center program to explore the nature of stratosphere-troposphere exchange processes occurring in the Intertropical Convergence Zone, simultaneous in situ measurements of nitric oxide and ozone mixing ratios were made with the Ames stratospheric air sampler SAS 2. The SAS 2 is a second-generation system; it employs four parallel sensors and was designed primarily for measurements at altitudes of 60,000 ft and above on the U-2 stratospheric research aircraft. The only modifications required for this study was the addition of an air sample flow restrictor. Data were obtained with the SAS 2 system on July 26, 27, 30 and 31, 1977. Generally, 30-min measurements were made at each of six altitudes ranging from 45,000 ft to 70,000 ft, and separated by 5,000 ft intervals.

Starr, W. L.↗
NASA NTRS1980

Polar nephelometer for atmospheric particulate studies

A unique polar nephelometer was designed and constructed for the measurement of atmospheric particulate characteristics. The nephelometer produces visible light from a self-contained laser to irradiate an air sample drawn into the instrument. The light scattered from the particulates and molecules in the sample is detected as a function of scattering angle for each of four different incident light polarizations. These measurements are used to determine the particulate scattering matrix which is a function of the size, shape, and index of refraction of the particles. The region of sensitivity for the measurements corresponds to the size range of particles that strongly affects visible radiative transfer in the atmosphere, which is the primary application for the derived information.

Hansen, M. Z.↗
NASA NTRS1980

Recent assessment of the performance and accuracy of a chemiluminescent rocket sonde for upper atmospheric ozone measurements

The chemiluminescent rocket ozonesonde utilizing rhodamine-B as a detector and self-pumping for air sampling has been improved. The instrument employs standard meteorological sounding systems and is the only technique available for routine nighttime ozone measurements above balloon altitudes. The chemiluminescent detector, when properly calibrated, is shown to be specific to ozone, stable, and of sufficient sensitivity for accurate measurements of ozone from about 65-20 km. An error analysis indicates that the measured ozone profiles have an absolute accuracy of about + or - 12% and a precision of about + or - 6%. Approximately 20 flights have been conducted for geophysical investigations, while additional flights were conducted with other rocket and satellite ozone soundings for comparisons. In general, these comparisons showed good agreement.

Hilsenrath, E.↗
NASA NTRS1981

A cloud condensation nucleus spectrometer designed for airborne measurements

The spectrometer is a simple extension of the continuous flow diffusion chamber (CFDC) operated in the vertical mode. The principal new design features of the instrument are its rapid time response and ability to rapidly measure the CCN activity spectrum. The activity spectrum of CCN in an air sample is measured by simultaneously operating the spectrometer at four supersaturations. The CCN spectrometer consists of four essentially indepenent CFDC's in a parallel array. Each CFDC is 61 cm long, 10 cm wide, and consists of two vertical parallel plates 1 cm apart, maintained at different temperatures. Each CFDC has a single particle optical counter located at the center of its base.

Radke, L. F.↗