Generation of long time creep data on refractory alloys at elevated temperatures Quarterly report, 14 Dec. 1967 - 27 Mar. 1968
Creep analysis of refractory metal alloys at high temperatures under ultrahigh vacuum conditions
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Creep analysis of refractory metal alloys at high temperatures under ultrahigh vacuum conditions
Cathode surface whiskers initiating electrical breakdown in ultrahigh vacuum
Collector gauge and orbitron gauge for ultrahigh vacuum measurements
Adhesion experiments with terrestrial materials in ultrahigh vacuum and comparison with lunar soil data
Au, Ag and Al films evaporation in ultrahigh vacuum on LiF and MgO surfaces, showing insignificant role of lattice misfit for epitaxy
Time dependent adhesion in ultrahigh vacuum of Apollo 11 lunar soil sample 10065-33, considering microchemical and microphysical properties
Solid lubricant applied to porous roller bearings prior to use in ultrahigh vacuum
Refractory alloy creep test data for molybdenum base alloy TZM, pure tantalum, and tantalum base alloys T-111 and ASTAR-811C at elevated temperatures in ultrahigh vacuum
Friction experiments in ultrahigh vacuum to evaluate sputtered MoS2 film lubricants
Properties of rocks, soils, and minerals in ultrahigh vacuum facility simulating lunar environment, for extraterrestrial resource utilization
Ultrahigh vacuum deposited Ni, Fe, W and Mo films, determining molecular oxygen adsorption efficiencies
Hydrogen and carbon monoxide coadsorption on platinum single crystal surface, examining interactions and species formation by thermal flash and electron impact techniques in ultrahigh vacuum
Contact potential measurements of work function dependence on adsorption of alkali metals on Ta/110/ and W/100/ crystals under ultrahigh vacuum
Epitaxial deposition of Au on ultrahigh vacuum cleaved mica during early nucleation and growth
The metallurgical structure and some of the mechanical properties of two cobalt alloys, cobalt-50% iron and cobalt-25% molybdenum-10% chromium, were determined under various heat treated conditions. The mechanical properties of the bcc disordered Co-50Fe alloy, which was found to be very brittle, indicated an exceedingly low fracture strength, low hardness, and very weak grain boundary strength. Ordering by suitable heat treatment only produced a more brittle material with a lower fracture strength and a slightly higher hardness value. Work hardening was found to produce a finer grain structure and a greater grain boundary strength. Tensile properties were examined. It was found that the Co-25Mo-10Cr alloy was difficult to place in the alpha Co solid solution condition, which limited the ability to use precipitation as a hardening reaction. Over two hundred adhesion cycles from zero contact load, to maximum load, to fracture were conducted between couples for each of the above alloys in an ultrahigh vacuum system which would permit the sample surfaces to be cleaned of all contaminant layers. In the Co-50Fe case, the calculated fracture stress from the adhesion tests showed values in the range of 80 to 150 k.s.i., which is about ten times greater than the values from tension tests.
Metallic transfer between polycrystalline metals in sliding contact was examined. Hemispherical riders of iron, nickel, and cobalt were slid on tungsten, tantalum, niobium, and molybdenum disks in ultrahigh vacuum. Auger emission spectroscopy was used to monitor the elemental composition of the disk surfaces. Iron, nickel, and cobalt transferred to tungsten, whereas only cobalt transferred to tantalum, niobium, and molybdenum. The results of this investigation are discussed in terms of the cohesive energy and strain hardening characteristics of the specimen materials.
The procedures are described along with results obtained in a test program conducted to demonstrate the performance of a candidate lunar mass spectrometer. The instrument was designed to sample and measure gases believed to exist in the lunar atmosphere at the surface. The subject instrument consists of a cold cathode ion source, a small quadrupole mass analyzer and an off axis electron multiplier ion counting detector. The major program emphasis was placed on demonstrating instrument resolution, sensitivity and S/N ratio over the mass range 0-150 amu and over a partial pressure range from 10 to the minus 9th power to 10 to the minus 13th power torr. Ultrahigh vacuum tests were conducted and the minimum detectable partial pressure for neon, argon, krypton and xenon was successfully determined for the spectrometer using isotopes of these gases. With the exception of neon, the minimum detectable partial pressure is approximately 4 x 10 to the minus 14th power torr for the above gases.
The adhesion and transfer of polytetrafluoroethylene (PTFE) to metals in ultrahigh vacuum has been studied using Auger emission spectroscopy. The transfer was effected both by compressive static contact and by sliding contact. The transfer observed after static contact was independent of the chemical constitution of the substrate. Electron induced desorption of the fluorine in the transferred PTFE showed that the fluorine had no chemical interaction with the metal substrate. The coefficient of friction on metals was independent of the chemical constitution of the substrate. However, sliding PTFE on soft metals such as aluminum, generated wear fragments that lodged in the PTFE and machined the substrate.