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NASA NTRS2018

Thermophysical Properties of Nickel-Based Superalloys

The NASA Marshall Space Flight Center (MSFC) electrostatic levitation (ESL) laboratory has a long history of providing materials research and thermophysical property data. The lab can measure thermophysical properties such as density, surface tension, and viscosity of liquid materials, including elements, alloys, glasses, ceramics, and oxides. Nickel-based superalloys (e.g. Inconel, Hastelloy, and Waspaloy) have many high performance applications, including turbine engines for aerospace. Superalloy parts are typically manufactured by casting and forging. These processes generate both polycrystalline and monocrystalline parts. A relatively new method of fabrication of turbine disk materials is additive manufacturing, which is typically done for aerospace parts by powder-bed methods such as selective laser melting (SLM). Accurate modeling of casting and forging, as well as additively manufacturing processes, require thermophysical properties (density, surface tension, and viscosity). The thermophysical properties of liquid nickel-based superalloys, both conventional and additively manufactured, were measured at several temperatures in both undercooled and superheated condition. Surface tension and viscosity was measured using the oscillating drop method and density and thermal expansion was measured using edge detection methods.

SanSoucie, Michael P.↗

DOE OSTI2025

Generative learning for slow manifolds and bifurcation diagrams

In dynamical systems characterized by separation of time scales, the approximation of so called “slow manifolds”, on which the long term dynamics lie, is a useful step for model reduction. Initializing on such slow manifolds is a useful step in modeling, since it circumvents fast transients, and is crucial in multiscale algorithms (like the equation-free approach) alternating between fine scale (fast) and coarser scale (slow) simulations. In a similar spirit, when one studies the infinite time dynamics of systems depending on parameters, the system attractors (e.g., its steady states) lie on bifurcation diagrams (curves for one-parameter continuation, and more generally, on manifolds in state parameter space. Sampling these manifolds gives us representative attractors (here, steady states of ODEs or PDEs) at different parameter values. Algorithms for the systematic construction of these manifolds (slow manifolds, bifurcation diagrams) are required parts of the “traditional” numerical nonlinear dynamics toolkit. In more recent years, as the field of Machine Learning develops, conditional score-based generative models (cSGMs) have been demonstrated to exhibit remarkable capabilities in generating plausible data from target distributions that are conditioned on some given label. It is tempting to exploit such generative models to produce samples of data distributions (points on a slow manifold, steady states on a bifurcation surface) conditioned on (consistent with) some quantity of interest (QoI, observable). In this work, we present a framework for using cSGMs to quickly (a) initialize on a low-dimensional (reduced-order) slow manifold of a multi-time-scale system consistent with desired value(s) of a QoI (a “label”) on the manifold, and (b) approximate steady states in a bifurcation diagram consistent with a (new, out-of-sample) parameter value. This conditional sampling can help uncover the geometry of the reduced slow-manifold and/or approximately “fill in” missing segments of steady states in a bifurcation diagram. Finally, the quantity of interest, which determines how the sampling is conditioned, is either known a priori or identified using manifold learning-based dimensionality reduction techniques applied to the training data.

Dynamical systems↗

NASA NTRS2009

The Soil Moisture Active and Passive (SMAP) Mission

The Soil Moisture Active and Passive (SMAP) Mission is one of the first Earth observation satellites being developed by NASA in response to the National Research Council s Decadal Survey. SMAP will make global measurements of the moisture present at Earth's land surface and will distinguish frozen from thawed land surfaces. Direct observations of soil moisture and freeze/thaw state from space will allow significantly improved estimates of water, energy and carbon transfers between land and atmosphere. Soil moisture measurements are also of great importance in assessing flooding and monitoring drought. SMAP observations can help mitigate these natural hazards, resulting in potentially great economic and social benefits. SMAP soil moisture and freeze/thaw timing observations will also reduce a major uncertainty in quantifying the global carbon balance by helping to resolve an apparent missing carbon sink on land over the boreal latitudes. The SMAP mission concept would utilize an L-band radar and radiometer. These instruments will share a rotating 6-meter mesh reflector antenna to provide high-resolution and high-accuracy global maps of soil moisture and freeze/thaw state every two to three days. The SMAP instruments provide direct measurements of surface conditions. In addition, the SMAP project will use these observations with advanced modeling and data assimilation to provide deeper root-zone soil moisture and estimates of land surface-atmosphere exchanges of water, energy and carbon. SMAP is scheduled for a 2014 launch date

Entekhabi, Dara↗

NASA NTRS2017

Land Surface Precipitation and Hydrology in MERRA-2

The Modern-Era Retrospective Analysis for Research and Applications, version 2 (MERRA-2), provides global, 1-hourly estimates of land surface conditions for 1980-present at 50-km resolution. Outside of the high latitudes, MERRA-2 uses observations-based precipitation data products to correct the precipitation falling on the land surface. This paper describes the precipitation correction method and evaluates the MERRA-2 land surface precipitation and hydrology. Compared to monthly GPCPv2.2 observations, the corrected MERRA-2 precipitation (M2CORR) is better than the precipitation generated by the atmospheric models within the cyclingMERRA-2 system and the earlier MERRA reanalysis. Compared to 3-hourlyTRMM observations, the M2CORR diurnal cycle has better amplitude but less realistic phasing than MERRA-2 model-generated precipitation. Because correcting the precipitation within the coupled atmosphere-land modeling system allows the MERRA-2 near-surface air temperature and humidity to respond to the improved precipitation forcing, MERRA-2 provides more self-consistent surface meteorological data than were available from the earlier, offline MERRA-Land reanalysis. Overall, MERRA-2 land hydrology estimates are better than those of MERRA-Land and MERRA. A comparison against GRACE satellite observations of terrestrial water storage demonstrates clear improvements in MERRA-2 over MERRA in South America and Africa but also reflects known errors in the observations used to correct the MERRA-2 precipitation. The MERRA-2 and MERRA-Land surface and root zone soil moisture skill vs. in situ measurements is slightly higher than that of ERA-Interim Land and higher than that of MERRA (significantly for surface soil moisture). Snow amounts from MERRA-2 have lower bias and correlate better against reference data than do those of MERRA-Land and MERRA, with MERRA-2 skill roughly matching that of ERA-Interim Land. Seasonal anomaly R values against naturalized stream flow measurements in the United States are, on balance, highest for MERRA-2 and ERA-Interim Land, somewhat lower for MERRA-Land, and lower still for MERRA.

MERRA-↗

NASA NTRS2018

GEONEX: Webpage to Display NASA-NOAA Collaboration of Producing Land Surface Products from Geostationary Sensors

The latest generation of geostationary satellites carry sensors such as the Advanced Baseline Imager (GOES-16/17) and the Advanced Himawari Imager (Himawari-8/9) that closely mimic the spatial and spectral characteristics of MODIS and VIIRS, useful for monitoring land surface conditions. The NASA Earth Exchange (NEX) team at Ames Research Center has embarked on a collaborative effort among scientists from NASA and NOAA exploring the feasibility of producing operational land surface products similar to those from MODIS/VIIRS. The team built a processing pipeline called GEONEX that is capable of converting raw geostationary data into routine products of Fires, surface reflectances, vegetation indices, LAI/FPAR, ET and GPP/NPP using algorithms adapted from both NASA/EOS and NOAA/GOES-R programs. The GEONEX pipeline has been deployed on Amazon Web Services cloud platform and it currently leverages near-realtime geostationary data hosted in AWS public datasets under a NOAA-AWS agreement.In order to better introduce the GEONEX products to the science community, we set up a simple webpage (www.geonex.org) to describe the background and the motivation of the project, the algorithms used in deriving the products, and user manuals to the data files. We will also update the status of the data processing, in particular the near-real-time products, on the website and provide links (in text or json files) to the latest datasets.

geostationary↗

NASA NTRS2019

GEONEX Data Products: Geostationary Satellite Derived Land Surface and Atmospheric Public Data Products

The latest generation of geostationary satellites carry sensors such as the Advanced Baseline Imager (GOES-16/17) and the Advanced Himawari Imager (Himawari-8/9) that closely mimic the spatial and spectral characteristics of MODIS and VIIRS, useful for monitoring land surface conditions. The NASA Earth Exchange (NEX) team at Ames Research Center has embarked on a collaborative effort among scientists from NASA and NOAA exploring the feasibility of producing operational land surface products similar to those from MODIS/VIIRS. The team built a processing pipeline called GEONEX that is capable of converting raw geostationary data into routine products of Fires, surface reflectances, vegetation indices, LAI/FPAR, ET and GPP/NPP using algorithms adapted from both NASA/EOS and NOAA/GOES-R programs. The GEONEX pipeline will begin to produce provisional data products to be consumed by external collaborators and the academic community. In order to better inform and introduce the GEONEX products to the science community, the provisional products shall be distributed from the NAS data portal, located at data.nas.nasa.gov, and simple webpage at www.nasa.gov/geonex has been deployed, which describes any algorithms used in deriving the products, user manuals and data file information. We will also update the status of the data processing, on the website and provide links to the latest datasets, and use a geonex mailing list, using lists.nasa.gov.

Wang, Weile↗

NASA NTRS2020

A Review of LIBS for Real-Time Detection of Trace Silicone Contaminants on CFRP Surfaces

Laser ablation is the removal of material by laser pulses through photochemical, photothermal, or photophysical mechanisms, which is useful to prepare an adherend surface for adhesive bonding. Laser surface treatment is a method that has been under research for the past decade at NASA Langley Research Center (LaRC) to prepare surfaces for adhesive joining of aerospace composite materials and metallic alloys. Laser ablation of composite materials increases surface area and removes the surface contaminants introduced during material handling and fabrication processes. By adjustment of laser parameters, it is possible to obtain repeatable surface conditions, and superficial contaminants can be selectively and efficiently removed without damaging the underlying carbon fibers or the carbon fiber reinforced polymer (CFRP) substrate. Laser induced breakdown spectroscopy (LIBS) is a surface characterization and inspection technique that can be seamlessly integrated into the laser surface treatment process. At NASA LaRC, a single laser system has been used for both laser surface treatment and LIBS, which enables in-situ monitoring of surface contaminants. This work focuses on the advancements at LaRC using LIBS to detect surface silicone contaminants on aerospace CFRP materials and to provide surface quality control in adhesive bonding.

Rodolfo I Ledesma↗

NASA NTRS2020

A Review of LIBS for Real-Time Detection of Trace Silicone Contaminants on CFRP Surfaces

Rodolfo I Ledesma↗

NASA NTRSDate not supplied

Deriving Broadband Radiances from Geostationary Satellite Visible Radiance Channels for Use in the CERES SYN1deg Product

The NASA CERES project was designed to monitor the Earth’s radiation budget, both at the regional and global scale. The CERES SSF1deg single satellite product provides TOA flux observations from Aqua, Terra, NPP, and NOAA-20. The SYN1deg product incorporates observations from Terra, Aqua, and geostationary (GEO) satellites. The GEO observations are included in the SYN1deg product to infer the regional diurnal cycle between CERES observations. GEO satellites throughout the CERES record have different narrowband spectral response functions and do not directly observe radiances over the broadband spectra of CERES instruments. Hence the emphasis of this study is improving the process of deriving broadband radiances from the myriad GEO visible channel observations. We present a new method for converting the narrowband radiances observed from GEO operational satellites. This study relies on radiative transfer model hyper-spectral radiances for many cloud and surface conditions under all angular conditions observed by GEO sensors. First, the hyper-spectral radiances from a radiative transfer model must be convolved with the spectral response function of the visible imager for each GEO sensor in the CERES record. For each angular bin and surface type, the clear-sky and multiple optical depth and phase cloudy-sky narrowband and broadband reflectance pairs are linearly regressed. This study found that, no matter how the scene conditions are stratified, for example the all-sky, clear-sky, ice or water clouds, they all provide similar linear regressions. This includes ocean glint conditions, where the clear-sky reflectance exceeds cloudy conditions and yet the relationship was found to be linear in the given angular bin. This infers that no GEO retrieved cloud information is necessary in the narrowband to broadband conversion process, which relies only on visible channel reflectance. Over land, most of the GEO visible channels do not observe the NIR vegetation reflectance. We intend to use land adjustment factors developed using the TOA reflectance difference between the real-time MODIS .86um and the .64um channel. We validate this approach by using coincident observational data between CERES and MODIS aboard Aqua and Terra as well as GEO and CERES observations .

CERES↗

NASA NTRS1993

Mineralogical diversity (spectral reflectance and Moessbauer data) in compositionally similar impact melt rocks from Manicouagan Crater, Canada

Meteoritic impacts under oxidizing surface conditions occur on both earth and Mars. Oxidative alteration of impact melt sheets is reported at several terrestrial impact structures including Manicouagan, West Clearwater Lake, and the Ries Basin. A number of studies have advocated that a significant fraction of Martian soil may consist of erosional products of oxidatively altered impact melt sheets. If so, the signature of the Fe-bearing mineralogies formed by the process may be present in visible and near infrared reflectivity data for the Martian surface. Of concern is what mineral assemblages form in impact melt sheets produced under oxidizing conditions and what their spectral signatures are. Spectral and Moessbauer data for 19 powder samples of impact melt rock from Manicouagan Crater are reported. Results show for naturally occurring materials that composite hematite-pyroxene bands have minima in the 910-nm region. Thus many of the anomalous Phobos-2 spectra, characterized by a shallow band minimum in the near-IR whose position varies between approximately 850 and 1000 nm, can be explained by assemblages whose endmembers (hematite and pyroxene) are accepted to be present on Mars. Furthermore, results show that a mineralogically diverse suite of rocks can be generated at essentially constant composition, which implies that variations in Martian surface mineralogy do not necessarily imply variations in chemical composition.

Morris, R. V.↗

NASA NTRS1993

NDE of PWA 1480 single crystal turbine blade material

Cantilever bending fatigue specimens were examined by fluorescent liquid penetrant and radioactive gas penetrant (Krypton) non-destructive evaluation (NDE) methods and tested. Specimens with cast, ground, or polished surface were evaluated to study the effect of surface condition on NDE and fatigue crack initiation. Fractographic and metallurgical analyses were performed to determine the nature of crack precursors. Preliminary results show that fatigue strength was lower for specimens with cast surfaces than for specimens with machined surfaces. The liquid penetrant and gas penetrant techniques both provided indications of a large population of defects on the cast surfaces. On ground or polished specimen surfaces, the gas penetrant appeared to estimate the actual number of voids more accurately than the liquid penetrant.

Klima, Stanley J.↗

NASA NTRS1994

Exopaleontology and the search for a fossil record on Mars

Although present Martian surface conditions appear unfavorable for life as we know it, there is compelling geological evidence that the climate of early Mars was much more Earth-like, with a denser atmosphere and abundant surface water. The fact that life developed on the Earth within the first billion years of its history makes it quite plausible that life may have also developed on Mars. If life did develop on Mars, it is likely to have left behind a fossil record. This has led to the development of a new subdiscipline of paleontology, herein termed 'exopaleontology', which deals with the exploration for fossils on other planets. The most important factor enhancing microbial fossilization is the rapid entombment of microorganisms by fine-grained, stable mineral phases, such as silica, phosphate, or carbonate. The oldest body fossils on Earth are preserved in this way, occurring as permineralized cells in fine-grained siliceous sediments (cherts) associated with ancient volcanic terranes in Australia and South Africa. Modern terrestrial environments where minerals may precipitate in the presence of microorganisms include subaerial thermal springs and shallow hydrothermal systems, sub-lacustrine springs and evaporitic alkaline lakes, zones of mineralization within soils where 'hardpans' (e.g. calcretes, silcretes) form, and high latitude frozen soils or ground ice.

Farmer, Jack D.↗

NASA NTRS1993

NDE of PWA 1480 single crystal turbine blade material

Cantilever bending fatigue specimens were examined by fluorescent liquid penetrant and radioactive gas penetrant (Krypton) Nondestructive Evaluation (NDE) methods and tested. Specimens with cast, ground, or polished surfaces were evaluated to study the effect of surface condition on NDE and fatigue crack initiation. Fractographic and metallurgical analyses were performed to determine the nature of crack precursors. Preliminary results show that fatigue strength was lower for specimens with cast surfaces than for specimens with machined surfaces. The liquid penetrant and gas penetrant techniques both provided indications of a large population of defects on the cast surfaces. On ground or polished specimen surfaces, the gas penetrant appeared to estimate the actual number of voids more accurately than the liquid penetrant.

Klima, Stanley J.↗

NASA NTRS1999

Origin and Reactivity of the Martian Soil: A 2003 Micromission

The role of water in the development of the martian surface remains a fundamental scientific question. Did Mars have one or more "warm and wet" climatic episodes where liquid water was stable at the surface? If so, the mineral phases present in the soils should be consistent with a history of aqueous weathering. More generally, the formation of hydrated mineral phases on Mars is a strong indicator of past habitable surface environments. The primary purpose of this investigation is to help resolve the question of whether such aqueous indicators are present on Mars by probing the upper meter for diagnostic mineral species. According to Burns [1993], the formation of the ferric oxides responsible for the visible color of Mars are the result of dissolution of Fe (+2) phases from basalts followed by aqueous oxidation and precipitation of Fe" mineral assemblages. These precipitates likely included iron oxyhydroxides such as goethite (a-FeOOH) and lepidocrocite (g-FeOOH), but convincing evidence for these phases at the surface is still absent. The stability of these minerals is enhanced beneath the surface, and thus we propose a subsurface search for hydroxylated iron species as a test for a large-scale chemical weathering process based on interactions with liquid water. It is also possible that the ferric minerals on Mars are not aqueous alteration products of the rocks. A chemical study of the Pathfinder landing site concluded that the soils are not directly derived from the surrounding rocks and are enhanced in Mg and Fe. The additional source of these elements might be from other regions of Mars and transported by winds, or alternatively, from exogenic sources. Gibson [1970] proposed that the spectral reflectivity of Mars is consistent with oxidized meteoritic material. Yen and Murray [1998] further extend Gibson's idea and show, in the laboratory, that metallic iron can be readily oxidized to maghemite and hematite under present-day martian surface conditions (in the absence of liquid water). A test for a meteoritic component of the soil can be conducted, as described below, by searching for the presence of Ni at the martian surface. The average abundance of nickel in an Fe-Ni meteorite is about 7% and, if present at measurable levels in the soil, would be indicative of an exogenic contribution. In addition, it may be possible to directly search for mineral phases common in meteorites. An understanding of the formation and evolution of the martian soil would not be complete without addressing the unusual reactivity discovered by the Viking Landers The presence of an inorganic oxidant, possibly one produced as a results of photochemical processes, is the most widely accepted explanation of the Viking results. Are these chemical species simply adsorbed on soil grains, or have they reacted with the metal oxide substrates and altered the mineral structures? Could a completely different (non-photochemical) process be responsible for the soil reactivity? The various ideas for the nature of this putative oxidant could be constrained by a measurement of the change in reactivity with depth. Different compositions will have different lifetimes and mobilities and thus will have different vertical profiles. Because the oxidizing compounds are believed to actively destroy organic molecules, determination of the reactivity gradient also has significant implications for the search for life on Mars. A DS2-based microprobe system can be instrumented for a 2003 micromission to investigate the origin and reactivity of the martian soil. These measurements would provide invaluable information regarding the climate history and exobiological potential of the planet. The NMR, X ray and chemiresistor measurement approach described embodies a highly synergistic and general set of soil interrogation methods for elements, compounds, and crystal structures and can also be applied to other geologic questions of interest. For example, if the capability for precise targeting of the probes is available, then in-situ investigations of suspected evaporite and hydrothermal deposits would be possible with the same set of instruments. Additional information is contained in the original.

Yen, Albert S.↗

NASA NTRS2001

Evaluation of The Performance of The Mars Environmental Compatibility Assessment Electrometer

The Mars Environmental Compatibility Assessment (MECA) electrometer is an instrument that was designed jointly by researchers at the Jet Propulsion Laboratory and the Kennedy Space Center, and is intended to fly on a future space exploration mission of the surface of Mars. The electrometer was designed primarily to study (1) the electrostatic interaction between the Martian soil and five different types of insulators, which are attached to the electrometer, as the electrometer is rubbed over the Martian soil. The MECA/Electrometer is also capable of measuring (2) the presence of charged particles in the Martian atmosphere, (3) the local electric field strength, and (4) the local temperature. The goal of the research project described in this report was to test and evaluate the measurement capabilities of the MECA/Electrometer under simulated Martian surface conditions using facilities located in the Labs and Testbeds Division at the Kennedy Space Center. The results of this study indicate that the Martian soil simulant can triboelectrically charge up the insulator surface. However, the maximum charge buildup did not exceed 18% of the electrometer's full-range sensitivity when rubbed vigorously, and is more likely to be as low as 1% of the maximum range when rubbed through soil. This indicates that the overall gain of the MECA/Electrometer could be increased by a factor of 50 if measurements at the 50% level of full-range sensitivity are desired. The ion gauge, which detects the presence of charged particles, was also evaluated over a pressure range from 10 to 400 Torr (13 to 533 mbar). The electric field sensor was also evaluated. Although the temperature sensor was not evaluated due to project time constraints, it was previously reported to work properly.

Mantovani, James G.↗

NASA NTRS2002

Evaluation of the Performance of the Mars Environmental Compatibility Assessment Electrometer

Mantovani, James G.↗

NASA NTRS2010

Ultra Low Temperature Ultra Low Power Instrument Packages for Planetary Surfaces

Achievement of solar system exploration roadmap goals will involve robotic or human deployment and longterm operation of surface science packages remote from human presence, thus requiring autonomous, self-powered operation. The major challenge such packages face will be operating during long periods of darkness in extreme cold potentially without the Pu238 based power and thermal systems available to Apollo era packages (ALSEP). Development of such science payloads will thus require considerable optimization of instrument and subsystem design, packaging and integration for a variety of planetary surface environments in order to support solar system exploration fully. Our work supports this process through the incorporation of low temperature operational components and design strategies which radically minimize power, mass, and cost while maximizing the performance under extreme surface conditions that are in many cases more demanding than those routinely experienced by spacecraft in deep space. Chief instruments/instrument package candidates include those which could provide long-term monitoring of the surface and subsurface environments for fundamental science and human crew safety. The initial attempt to design a 10 instrument environmental monitoring package with a solar/battery based power system led to a package with a unacceptably large mass (500 kg) of which over half was battery mass. In phase 1, a factor of 5 reduction in mass was achieved, first through the introduction of high performance electronics capable of operating at far lower temperature and then through the use of innovative thermal balance strategies involving the use of multi-layer thin materials and gravity-assisted heat pipes. In phase 2, reported here, involves strategies such as universal incorporation of ULT/ULP digital and analog electronics, and distributed or non-conventionally packaged power systems. These strategies will be required to meet the far more challenging thermal requirements of operating through a normal 28 day diurnal cycle. The limited temperature range of efficient battery operation remains the largest obstacle.

Clark, P. E.↗

NASA NTRS2015

Mars: Periglacial Morphology and Implications for Future Landing Sites

At the Mars Phoenix landing site and in much of the Martian northern plains, there is ice-cemented ground beneath a layer of dry permafrost. Unlike most permafrost on Earth, though, this ice is not liquid at any time of year. However, in past epochs at higher obliquity the surface conditions during summer may have resulted in warmer conditions and possible melting. This situation indicates that the ice-cemented ground in the north polar plains is likely to be a candidate for the most recently habitable place on Mars as near-surface ice likely provided adequate water activity approximately 5 Myr ago. The high elevation Dry Valleys of Antarctica provide the best analog on Earth of Martian ground ice. These locations are the only places on Earth where ice-cemented ground is found beneath dry permafrost. The Dry Valleys are a hyper-arid polar desert environment and in locations above 1500 m elevation, such as University Valley, air temperatures do not exceed 0 C. Thus, similarly to Mars, liquid water is largely absent here and instead the hydrologic cycle is dominated by frozen ice and vapor phase processes such as sublimation. These conditions make the high elevation Dry Valleys a key Mars analog location where periglacial processes and geomorphic features can be studied in situ. This talk will focus on studies of University Valley as a Mars analog for periglacial morphology and ice stability. We will review a landing site selection study encompassing this information gleaned from the Antarctic terrestrial analog studies plus Mars spacecraft data analysis to identify candidate landing sites for a future mission to search for life on Mars.

Martian ground ice↗