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At least 307 records · Page 17

Radiation-Hardened GaN HEMT and Cell Design, Modeling, and Fabrication for Nuclear Instrumentation Applications

Recent advances in nuclear power generation technologies show great promise for efficient, safe generation of carbon-free power in the near future. Consequently, many new generation reactor designs are being pursued by government and industry groups, including both fission- and fusion-based technologies. Radiation- and temperature-tolerant sensor technology continues to advance, yet development of the electronics/instrumentation technologies suitable for these environments have fallen behind. Industry has adequately addressed harsh environment electronics needs for low earth orbit satellites, but the much more extreme conditions associated with electronics placed near or in a reactor core remain unaddressed. This project investigates the use of gallium nitride (GaN) circuit technology to address the unique needs for sensor interface electronics and communications in reactor environments. This report provides a summary of the first year’s project activities related to developing and optimizing devices and circuits for this GaN high electronic mobility transistor (HEMT) process. Activities reported include multiple analog and digital circuit designs simulated using custom Verilog-A models generated from measured GaN devices fabricated in the target process. Digital circuit designs included fundamental logic circuits such as an inverter, NAND, NOR, AND and OR gates, as well as a 5-stage ring oscillator. Each design was simulated using an open-source SPICE simulator, and an integrated circuit layout was produced of each design for use in future fabrication. Analog circuit designs focused on the fundamental building blocks to be used to construct sensor interface and communications circuits. These included current mirrors, matched differential pairs, and a Gilbert cell mixer design, each with an associated integrated circuit layout. Layout tools used for these designs included two open-source packages—KLayout and Magic—which were customized for specific use with the OSU GaN process layers. Design rules and preliminary device extraction capabilities were built for the Magic tool to enable device extraction and subsequent netlist generation for SPICE simulation. Finally, future research directions for year two are summarized. When the year-two directions are implemented, the project will be in position to advance the state of the art in electronics for near- or in-reactor sensor interfacing and communications.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗

Combined Mixed Potential Electrochemical Sensors and Artificial Neural Networks for the Quantificationand Identification of Methane in Natural Gas Emissions Monitoring

Sensors capable of quantifying methane concentration and discriminating between possible sources are needed for natural gas leak detection where multiple spatially overlapping sources including wetlands and agriculture may be present. We report on the fabrication by an additive manufacturing process of a four electrode La 0.87 Sr 0.13 CrO 3 , Indium Tin Oxide (In 2 O 3 90 wt%, SnO 2 10 wt%), Au, Pt mixed potential electrochemical sensor using yttria-stabilized zirconia (YSZ) as a solid electrolyte to natural gas detection. Artificial neural networks (ANNs) are used to automatically decode the possible source and concentration of methane. The ANNs trained on sensor data are capable of correctly discriminating between three sources of methane emissions from simulated mixtures of emissions from cattle, wetlands, or natural gas with >98% accuracy. Quantification error for methane in mixtures of CH 4 in air, CH 4 + NH3 in air, and simulated natural gas is less than 1.5% ppm when a two-temperature dataset is employed.

03 NATURAL GAS↗

LGAD-Based Silicon Sensors for 4D Detectors

Low-Gain Avalanche Diodes (LGAD) are a class of silicon sensors developed for the fast detection of Minimum Ionizing Particles (MIPs). The development was motivated by the need of resolving piled-up tracks of charged particles emerging from several vertexes originating from the same bunch-crossing in High-Energy Physics (HEP) collider experiments, which, however, are separated not only in space but also in time by a few tens of picoseconds. Built on thin silicon substrates and featuring an internal moderate gain, they provide fast signals for excellent timing performance, which are therefore useful to distinguish the different tracks. Unfortunately, this comes at the price of poor spatial resolution. To overcome this limitation, other families of LGAD-based silicon sensors which can deliver in the same substrate both excellent timing and spatial information are under development. Such devices are, to name a few, capacitively coupled LGADs (AC-LGAD), deep-junction LGADs (DJ-LGAD) and trench-isolated LGADs (TI-LGADs). These devices can be fabricated by even small-scale research-focused clean rooms for faster development within the scientific community. However, to scale up production, efforts towards integrating these sensor concepts in CMOS substrates, with the obvious advantage of the possibility of integrating part of the read-out electronics in the same substrate, have begun.

spatial resolution↗

Fabrication of Six Degrees-of-Freedom Hexflex Positioner With Integrated Strain Sensing Using Nonlithographically Based Microfabrication

In this study, a process flow is described for the low cost, flexible fabrication of metal micro-electromechanical systems (MEMS) with high performance integrated sensing. The process is capable of producing new designs in ≈1 week at an average unit cost of <$1 k/device even at batch sizes of ≈1–10, with expected sensing performance limits of about 135 dB over a 10 kHz sensor bandwidth. This is a ≈20× reduction in cost, ≈25× reduction in time, and potentially >30× increase in sensing dynamic range over comparable state-of-the-art compliant nanopositioners. The nonlithographically based microfabrication (NLBM) process is uniquely suited to create high performance nanopositioning architectures which are customizable to the positioning requirements of a range of nanoscale applications. These can significantly reduce the cost of nanomanufacturing research and development, as well as accelerate the development of new processes and the testing of fabrication process chains without excess capital investment. A six degrees-of-freedom (6DOF) flexural nanopositioner with integrated sensing for all 6DOF was fabricated using the newly developed process chain. The fabrication process was measured to have ≈30 μ m alignment. Sensor arm, flexure, and trace widths of 150 μ m, 150 μ m, and 800 μ m, respectively, were demonstrated. Process capabilities suggest lower bounds of 25 μ m, 50 μ m, and 100 μ m, respectively. Dynamic range sensing of 52 dB was demonstrated for the nanopositioner over a 10 kHz sensor bandwidth. Improvements are proposed to approach sensor performance of about 135 dB over a 10 kHz sensor bandwidth.

42 ENGINEERING↗

Synthesis of nickel selenide thin films for high performance all-solid-state asymmetric supercapacitors

As a significant semiconductor, nickel selenide shows enormous potential and extensive application prospects in the field of sensor, photocatalysis and supercapacitor. In this paper, nickel selenide (Ni 3 Se 2 , NiSe) thin films were successfully fabricated on stainless-steel sheet using a facile, effective electrodeposition technique. The morphologies, microstructures and chemical compositions of the thin films are characterized systematically. Electrochemical tests exhibit that the Ni3Se2 and NiSe possess high specific capacitance of 581.1 F/g and 1644.7 F/g, respectively. A flexible, all-solid-state asymmetric supercapacitor is assembled by utilizing NiSe film as positive electrode and activated carbon as negative electrode. The solid device delivers a high areal capacitance of 27.0 mF/cm 2 at the current density of 0.7 mA/cm 2 . Furthermore, the maximum volumetric energy density and power density of the NiSe//AC asymmetric SCs can achieve 0.26 mWh/cm 3 and 33.35 mW/cm 3 , respectively. The device shows robust cycling stability with 84.6% capacitance retention after 10000 cycles, outstanding flexibility and satisfactory mechanical stability. Moreover, two devices in series can light up a red light-emitting diode, which displayed great potential applications for energy storage.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Quantum Sensing in Micro-Architected Scaffolds

Quantum sensing with nitrogen-vacancy centers in diamond has emerged as a powerful tool for measuring diverse physical parameters, yet the versatility of these measurement approaches is often limited by the achievable layout and dimensionality of bulk-crystal platforms. Here, in this study, we demonstrate a versatile approach to creating designer quantum sensors by surface-functionalizing multiphoton lithography microstructures with NV-containing nanodiamonds. We showcase this capability by fabricating a 150 μm × 150 μm × 150 μm triply periodic minimal surface gyroid structure with millions of attached nanodiamonds. We demonstrate a means to volumetrically image these structures using a refractive index matching confocal imaging technique and extract ODMR spectra from 1.86 μm × 1.86 μm areas of highly concentrated nanodiamonds across a cross-section of the gyroid. Furthermore, the high density of sensing elements enables ensemble temperature measurements with a sensitivity of 0.548 ± 0.084 K/√Hz at 5 mW excitation power. This approach to creating quantum-enabled microarchitectures opens new possibilities for multimodal sensing in complex three-dimensional environments.

Materials science↗

Autonomous alignment and healing in multilayer soft electronics using immiscible dynamic polymers

Self-healing soft electronic and robotic devices can, like human skin, recover autonomously from damage. While current devices use a single type of dynamic polymer for all functional layers to ensure strong interlayer adhesion, this approach requires manual layer alignment. In this study, we used two dynamic polymers, which have immiscible backbones but identical dynamic bonds, to maintain interlayer adhesion while enabling autonomous realignment during healing. These dynamic polymers exhibit a weakly interpenetrating and adhesive interface, whose width is tunable. When multilayered polymer films are misaligned after damage, these structures autonomously realign during healing to minimize interfacial free energy. Finally, we fabricated devices with conductive, dielectric, and magnetic particles that functionally heal after damage, enabling thin-film pressure sensors, magnetically assembled soft robots, and underwater circuit assembly.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Templating Functional Materials Using Self-Assembled Block Copolymer Thin-Film for Nanodevices

The nanomorphologies and nanoarchitectures that can be synthesized using block copolymer (BCP) thin-film self-assembly have inspired a variety of new applications, which offer various advantages, such as, small device footprint, low operational power and enhanced device performance. Imperative for these applications, however, is the ability to transform these small polymeric patterns into useful inorganic structures. BCP-templated inorganic nanostructures have shown the potential for use as active materials in various electronic device applications, including, field-effect transistors, photodetectors, gas sensors and many more. This article reviews various strategies that have been implemented in the past decade to fabricate devices at nanoscale using block copolymer thin films.

Subramanian, Ashwanth↗

Magnetic Field Sensing via Acoustic Sensing Fiber with Metglas® 2605SC Cladding Wires

Magnetic field sensing has the potential to become necessary as a critical tool for long-term subsurface geophysical monitoring. The success of distributed fiber optic sensing for geophysical characterization provides a template for the development of next generation downhole magnetic sensors. In this study, Sentek Instrument’s picoDAS is coupled with a multi-material single mode optical fiber with Metglas® 2605SC cladding wire inclusions for magnetic field detection. The response of acoustic sensing fibers with one and two Metglas® 2605SC cladding wires was evaluated upon exposure to lateral AC magnetic fields. An improved response was demonstrated for a sensing fiber with in-cladding wire following thermal magnetic annealing (~400 °C) under a constant static transverse magnetic field (~200 μT). A minimal detectable magnetic field of ~500 nT was confirmed for a sensing fiber with two 10 μm cladding wires. The successful demonstration of a magnetic field sensing fiber with Metglas® cladding wires fabricated via traditional draw processes sets the stage for distributed measurements and joint inversion as a compliment to distributed fiber optic acoustic sensors.

Dejneka, Zach (ORCID:0000000179415708)↗

Characterization of Transition Edge Sensors for the Simons Observatory

The Simons Observatory is building both large (6 m) and small (0.5 m) aperture telescopes in the Atacama Desert in Chile to observe the cosmic microwave background CMB radiation with unprecedented sensitivity. Simons Observatory telescopes in total will use over 60,000 transition edge sensor (TES) detectors spanning center frequencies between 27 and 285 GHz and operating near 100 mK. TES devices have been fabricated for the Simons Observatory by NIST, Berkeley, and HYPRES/SeeQC corporation. Iterations of these devices have been tested cryogenically in order to inform the fabrication of further devices, which will culminate in the final TES designs to be deployed in the field. The detailed design specifications have been independently iterated at each fabrication facility for particular detector frequencies. We present test results for prototype devices, with emphasis on NIST high frequency detectors. A dilution refrigerator was used to achieve the required temperatures. Measurements were taken both with 4-lead resistance measurements and with a time-domain Superconducting Quantum Interference Device (SQUID) multiplexer system. The SQUID readout measurements include analysis of current versus voltage (IV) curves at various temperatures, square wave bias step measurements, and detector noise measurements. Lastly, normal resistance, superconducting critical temperature, saturation power, thermal and natural time constants, and thermal properties of the devices are extracted from these measurements.

47 OTHER INSTRUMENTATION↗

In situ characterization of the biological performance of a Francis turbine retrofitted with a modular guide vane

There are two strategies to lower overall project costs to an extent that will make many potential sustainable hydropower sites economically viable: (1) design standardized/modular components; (2) use advanced tools to reduce environmental evaluation costs. In this study an autonomous sensor device (Sensor Fish) was used to study a Francis turbine retrofitted with a modular guide vane. The median nadir pressures measured were 74.7, 66.6, and 56.6 kPaA for 90-, 190-, and 380-kW operating conditions respectively. These nadir pressures were compared to other Francis turbines studied using Sensor Fish and were found to be within the same range. The proportion of Sensor Fish releases with severe acceleration events (acceleration = 95G) was also investigated. The proportion ranged from 73 to 80% (runner region), 50 to 64% (guide vane region), and 9 to 28% (draft tube region), which was within the range of the other turbines used for comparison. The Sensor Fish testing that was conducted at Hurley Dam demonstrates that the modular guide vane that was retrofitted to the existing Francis turbine is potentially a suitable replacement that can provide biological performance similar to the guide vane used with other existing Francis turbines, but with the benefit of reduced fabrication costs.

13 HYDRO ENERGY↗

Embedment of sensors in ceramic structures

Ceramic materials such as silicon carbide (SiC) are attractive for many nuclear applications due to their ability to withstand high temperatures, which inherently improve the thermal efficiency of the power conversion cycle and can in some cases provide high-temperature process heat. SiC is particularly attractive because of its high-temperature strength retention, stability under neutron irradiation, and low neutron absorption. The TCR program has recently demonstrated the ability to fabricate monolithic SiC components with complex geometries using a binder jet additive manufacturing technique followed by densification using chemical vapor infiltration (CVI). This technology presents an opportunity to embed sensors within ceramic components at critical locations that allow for enhanced process monitoring and control of advanced nuclear energy systems. The challenges with embedding sensors in ceramic components are to identify appropriate materials that can survive the CVI process, remain embedded after cooling to room temperature, and be suitable for operation in a high-temperature nuclear environment. This report summarizes the sensors that are being considered for embedding within ceramics, the sensor embedding process, material compatibility studies, and characterization of the embedded components. Material selection is first guided by computational thermodynamics and is confirmed by embedding coupons and examining material interactions using electron microscopy. This work shows that a wide range of refractory metals, as well as certain fiber optic sensors, can be successfully embedded in 3D-printed SiC. Future work will involve testing of functional sensors including thermocouples and optical fiber-based, spatially distributed temperature/strain sensors.

36 MATERIALS SCIENCE↗

Toward Fully Soft and Multifunctional Shape Sensing via Optical Waveguide Arrays

For soft bodies, surface deformation and pressure provide proprioceptive and exteroceptive information, including body configuration, body compliance, and external forces. We develop a sheet sensor with a fully soft sensing surface that provides surface shape reconstruction using optical waveguide arrays. The waveguides are fabricated to achieve a tunable linear response to bi‐directional bending curvature, and the waveguide arrays are configured to differentiate between ambiguous shapes. We characterize the waveguide performance, relating curvature sensitivity to the core's surface roughness. Synergy of waveguide responses reduces the number of sensing elements required and achieves damage resilience. Using waveguide sensitivity to pressure, we also demonstrate feasibility for exteroception. We demonstrate the multifunctional sensing capability by wrapping the sheet around an upper arm, showcasing joint motion and external force sensing. Integrated into or applied onto surfaces of robotic or living systems, this design can be implemented in applications such as virtual reality, teleoperation, physical therapy, and soft robotics.

Yu, Qifan [Department of Mechanical Engineering Ma↗

TRUST Testing Procedure Documentation

The TRUST testbed was designed and fabricated to conduct vibration testing and validate the behavior of hyper-elastic foams in a pre-loaded condition. The main goals of this testbed design were to ensure symmetry, proper instrumentation alignment and mounting, simplified geometry to make the data analysis validation process more straightforward, and to apply and monitor the applied pre-load. Based off of the test parameters, a shaker system was purchased. The baseplate was designed to mount directly to the bolt holes provided on the top of the shaker table. It was determined that the specimens will be cylindrical and vary in thickness from 2-10mm. The baseplate riser, center-mass, and testbed cap were designed to be cylindrical to make alignment about the center axis more straightforward. It was determined to fabricate the parts previously mentioned using Aluminum 6061-T6 due to its stiffness in order to reduce the likelihood of the stiff material impacting the data being collected for the foam specimens. The design concept used to apply the pre-load to the testbed was a through bolt/nut configuration. A through hole was included in each piece of the testbed, specimens, and instrumentation large enough to allow for 1/8” clearance between the through bolt and each of these pieces. This was imperative to avoid causing friction and complicating the validation model. A load cell was then purchased and used to measure the pre-load being applied to the testbed. It was also required to collect data for 3 axes at 3 different locations 120° apart on the center-mass. This configuration was required to be placed on the cylindrical face and toward the top and bottom of the center-mass. Slots were milled out in the middle of each sensor block with tight tolerances for mounting each of the accelerometers at 120° apart. This same approach was taken to mount 2 accelerometers on the baseplate at 180° apart. Holes were milled out of the corners of each accelerometer mounting slot to relieve the corner and allow for a flat edge at the back of each slot. Sensor blocks were mounted into the center-mass using 6-32 bolts at the required locations. This initial testbed design was fabricated at the TA53 machine shop.

42 ENGINEERING↗

Scanning Probe Microscope to Map Thermal and Thermoelectric Properties of Combinatorial Materials

The combinatorial methodology offers a high-throughput process for developing radiation-resistant sensor materials for nuclear energy applications through the synthesis and screening of large numbers of compositions and processing conditions in a single process. The combinatorial materials fabrication coupled with an automated screening process enables us to identify the optimal materials composition and processing conditions that yield both desired properties and required irradiation resistance in the most efficient and economic manner. The report focuses on the development of scanning probe technique to map with high resolution the thermal conductivity, Seebeck coefficient and electrical conductivity of combinatory materials with gradient compositions, which has been a key challenge in combinatory materials science. The above three properties play important roles in many sensor materials for nuclear energy applications.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Additive Manufacturing of Energy Harvesting Material System for Active Wireless MEMS Sensors

Combustion systems make up a large sum of the world’s yearly energy production despite advances in renewable energy sources. Precise control of pressure and temperature in combustion chambers allows for lower carbon emissions, and overall higher efficiency. Wireless temperature and pressure sensors are critical for the operation of combustion chambers. Energy harvesters have emerged as a viable way to power wireless sensors when heat and mechanical energy are available. Lithium niobate (LNB), barium titanate (BTO), and lead zirconate titanate (PZT) pyroelectric ceramics were studied and fabricated through additive manufacturing (AM) for use as energy harvesting structures in combustion environments. The electric power generation potential of LNB and PZT ceramics was studied by varying the temperature from 50 to 60 °C and by introducing cyclic compression loads of 2000 N amplitude. It was found that thermal energy conversion had the highest output of 500 nW and that combined thermal and mechanical conversion did not increase the harvesting potential because of the competing contributions of both effects. Powder bed and slurry extrusion AM methods were used to fabricate BTO and PZT ceramic structures. Optimization of the powder-based binder jetting method produced BTO ceramics with a relative density of 36.77% a piezoelectric coefficient of 153 pC/N. The density of the ceramics increased up to 56% when increasing the saturation of binder in the powder to because of liquid phase sintering. Finally, PZT structures were manufactured through AM and fin features were added to the design to enhance the heat transfer along the material. The harvested power density of the flat samples was 3.643 μW/cm 3 and of the finned samples was 3.034 μW/cm3. This research paves the ways for the development of self-powered wireless sensors in critical areas of operation such as combustion.

01 COAL, LIGNITE, AND PEAT↗

Testing of an Optical Fiber--Based Gamma Thermometer in the High Flux Isotope Reactor Gamma Irradiation Facility

This report describes the design, thermal modeling, and gamma irradiation testing of an optical fiber–based gamma thermometer (OFBGT), which was irradiated in the High Flux Isotope Reactor (HFIR) Gamma Irradiation Facility (GIF). OFBGTs are a promising technology for application in nuclear reactors because they can provide a distributed measurement of gamma ray heating rate, unlike thermocouple-based gamma thermometers, which are fixed in-core sensors that can be used in boiling water reactors to calibrate local power range monitors. OFBGTs measure gamma ray heating rate by measuring the temperature difference between a pair of optical fibers; one fiber is in thermal contact with a heat sink (usually the reactor coolant), and the other is in thermal contact with a thermally isolated mass. The device can be calibrated with a heating wire within the thermal mass. The OFBGT that was designed and fabricated at Oak Ridge National Laboratory can measure distributed gamma ray heating rate over an effective measurement length of 61 cm, and the outer diameter of the sensor is 12.7 mm, giving the prototypical sensor design a relatively small footprint. The sensor housing is backfilled with Ar to ensure a well-predicted thermal response that is not affected by humidity or chemical interactions during operation. For calibration, the sensor design uses a Ni–Cr wire, which can be supplied with currents from 0 to 1 A to capture the wide range of potential gamma ray heating rates expected in HFIR’s spent fuel elements. The OFBGT was thermally modeled analytically and numerically; both models account for temperature-dependent thermal conductivities of the materials and show good agreement. The thermal response of the sensor inside spent HFIR fuel elements was simulated for times up to 1 year after discharge of the fuel element. Out-of-pile open-air tests indicated that the steady-state response of the sensor matches modeled results within experimental uncertainty. Calibration tests were performed using electrical heating in the HFIR spent fuel pool, above the fuel elements, to establish a relationship between the difference in spectral shift measured by optical fibers located inside and outside the OFBGT and the applied electrical heating. Subsequently, the OFBGT was placed within the the spent fuel element from HFIR cycle 501 to measure the spatial profile of the gamma heating rates. Results showed good agreement between the theoretical and measured gamma dose rate profiles, with maximum deviations of ~10% or less.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Development Status of the KIPM Detector Consortium

A kinetic inductance phonon-mediated detector is a calorimeter that uses kinetic inductance detectors (KIDs) to read out phonon signals from the device substrate. We have established a consortium comprising university and national lab groups dedicated to advancing the state of the art in these detectors, with the ultimate goal of designing a detector with sub-eV threshold on energy deposited in the substrate, enabling searches for both light dark matter and low-energy neutrino interactions. This consortium brings together experts in KID design, phonon and quasi-particle dynamics, and noise modeling, along with specialized fabrication facilities, test platforms, and unique calibration capabilities. Recently, our consortium has demonstrated a resolution on energy absorbed by the sensor of 2.1 eV, the current record for phonon-sensitive KIDs. However, due to ∼ 1% phonon collection efficiency, the overall detector resolution was limited to 320 eV. Finally, the current focus of the consortium is modeling and improving the phonon collection efficiency and implementing low-T c superconductors, both of which serve to improve the overall energy resolution and threshold of the detectors.

Temples, Dylan J. [Fermi National Accelerator Labo↗