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At least 307 records · Page 17

Estimate of conjugate gamma and gamma prime compositions in Ni-base superalloys

Approaches for estimating the composition of the matrix phase of alloys from the melt composition are reviewed. The first method is based on assigning essentially fixed stoichiometry to precipitating phases and is typified by PHACOMP. The second method uses analytical geometry to interpret phase diagrams and is applicable to a two-phase region of a six-component Ni-base system. The geometric method is also applicable to commercial Ni-base superalloys.

Dreshfield, R. L.↗

Estimation of conjugate gamma and gamma-prime compositions in Ni-base superalloys

To control the formation of unwanted phases, superalloy metallurgists have developed methods of estimating the composition of the matrix phase of alloys. That composition is then used to estimate the alloy's propensity toward sigma and other unwanted phase formations upon prolonged exposure to elevated temperatures in service. This paper reviews two approaches for estimating phase composition from the melt composition. One method is based on assigning essentially fixed stoichiometry to precipitating phases and is typified by 'PHACOMP'. The second method uses analytical geometry to interpret phase diagrams and is shown to be applicable to a two-phase region of a six-component Ni-base system. The geometric method is also shown to be applicable to commercial Ni-base superalloys.

Dreshfield, R. L.↗

Gamma-ray burst observations by the HEAO-3 high-resolution gamma-ray spectrometer

Special attention is given to two bursts occurring on November 16, 1979. Because of the close temporal coincidence of the two events, the possibility that both originated from a single celestial source is considered, as is the possibility that the scanning motion of HEAO-3 (nominal spin period, 20 min) was such as to exclude the first from the (approximately 30 deg FWHM) field of view of the germanium detectors and include the second. Directional data from the relative response of the shield pieces and earth occultation constraint are found to be consistent with this interpretation, and high-resolution spectral data from the second burst are discussed in this light. It is noted that recent unpublished analyses of long-baseline timing data from interplanetary spacecraft reveal that the response in the HEAO high-resolution detectors is probably earth albedo scattering. This, it is noted, can be an important systematic effect in low-earth orbit.

Wheaton, W. A.↗

Spectral and other physicochemical properties of submicron powders of hematite (alpha-Fe2O3), maghemite (gamma-Fe2O3), magnetite (Fe3O4), goethite (alpha-FeOOH), and lepidocrocite (gamma-FeOOH)

The spectral properties (0.35-2.20 microns) of submicron powders of hematite, maghemite, magnetite, goethite, and lepidocrocite are determined. Other physicochemical data are obtained for the powders in order to determine if deviations from stoichiometry occur due to their small particle size, to determine their state of chemical and phase purity, and to determine the physical characteristics of the individual powders. The physicochemical data obtained include mean particle diameter, discrete particle shape, chemical composition, crystallographic phase, magnetic parameters, and Moessbauer parameters. The positions of the spectral features for the hematite, maghemite, and magnetite powders are independent of temperature over the interval between about +20 and -110 C. For the goethite and lepidocrocite powders, a small shift of about 0.02 micron to shorter wavelengths is observed for some of the features after cooling to about -110 C. The spectral properties of the iron oxides and oxyhydroxides are important not only for understanding the basic physics and chemistry of the compounds but also for applications such as the remote sensing of the earth and Mars.

Morris, R. V.↗

The stability of lamellar gamma-gamma-prime structures

The stability of stress-annealed gamma/gamma-prime lamellar structures were investigated using three nickel-base single-crystal alloys (the NASAIR 100 and two similar alloys, E and F, containing 5 and 10 wt pct Co, respectively) stress-annealed at 1000 C to form lamellae perpendicular to the applied stress. The rate of the lamellar thickening under various thermal and creep exposures was examined by SEM. For unstressed aging at 1100 C, the lamellar structures of the NASAIR and the E alloys exhibited continuous but slow lamellar coarsening, whereas the lamellae of the alloy F showed pronounced thickening plus spheroidization. Resistance to lamellar thickening was correlated with high magnitudes of lattice mismatch, which promoted a more regular lamellar structure and a finer spacing of misfit dislocations. Specimens which were tension-annealed prior to compressive creep testing exhibited an earlier onset of tertiary creep in comparison with only heat-treated specimens. This was associated with accelerated lamellar coarsening in the stress-annealed specimens.

Nathal, M. V.↗

Timing analysis of low-energy gamma ray emission from galactic compact objects using the Gamma Ray Observatory

The principal goal of our phase 1 investigation was the development of techniques and data analysis tools for pulsar searches and timing. After the launch of the Compton Observatory, we received from the Burst and Transient Source Experiment (BATSE) team one day of discriminator large area (DISCLA) data for use in the development and testing of data analysis techniques. Using this first day of data for testing and optimizing our timing tools we detected four x-ray binary pulsars, Vela X-1, Cen X-3, 4U 0115+63, and GX 301-2. Subsequently, we received four more days of data, allowing us to test our timing tools with data from a variety of days. In summary, using the tools we developed based on the first day of data that we received, we have detected 8 pulsars in 5 days of data, or roughly one quarter of the approximately 30 known x-ray binary pulsars. In addition to the pulsars listed above, we detected GX 1+4, 4U 1626-67, OAO 1657-415, and Her X-1. Many of the data analysis tools that we developed have been ported to MSFC and are being used for the analysis of BATSE data. This appendix describes some of the timing tools and presents preliminary pulse period and phase profile results.

Prince, Thomas A.↗