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At least 289 records · Page 16

All sources NASA NTRS DOE OSTI

NASA NTRS1983

Toughening mechanism in elastometer-modified epoxy resins: Part 1

Several plaques of Epon 828, cured with piperidine, modified with hycar(r) CTBN 1300X8, Hycar(R) CTBN 1300X13, and Hycar(R) CTBN 1300x15, and in some cases modified with biphenol A (BPA), yielded properly toughened epoxies with rubber particle diameters ranging from 0.1 to 10 microns. Fracture toughness experiments indicate that toughness was more a function of rubber content than the rubber particle size. Tensile volumetric behavior of the near resin exhibits two regions: an initial region where the increase in volume strain was due to the Poisson's effect, and a second region where a slower rate of increase in volume strain was due to shear deformation. Tensile volumetric deformation of an elastomer-modified epoxy exhibits the same type of behavior to that of the neat resin at low rates ( 3.2x0.01 sec(-1)). But at very high strain rates, which correspond more closely to the strain rates at the crack tip, there exists an increase in volume strain beyond the Poisson's effect. TEM, SEM and OM studies indicate that the rubber particles had voided. When a thin section from the deformed region is viewed under crossed-polarized light, shear bands are seen connecting voided rubber particles. From this information cavitation and enhanced shear band formation is proposed as the toughening mechanism.

Yee, A. F.↗

NASA NTRS1983

Influence of the microstructure on the corrosion behavior of magnetron sputter-quenched amorphous metallic alloys

The microstructure and corrosion behavior of magnetron sputter deposited amorphous metallic films of (Mo6ORu40)82B18 under varying sputtering atmospheres have been investigated. The microstructural details and topology of the films have been studied by scanning electron microscopy and correlated with the deposition conditions. By reducing the pressure of pure argon gas, the characteristic features of rough surface and columnar growth full of vertical voids can be converted into a mirror-smooth finish with very dense deposits. Films deposited in the presence of O2 or N2 exhibit columnar structure with vertical voids. Film deposited in pure argon at low pressure show remarkably high corrosion resistance due to the formation of a uniform passive surface layer. The influence of the microstructure and surface texture on the corrosion behavior is discussed.

Thakoor, A. P.↗

NASA NTRS1984

Research in extragalactic astrophysics

The spatial distribution of clusters of galaxies and the large scale structure of the universe is investigated. Correlations in the spatial cluster distribution are much stronger than those seen for galaxies, and over scales much larger than previously anticipated. The following main studies are completed and published; (1) The determination of the correlation functions of rich clusters of galaxies, and its dependence on richness and other parameters. Very large scale structure exists in the universe, and rich clusters participate in this structure more efficiently than galaxies. (2) A complete catalog of superclusters, is determined. The selection criteria is that of a volume density enhancement, and is done in 3 dimensions. (3) The giant galaxy void in Bootes is found to be surrouned by rich, large superclusters from the catalog described above. (4) A very large scale void of rich clusters of galaxies is found in the study of the spatial distribution of rich clusters.

Bahcall, N.↗

NASA NTRS1986

Development of a Prosthesis for Urinary Control

Report describes development and marketing of prosthetic sphincter for urinary control. With prosthetic device, patients void bladder every 3 to 4 hours. Periodic voiding keeps bladder muscles exercised and healthy and avoids bladder infections and kidney damage.

Tenney, J. B.↗

NASA NTRS1984

Thermoplastic-carbon fiber hybrid yarn

Efforts were directed to develop processing methods to make carbon fiber/thermoplastic fiber preforms that are easy to handle and drapeable, and to consolidate them into low void content laminates. The objectives were attained with the development of the hybrid yarn concept; whereby, thermoplastic fiber can be intimately intermixed with carbon fiber into a hybrid yarn. This was demonstrated with the intermixing of Celion 3000 with a Celanese liquid crystal polymer fiber, polybutylene terepthalate fiber, or polyetheretherketone fiber. The intermixing of the thermoplastic matrix fiber and the reinforcing carbon fiber gives a preform that can be easily fabricated into laminates with low void content. Mechanical properties of the laminates were not optimized; however, initial results indicated properties typical of a thermoplastic/carbon fiber composites prepared by more conventional methods.

Ketterer, M. E.↗

NASA NTRS1984

NDE for heat engine ceramics

Radiographic, ultrasonic, and scanning laser acoustic microscopy (SLAM) techniques were used to characterize silicon nitride and silicon carbide MOR bars in various stages of fabrication. Conventional and microfocus x-ray techniques were found capable of detecting minute high density inclusions in as-received powders, green compacts, and fully densified specimens. Significant density gradients in sintered bars were observed by radiography, ultrasonic velocity, and SLAM. Ultrasonic attenuation was found sensitive to microstructural variations due to grain and void morphology and distribution. SLAM was also capable of detecting voids, inclusions, and cracks in finished test bars. It was determined that thermoacoustic microscopy techniques have promise for application to green and densified ceramics.

Klima, S. J.↗

NASA NTRS1985

Film and interstitial formation of metals in plasma-sprayed ceramics

A method is described to electrodeposit noble metals such as platinum and ordinary metals such as copper on and within plasma-sprayed ceramic materials and ceramic fiber materials. Low-density ceramic fiber bodies were vacuum impregnated with plating solution and attached to an electrode. Light micrographs illustrating the density and location of deposited materials are presented and discussed. Voids in the plasma-sprayed ceramic were filled with deposits that vary from spherical to lens-shaped circular and have particle size corresponding to the full range of void size. Multiple coatings of ceramic and metal can be sequenced.

Hendricks, R. C.↗

NASA NTRS1986

NDE of structural ceramics

Radiographic, ultrasonic, scanning laser acoustic microscopy (SLAM), and thermo-acoustic microscopy techniques were used to characterize silicon nitride and silicon carbide modulus-of-rupture test specimens in various stages of fabrication. Conventional and microfocus X-ray techniques were found capable of detecting minute high density inclusions in as-received powders, green compacts, and fully densified specimens. Significant density gradients in sintered bars were observed by radiography, ultrasonic velocity, and SLAM. Ultrasonic attenuation was found sensitive to microstructural variations due to grain and void morphology and distribution. SLAM was also capable of detecting voids, inclusions and cracks in finished test bars. Consideration is given to the potential for applying thermo-acoustic microscopy techniques to green and densified ceramics. The detection probability statistics and some limitations of radiography and SLAM also are discussed.

Klima, S. J.↗

NASA NTRS1985

Film and interstitial formation of metals in plasma-sprayed ceramics

Hendricks, R. C.↗

NASA NTRS1986

NDE of advanced ceramics

Radiographic, ultrasonic, and scanning laser acoustic microscopy (SLAM) techniques were used to characterize silicon nitride and silicon carbide modulus-of-rupture test specimens in various stages of fabrication. Conventional and microfocus X-ray techniques were found capable of detecting minute high-density inclusions in as-received powders, green compacts, and fully densified specimens. Significant density gradients in sintered bars were observed by radiography, ultrasonic velocity, and SLAM. Ultrasonic attenuation was found sensitive to microstructural variations due to grain and void morphology and distribution. SLAM was capable also of detecting voids, inclusions, and cracks in finished test bars. Consideration is given to the potential for applying thermoacoustic microscopy techniques to green and densified ceramics. Some limitations and the detection probability statistics of the aforementioned nondestructive evaluation (NDE) processes are also discussed.

Klima, S. J.↗

NASA NTRS1986

NDE of structural ceramics

Klima, S. J.↗

NASA NTRS1987

Processable Polyimides Containing ATBN Elastomers

Void-free moldings obtained without serious sacrifice in other properties. New synthesis produces high-temperture linear aromatic polyimide processed in imide form to yield tough, void-free components without serious sacrifice in other properties. Linear aromatic condensation polyimides are materials of prime choice for use as adhesives, composite matrix resins, films, coatings, and/or moldings where durability at temperatures as high as 200 to 300oC needed. Finding increasing use in aircraft and spacecraft applications.

St. Clair, Anne K.↗

NASA NTRS1987

Nondestructive evaluation of structural ceramics

A review is presented on research and development of techniques for nondestructive evaluation and characterization of advanced ceramics for heat engine applications. Highlighted in this review are Lewis Research Center efforts in microfocus radiography, scanning laser acoustic microscopy (SLAM), scanning acoustic microscopy (SAM), scanning electron acoustic microscopy (SEAM), and photoacoustic microscopy (PAM). The techniques were evaluated by applying them to research samples of green and sintered silicon nitride and silicon carbide in the form of modulus-of-rupture bars containing seeded voids. Probabilities of detection of voids were determined for diameters as small as 20 microns for microfucus radiography, SLAM, and SAM. Strengths and limitations of the techniques for ceramic applications are identified. Application of ultrasonics for characterizing ceramic microstructures is also discussed.

Klima, Stanley J.↗

NASA NTRS1986

An observational view of large scale structure

A summary of recent observations of galaxy clustering is presented, including a brief review of redshift maps and galaxy clustering statistics. Simple arguments are presented that argue the underlying mass fluctuations are most likely associated with a clustering scale no larger than that of individual galaxies. The acceleration of the local group from the comoving frame of the universe and its connection to the microwave dipole anisotropy are also discussed. A final topic for consideration is the existence of large voids and clusters, and whether they are consistent with Gaussian initial conditions. The extreme size and depth of the Bootes void, if real, do present a puzzle. Finally, future directions for observational study of large scale structure are discussed.

Davis, Marc↗

NASA NTRS1987

Plasma depletions in the Jovian magnetosphere - Evidence of transport and solar wind interaction

A series of plasma voids ('dropouts') was observed by the Plasma Science (PLS) experiment in Jupiter's magnetosphere during the Voyager 2 encounter with that planet. A reexamination of Voyager 2 data has led to the conclusion that the dropout phenomenon cannot be a manifestation of a plasma wake produced by Ganymede. Rather, the appearance of the dropouts is attributed to changes in the upstream solar wind conditions and the global state of the magnetosphere; the proximity of Voyager 2 to Ganymede at the time is considered to be coincidental. It is suggested that these dropouts are evidence of a state of 'bubbling' of the magnetosphere that alternates with 'laminar' states in which, as in the case of the Voyager 1 encounter with Jupiter, voids are not present and that these states correspond to different processes by which plasma is transported out of the system. The nature of these states is related to changes in the magnitude of the upstream solar wind ram pressure. In the bubbling state, this pressure is higher than in the laminar state and drives an intermittent instability. The analysis presented is one of the first attempts to introduce, in space physics, recently acquired theoretical notions of the physics of the finite-beta plasmas of which the Jovian magnetospheric plasma is an important example.

Mcnutt, Ralph L., Jr.↗

NASA NTRS1987

The spatial distribution of dwarf galaxies in the CfA slice of the universe

A complete (with the the exception of one) redshift sample of 58 galaxies in the Nilson catalog classified as dwarf, irregular, or Magellanic irregular is used to investigate the large-scale clustering properties of these low-surface brightness galaxies in the CfA slice of the universe (alpha in the range of 8-17 h, delta in the range of 26.5-32.5 deg). It is found that the low-surface brightness dwarf galaxies also lie on the structures delineated by the high-surface brightness normal galaxies and that they do not fill in the voids. This is inconsistent with a class of biased galaxy formation theories which predict that dwarf galaxies should be present everywhere, including the voids.

Thuan, Trinh X.↗

NASA NTRS1988

Spectrogoniometer for measuring planetary surface materials at small phase angles

This paper describes an instrument, termed spectrogoniometer, which was designed to measure the bidirectional reflectance properties of planetary surface analogs at very small phase angles. By using a pellicle beam splitter, a highly collimated laser light source, and a carefully aligned apparatus it was possible to measure the reflectance properties of geologic samples under any viewing geometry: the angles of incidence and emission ranging from 0 to 90 deg, and the azimuthal angle ranging from 0 to 360 deg. The results on the effect of porosity are demonstrated by comparing measurements on a compact sample (with a void space of 25 percent) and a fluffy sample (with a void space of 90 percent). The fluffy sample exhibited a 30-percent increase in intensity between 10 and 0 deg, whereas the compact sample exhibited only a 20-percent increase.

Buratti, Bonnie J.↗

NASA NTRS1988

Hydrogen effects in 001-line oriented nickel-base superalloy single crystals

The entry and subsequent interaction of hydrogen on the mechanical properties of the single crystal nickel-base superalloy CMSX-2 has been studied. Significant amounts of hydrogen were introduced by high temperature hydrogen charging in molten salts which led to an increased lattice parameter and microhardness and to a degradation in tensile elongation to failure whose extent scales with the depth of the hydrogenated zone. In this region a fracture mode change from a 111 to a 100 plane type also occurred. The values of the binding energy of hydrogen to solidification voids and the effective hydrogen pressure in the voids were estimated.

Baker, C. L.↗