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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 289 records · Page 16
All sourcesNASA NTRSDOE OSTI
DOE OSTI2024

Quadrupling the depairing current density in the iron-based superconductor SmFeAsO1–xHx

Abstract Iron-based 1111-type superconductors display high critical temperatures and relatively high critical current densities J c . The typical approach to increasing J c is to introduce defects to control dissipative vortex motion. However, when optimized, this approach is theoretically predicted to be limited to achieving a maximum J c of only ∼30% of the depairing current density J d , which depends on the coherence length and the penetration depth. Here we dramatically boost J c in SmFeAsO 1– x H x films using a thermodynamic approach aimed at increasing J d and incorporating vortex pinning centres. Specifically, we reduce the penetration depth, coherence length and critical field anisotropy by increasing the carrier density through high electron doping using H substitution. Remarkably, the quadrupled J d reaches 415 MA cm –2 , a value comparable to cuprates. Finally, by introducing defects using proton irradiation, we obtain high J c values in fields up to 25 T. We apply this method to other iron-based superconductors and achieve a similar enhancement of current densities.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2023

Electrically enhanced thermochemical cycles for hydrogen generation

In two-step metal-oxide (MO) solar thermochemical cycles, high temperature solar thermal energy is first converted to chemical energy in the form of a reduced MO. The reduced MO is then reoxidized in a second step with steam (or carbon dioxide) to produce hydrogen (or carbon monoxide) at a lower temperature. Solar thermochemical cycles of this type circumvent heat-to-electrical conversion required for electrochemical water splitting and promise high efficiencies. However, significant challenges remain to implementation. Ultra-high temperatures and efficiency-sapping low per-cycle conversion stand out as particularly difficult hurdles. Hybrid approaches utilizing both thermal and electrical energy provide some of the advantages of each, and can facilitate lower temperature operation and offer better per-pass utilization than thermochemical alone. However, early concepts for implementing the thermo-electrochemical approach introduced substantial new challenges including difficult separations, corrosive environments, and energy losses from large temperature swings and phase changes. We are currently investigating two different options for implementation. In the first, a MO that reduces at lower temperature is selected. As the reduced MO lacks the full thermodynamic driving force to effectively split water, the reaction is driven forward by an electrically-assisted proton-conducting membrane that separates and recovers hydrogen as it is produced. This approach produces a pure hydrogen stream, is mechanically simple, and has unique thermodynamic advantages. The second option seeks to more directly couple the electrical boost to the solid MO to drive either the reduction or oxidation step, or both, through the utilization of layered MO materials and advanced reactors. This approach could be applied to both water and carbon dioxide splitting. The results of process modeling and optimization will be presented, and progress towards demonstrating the concepts at the laboratory scale will be discussed.

08 HYDROGEN↗
DOE OSTI2020

Numerical Investigation of a Central Fuel Property Hypothesis Under Boosted Spark-Ignition Conditions

In the present work, a central fuel property hypothesis (CFPH), which states that fuel properties are sufficient to provide an indication of a fuel’s performance irrespective of its chemical composition, was numerically investigated. In particular, the objective of the study was to determine whether Research Octane Number (RON) and Motor Octane Number (MON), as fuel properties, are sufficient to describe a fuel’s knock-limited performance under boosted spark-ignition (SI) conditions within the framework of CFPH. To this end, four TPRF-bioblendstock surrogates having different compositions but matched RON (=98) and MON (=90), were first generated using a non-linear regression model based on artificial neural network (ANN). Additionally, three unconventional bioblendstocks were included in the analysis: di-isobutylene (DIB), isobutanol, and Anisole. Skeletal reaction mechanisms were generated for the TPRF-DIB, TPRF-isobutanol, and TPRF-anisole blends from a detailed kinetic mechanism. Thereafter, numerical simulations were performed for the fuel surrogates using the skeletal mechanisms and a virtual cooperative fuel research (CFR) engine model, under a representative boosted operating condition. In the computational fluid dynamics (CFD) model, the G-equation approach was employed to track the turbulent flame front and the well-stirred reactor model combined with the multi-zone binning strategy was used to capture auto-ignition in the end-gas. In addition, laminar flame speed (LFS) was tabulated for each blend as a function of pressure, temperature, and equivalence ratio a priori, and the lookup tables were used to prescribe laminar flame speed as an input to the G-equation model. Parametric spark timing sweeps were performed for each fuel blend to determine the corresponding knock-limited spark advance (KLSA) and 50% burn point (CA50) at the respective KLSA timing. It was observed that despite same RON, MON, and engine operating conditions, the TPRF-anisole blend exhibited markedly different knock-limited performance from the other three blends. This deviation from the octane index (OI) expectation was shown to be caused by differences in laminar flame speed. However, it was found that relatively large fuel-specific differences in LFS (>20%) would have to be present to cause any appreciable deviation from the OI framework. Otherwise, RON and MON would still be robust enough to predict a fuel’s knock-limited performance.

42 ENGINEERING↗
DOE OSTI2021

Boosting the use of bauxite residue (red mud) in cement - Production of an Fe-rich calciumsulfoaluminate-ferrite clinker and characterisation of the hydration

Highlights: • Incorporation of 35 wt% of bauxite residue for production of CSAF clinker • Thermochemical calculations as suitable tool for predicting phase assemblage • Hydration of the cement was found to be accelerated in contrast to other CSA cements. • High early compressive strengths of 40 MPa In the present work, calciumsulfoaluminate-ferrite clinker was produced using 35 wt% of bauxite residue in combination with alumina, clay, limestone and gypsum. At a temperature of 1300 °C, the hydraulic phases ye'elimite, ferrite and C{sub 2}S were formed. Computed thermochemical predictions were a significantly better match for the real mineralogy than modified Bogue equations. Hydration of the clinker led to the formation of ettringite and monosulfate, resulting in compressive strengths of 17 MPa after 28d. Compressive strengths of 40 MPa after 2d, and 28d-strengths exceeding 50 MPa, were reached in blends with 10 wt% of anhydrite. The strength development was due to the rapid formation of ettringite, mainly originating from ye'elimite, which did not convert to AFm phases and led to a compact microstructure. Only when the ye'elimite dissolution decreased, did the ferrite phase react. In pastes with additional sulfates, ferrite hydration led to the formation of ettringite and to hydrogarnet. Cement nomenclature is used in this work.{sup 1}.

36 MATERIALS SCIENCE↗
DOE OSTI2021

Surface enhanced performance of La 0.6 Sr 0.4 Co 0.2 Fe 0.8 O 3-δ cathodes by infiltration Pr-Ni-Mn-O progress

Herein the present study reports the enhancement of electrochemical oxygen reduction activity of porous La 0.6 Sr 0.4 Co 0.2 Fe 0.8 O 3–δ (LSCF) cathodes by coating a thin film of Pr-Ni-Mn oxide (PNM5) using a multi-step infiltration process. XRD examination reveals that PNM5 mainly contains a multiphase mixture of Pr 6 O 11 , PrNiO 3 , MnO and NiO. SEM morphology shows a thin PNM5 film and small particles are formed on the surface of LSCF backbone particles. Impedance spectrum analysis indicates that PNM5 infiltrated LSCF exhibits dramatically reduced polarization resistance (R p ), reaching R p of 0.244 Ω cm 2 at 973 K, which is one-half of the baseline LSCF cathode. The activation energy of LSCF cathodes infiltrated with PNM5 is 1.45 eV, slightly lower than the baseline LSCF cathode (1.77 eV). Distribution of relaxation time (DRT) function analysis shows PNM5 infiltration layer significantly promotes the oxygen reduction reaction (ORR) of cathode surface. With the increase in firing temperature, the total resistance increases and R p changes from ion transport to oxygen reduction reaction. Degradation rate of the PNM5-infiltrated LSCF is also lower, 0.02168% vs 0.07093% for the baseline LSCF over a 200-h period. A single cell testing indicated that the peak power density of the PNM5-infiltrated cell was increased by 140.66%. Overall, PNM5 could be a potential catalyst for boosting the performance of a commercial LSCF cathode for solid oxide fuel cells (SOFC).

36 MATERIALS SCIENCE↗
NASA NTRS1962

United States Space Explorations 1958

The film describes preparation and launch of five satellites and two space probes during 1958. On January 31, a Jupiter vehicle launched Explorer I into space. Data from this satellite was used to identify the van Allen radiation belts. On March 17, a Vanguard I rocket launched an Earth satellite with solar batteries. Data from the mission was used to determine that the Earth is slightly pear-shaped. On March 26, Explorer III was launched to further study the van Allen belts, micrometeoroid impacts, and internal and external temperatures. Explorer IV, launched on July 26, was intended to study radiation and temperature data. A lunar probe, ABLE I, was intended to measure radiation, magnetic fields of Earth and the Moon, density of micrometeoric matter, and internal temperatures. A four-stage rocket was used in the launch. However, a turbo-pump failed and the liquid oxygen pump stopped, resulting in a failed mission. On October 10, Pioneer I was launched by an ABLE vehicle. First and second stage velocity was less than desired and the probe did not leave Earth orbit. Attempts to attain escape velocity were unsuccessful. On December, a Jupiter boost vehicle was used to launch Juno II, with Pioneer III as the payload. Escape velocity was reached and Pioneer III left Earth's atmosphere. Failed launches, such as those of Vanguard boost vehicles and several Explorer satellites, also added to scientific knowledge.

Source record↗
DOE OSTI2021

Dynamics of Laterally Propagating Flames in X-Ray Bursts. II. Realistic Burning and Rotation

In this work, we continue to investigate two-dimensional laterally propagating flames in type I X-ray bursts using fully compressible hydrodynamics simulations. In the current study we relax previous approximations where we artificially boosted the flames. We now use more physically realistic reaction rates, thermal conductivities, and rotation rates, exploring the effects of neutron star rotation rate and thermal structure on the flame. We find that at lower rotation rates the flame becomes harder to ignite, whereas at higher rotation rates the nuclear burning is enhanced by increased confinement from the Coriolis force and the flame propagates steadily. At higher crustal temperatures, the flame moves more quickly and accelerates as it propagates through the atmosphere. If the temperature is too high, instead of a flame propagating across the surface the entire atmosphere burns uniformly. Our findings could have implications for the relationship between observed burst rise times and neutron star rotation and accretion rates. All of the software used for these simulations is freely available.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2025

NLR HPC Facility Power Usage Effectiveness (PUE) Data

Timeseries of Energy Systems Integration Facility (ESIF) Data Center Power Usage Effectiveness (PUE) Data provided in Parquet and compressed CSV formats Power Metrics Timeseries Fields: ts: Timestamp cooling_kw: Cooling (kilowatts) - Captures the power used by fans and pipe trace heaters associated with outdoor cooling equipment. The dedicated tower filter pump power is also captured as cooling load. energy_reuse: Energy Reuse Effectiveness hvac_kw: Heating, ventilation, and air conditioning (kilowatts) - Captures fan walls, fan coils that support the data center electrical rooms, and the make-up air unit. it_power_kw: IT equipment (kilowatts) - Captures power used by the IT equipment on the data center floor. plug_and_light_kw: Lights and utility plugs (kilowatts) - Captures power associated with the data center and dedicated mechanical room. The crank-case heater for the emergency standby generator is also captured as light and plug load. pue: Power Usage Effectiveness pump_kw: Pumps (kilowatts) - Captures power from pumps that move water in the data center Energy Recover Water loop and the Tower Water loops, and also captures power used by the boost pumps that circulate water through the fan walls. Note: The tower filter pump runs constantly to filter water from the data center cooling tower system, so 2.67 kilowatts are attributed to this pump and that is not reflected in this data field. day: Day of month Outside Weather Station Timeseries Fields: ts: Timestamp outside_air_humidity: Outside air humidity - Relative humidity percent outside_air_temp: Outside air temperature - Degrees Fahrenheit day: Day of month More detail: High-Performance Computing Data Center Power Usage Effectiveness

97 MATHEMATICS AND COMPUTING↗
DOE OSTI2024

Advanced silver sheathed 2212/Ag wire for high field magnets

Commercial High Temperature Superconductors (HTS) are all tape shaped (widths > 10 times thickness), because achieving useful current densities required them to be processed into this form, even though this also makes it more problematic to use them in some important coil types. Our product is based on 2212 (Bi2Sr2CaCu2O8) and it is the only HTS that can be processed into high current density wire forms that are similar to proven low temperature superconductors (LTS), while surpassing them in field generating and operating temperature capability. Required now are higher current density, lower cost and longer length 2212 wires to enable broad utilization where HTS tape usage is problematic. In Phase II we developed vital cost-lowering process technology elements and we test-processed longer wires with the standard commercial design as baseline and benchmark for our lower cost, higher quality and longer piece length wire advances. By initial application of Jc-boosting wire features, these wires exhibited significant performance increases. This Phase IIA program has now developed and qualified these technologies for lower cost, higher quality and longer piece length manufacturing in combination with current density-boosting wire features, paving the way to manufacturing capability that is essential for cost-effective commercial utilization of 2212 wire. Technical areas included automated, high uniformity powder packing, advanced drawing, annealing, lubricant cleaning and filament bundling, followed by integration of higher current density wire features and process variations.

17 WIND ENERGY↗
NASA NTRS2012

Optical Diagnostic Characterization of High-Power Hall Thruster Wear and Operation

Optical emission spectroscopy is employed to correlate BN insulator erosion with high-power Hall thruster operation. Specifically, actinometry leveraging excited xenon states is used to normalize the emission spectra of ground state boron as a function of thruster operating condition. Trends in the strength of the boron signal are correlated with thruster power, discharge voltage, and discharge current. In addition, the technique is demonstrated on metallic coupons embedded in the walls of the HiVHAc EM thruster. The OES technique captured the overall trend in the erosion of the coupons which boosts credibility in the method since there are no data to which to calibrate the erosion rates of high-power Hall thrusters. The boron signals are shown to trend linearly with discharge voltage for a fixed discharge current as expected. However, the boron signals of the higher-power NASA 300M and NASA 457Mv2 trend with discharge current and show an unexpectedly weak to inverse dependence on discharge voltage. Electron temperatures measured optically in the near-field plume of the thruster agree well with Langmuir probe data. However, the optical technique used to determine Te showed unacceptable sensitivity to the emission intensities. Near-field, single-frequency imaging of the xenon neutrals is also presented as a function of operating condition for the NASA 457 Mv2.

Williams, George J., Jr.↗
DOE OSTI2021

A machine learning aided interpretable model for rupture strength prediction in Fe-based martensitic and austenitic alloys

Abstract The class of 9–12% Cr ferritic-martensitic alloys (FMA) and austenitic stainless steels have received considerable attention due to their numerous applications in high temperature power generation industries. To design high strength steels with prolonged service life requires a thorough understanding of the long-term properties, e.g., creep rupture strength, rupture life, etc., as a function of the chemical composition and processing parameters that govern the microstructural characteristics. In this article, the creep rupture strength of both 9–12% Cr FMA and austenitic stainless steel has been parameterized using curated experimental datasets with a gradient boosting machine. The trained model has been cross validated against unseen test data and achieved high predictive performance in terms of correlation coefficient ( $$R^{2} > 0.98 $$ R 2 > 0.98 for 9–12% Cr FMA and $$R^{2} > 0.95 $$ R 2 > 0.95 for austenitic stainless steel) thus bypassing the need for additional comprehensive tensile test campaigns or physical theoretical calculations. Furthermore, the feature importance has been computed using the Shapley value analysis to understand the complex interplay of different features.

36 MATERIALS SCIENCE↗
DOE OSTI2024

Low-temperature etching of silicon oxide and silicon nitride with hydrogen fluoride

Etching of high aspect ratio features into alternating SiO 2 and SiN layers is an enabling technology for the manufacturing of 3D NAND flash memories. In this paper, we study a low-temperature or cryo plasma etch process, which utilizes HF gas together with other gas additives. Compared with a low-temperature process that uses separate fluorine and hydrogen gases, the etching rate of the SiO 2 /SiN stack doubles. Both materials etch faster with this so-called second generation cryo etch process. Pure HF plasma enhances the SiN etching rate, while SiO 2 requires an additional fluorine source such as PF 3 to etch meaningfully. Further, the insertion of H 2 O plasma steps into the second generation cryo etch process boosts the SiN etching rate by a factor of 2.4, while SiO 2 etches only 1.3 times faster. We observe a rate enhancing effect of H 2 O coadsorption in thermal etching experiments of SiN with HF. Ammonium fluorosilicate (AFS) plays a salient role in etching of SiN with HF with and without plasma. AFS appears weakened in the presence of H 2 O. Density functional theory calculations confirm the reduction of the bonding energy when NH 4 F in AFS is replaced by H 2 O.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2021

Fuel Effects on Advanced Compression Ignition Load Limits

In order to increase the efficiency of light-duty gasoline engines, the Co-Optimization of Fuels and Engines (Co-Optima) initiative from the U.S. Department of Energy is investigating multi-mode combustion strategies. Multi-mode combustion can be describe as using conventional spark-ignited combustion at high loads, and at the part-load operating conditions, various advanced compression ignition (ACI) strategies are being investigated to increase efficiency. Of particular interest to the Co-Optima initiative is the extent to which optimal fuel properties and compositions can enable higher efficiency ACI combustion over larger portions of the operating map. Extending the speed-load range of these ACI modes can enable greater part-load efficiency improvements for multi-mode combustion strategies. In this manuscript, we investigate fuel effects for six different fuels, including four with a research octane number (RON) of 98 and differing fuel chemistries, iso-octane, and a market representative E10 fuel, on the load limits for two different ACI strategies: spark-assisted compression ignition (SACI) and partial fuel stratification-gasoline compression ignition (PFS-GCI) operation. Experimental results show that limits to intake boosting limit high load operation for most fuels, but high smoke emissions for high particulate matter index (PMI) fuels under SACI conditions could also be a limitation. Contrastingly, low load is limited by combustion efficiency, but these effects have more pronounced variation with fuel chemistry for PFS-GCI than with SACI. Additional, distinct effects affecting autoignition timing and peak heat release at higher speeds were identified for fuels having different low temperature heat release (LTHR) propensities for both ACI modes.

33 ADVANCED PROPULSION SYSTEMS↗
DOE OSTI2025

Synergistic effects of Pd single atoms and nanoclusters boosting SnO 2 gas sensing performance

Tin(IV) oxide-supported Pd is a promising heterogenous catalyst for CO oxidation relevant for environmental cleanup reactions. In this study, an atomically dispersed Pd catalyst on SnO 2 (ADC Pd/SnO 2 ) hybrid material is successfully synthesized via a straightforward wet chemistry method and is found to exhibit superior performance toward CO sensing. Ex situ EXAFS analysis confirms the formation of single Pd atoms and small Pd nanoclusters stabilized on the SnO 2 (110) surface. Further, the material exhibits high efficiency in generating adsorbed O 2 - as well as high activity in catalyzing CO oxidation at low temperatures, resulting in exceptional sensitivity and selectivity toward CO in comparison to pure SnO 2 and Pd nanoparticles loaded on SnO 2 respectively. In situ FTIR measurements unravel CO adsorption kinetics on ADC Pd/SnO 2 under reaction conditions, and a possible sensing mechanism is put forth in which CO is transformed into CO 2 by reaction with active oxygen species; and concurrently, carbon-related species (bicarbonates and carbonates) are formed and decomposed into CO 2 .

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2021

Highly Perfluorinated Covalent Triazine Frameworks Derived from a Low-Temperature Ionothermal Approach Towards Enhanced CO 2 Electroreduction

Perfluorinated covalent triazine frameworks (F-CTFs) have shown unique features and attractive performance in separation and catalysis. However, state-of-art F-CTFs synthesized via the ZnCl 2 -promoted procedure have quite low fluorine contents due to C-F bond cleavage induced by chloride (a Lewis base) and the harsh conditions deployed (400-700 °C). Fabricating F-CTFs with high fluorine contents (> 30 wt%) remains challenging. Herein, we present a low-temperature ionothermal approach (275 °C) to prepare F-CTFs, which is achieved via polymerization of tetrafluoroterephthalonitrile (TFPN) over the Lewis superacids, e.g., zinc triflimide [Zn(NTf 2 ) 2 ] without side reactions. With low catalyst loading (equimolar), F-CTFs are afforded with high fluorine content (31 wt%), surface area up to 367 m 2 g -1 , and micropores around 1.1 nm. The highly hydrophobic F-CTF-1 exhibits good capability to boost electroreduction of CO 2 to CO, with faradaic efficiency of 95.7% at –0.8 V and high current density (–141 mA cm -2 ) surpassing most of the metal-free electrocatalysts.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2026

Enhanced Electrocatalytic and Cathode‐Electrolyte Interfacial Properties With a Pr‐Based Simple Perovskite/Ruddlesden‐Popper Nanocomposite Cathode in Protonic Ceramic Fuel Cells

The sluggish kinetics and poor stability of the oxygen reduction reaction (ORR) remain the primary bottleneck for achieving high performance in protonic ceramic fuel cells (PCFCs) at intermediate temperatures (400–650°C). In this work, a Pr-based nanocomposite cathode comprised of simple perovskite phase (PrNi 0.7 Co 0.3 O 3-δ ) and Ruddlesden-Popper phase (Co-doped Pr 4 Ni 3 O 10+δ ) is developed. Although PrNi 0.7 Co 0.3 O 3-δ solely stands as a good cathode with facile proton transfer, combining the superior catalytic activity against oxygen on the Ruddlesden-Popper phase boosts the ORR performance further. The designed nanocomposite cathode outperforms the simple perovskite cathode, attributed to enhanced oxygen absorption and surface diffusion with the Ruddlesden-Popper phase. A precursor-based cathode deposition technique is also developed to achieve cathode grain sizes of ∼100 nm. A single cell with the nanocomposite cathode delivers a peak power density of 1.38 W cm −2 at 650°C, among the highest in reported PCFCs with Pr-based cathodes, with a small degradation rate of 0.145 mV h −1 during 250 h stability test. Further investigation of cathode-electrolyte interface revealed interfacial PrO 2 phase formation, promoted by abundant Pr 6 O 11 in the nanocomposite precursor powder, thereby improving both ohmic resistance and stability. These findings highlight the effectiveness of the nanocomposite cathode and underscore its advantages on interfacial properties.

08 - HYDROGEN↗
DOE OSTI2020

Evaluation of short-term initial performance of a “Molekule Air” portable air cleaner

The aim of this project was to evaluate and characterize the performance of a MOLEKULE AIR air cleaner unit. The testing protocol comprised the evaluation of an unused Molekule Air unit operating at maximum (“boost” setting) fan speed setting. The device was tested over initial short-term periods of 70-80 h of continuous operation. The tested air cleaner was challenged in separate experiments with a well-characterized mixture of volatile organic compounds (VOCs), and with ozone. All tests were performed at realistic pollutant levels in a 20-m 3 environmental stainless-steel chamber. Variables controlled and measured in this study included the chamber temperature, relative humidity, the composition and concentration of the challenge VOCs, and the concentrations of ozone. Potential formation of byproducts was also investigated to assess the overall performance.

47 OTHER INSTRUMENTATION↗
DOE OSTI2025

Single-atom Zr promoter boosts oxygen activation on ceria-supported Pt catalysts

Activation of surface lattice oxygen and chemisorbed oxygen on catalyst surfaces constitutes a pivotal step in heterogeneous oxidative catalysis. Herein, we report a strategy for enhancing oxygen activation by rational design of catalysts with single-atom promoters. Single-site Zr species in CeO 2 (Zr 1 -CeO 2 ) are synthesized using the atom-trapping method. The Zr 1 -CeO 2 -supported Pt catalyst exhibits enhanced catalytic performance over the CeO 2 -supported Pt catalyst in the oxidation of CO, C 3 H 8 , and C 3 H 6 , achieving significantly lower T 50 values (temperature required to reach 50% conversion). This enhanced catalytic activity is attributed to the formation of an asymmetric Zr 1 -O-Pt 1 structure, which favors the activation of the adjacent surface lattice oxygen and chemisorbed molecular oxygen. This work exemplifies that incorporating single-site atoms into oxide support facilitates oxygen activation, providing new insights into the role of atomically dispersed promoters in heterogeneous catalysis.

Science & Technology - Other Topics↗