Advances in High-Resolution Radiation Detection Using 4H-SiC Epitaxial Layer Devices
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99 GENERAL AND MISCELLANEOUS↗
SEARCH · Engineering Papers
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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.
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Wireless Passive Ceramic Sensor for Far-Field Temperature Measurement at High Temperatures
A passive wireless high-temperature sensor for far-field applications was developed for stable temperature sensing up to 1000 °C. The goal is to leverage the properties of electroceramic materials, including adequate electrical conductivity, high-temperature resilience, and chemical stability in harsh environments. Initial sensors were fabricated using Ag for operation to 600 °C to achieve a baseline understanding of temperature sensing principles using patch antenna designs. Fabrication then followed with higher temperature sensors made from (In, Sn) O2 (ITO) for evaluation up to 1000 °C. A patch antenna was modeled in ANSYS HFSS to operate in a high-frequency region (2.5–3.5 GHz) within a 50 × 50 mm2 confined geometric area using characteristic material properties. The sensor was fabricated on Al2O3 using screen printing methods and then sintered at 700 °C for Ag and 1200 °C for ITO in an ambient atmosphere. Sensors were evaluated at 600 °C for Ag and 1000 °C for ITO and analyzed at set interrogating distances up to 0.75 m using ultra-wideband slot antennas to collect scattering parameters. The sensitivity (average change in resonant frequency with respect to temperature) from 50 to 1000 °C was between 22 and 62 kHz/°C which decreased as interrogating distances reached 0.75 m.
47 OTHER INSTRUMENTATION↗
Scheimpflug LIDAR for Gas Sensing at Elevated Temperatures
Localized operating conditions inside boilers, heat recovery steam generators, or other large thermal systems have a huge impact on the efficiency, environmental performance, and lifetime of components. It is extremely difficult to measure species accurately within these systems due to the high temperatures and harsh environments, locally oxidizing or reducing atmospheres, ash, other particulates, and other damaging chemical species. Physical probes quickly suffer damage and are rendered nonfunctional. This work has attempted to adapt the measurement approach based on Scheimpflug light detection and ranging (S-LIDAR) for the remote sensing of gas species inside the high-temperature boiler environment. For a proof-of-concept, the detection of Raman signals of N 2 , O 2 , and CO 2 and their behavior with increasing temperature have been presented.
47 OTHER INSTRUMENTATION↗
Progress in Understanding the Origins of Excellent Corrosion Resistance in Metallic Alloys: From Binary Polycrystalline Alloys to Metallic Glasses and High Entropy Alloys
Some of the factors responsible for good corrosion resistance of select polycrystalline and emerging alloys in chloride solutions are discussed with a goal of providing some perspectives on the current status and future directions. Traditional metallic glass alloys, single phase high entropy alloys (HEAs), early metallic glasses, and high entropy metallic glasses are all emerging corrosion-resistant alloys (CRAs) that utilize traditional strategies for improved corrosion resistance as well as take advantage of some other novel beneficial attributes. These materials enjoy many degrees of freedom as far as choice of both composition and structure, providing great flexibility in the pursuit of superior corrosion resistance. The new materials depart from classical solvent-solute type polycrystalline binary or ternary alloys. Thus, such emerging materials provide significant opportunities to achieve even greater improvements in corrosion resistance in harsh environments. Several examples of the unique corrosion properties of selected materials in the context of modern theories of corrosion are discussed herein. Discussion is restricted to solid-solution binary or ternary polycrystalline alloys, several metallic glass alloys, and single phase HEAs. A common feature of many CRAs is that composition and microstructure often affect both passivity and resistance to localized corrosion that can be divided into initiation, stabilization, and propagation stages. Enormous complexities in protective oxide structures and chemistries and the large number of combinatorial possibilities in newer materials such as HEAs preclude trial-and-error approaches and perhaps even combinatorial experimental design. Computational materials methodologies will be required in the search for new corrosion-resistant alloys in these material classes. The search must consider the best scientific insights available regarding how major and minor alloy additions, as well as various microstructural attributes, contribute to corrosion mitigation. Additional scientific insights, as they emerge, will enable choices beyond the reliance on high concentrations of alloying elements that are known to affect passivity breakdown and pit stabilization. A challenge is to connect the “basic attributes” of an alloy with its properties. The strength of this connection will likely require new scientific principles enabling deep multiphysics insights in order to link feature(s) such as composition and metallurgical phases to the desired corrosion properties. Application of data informatics will likely also play a role given the plethora of variables that are important in corrosion and the difficulty in assessing all relationships. Here, the opportunity exists to accelerate the design of emerging materials for high corrosion resistance.
36 MATERIALS SCIENCE↗
Data Associated with "Identifying Suitable Front Contacts for High-Efficiency Cd(Se,Te) Solar Cells on Space-Qualified Cover Glass"
This is data associated with the publication " Identifying Suitable Front Contacts for High-Efficiency Cd(Se,Te) Solar Cells on Space-Qualified Cover Glass " by Aesha P. Patel, Ryan Muzzio, Matthew R. Young, Robert Morrissey, Suresh Chaulagain, B. Edward Sartor, Prabodika N. Kaluarachchi, Christian Velez, Joshua A. Brown, Joel N. Duenow, Stephen Glynn, Michael J. Heben, Zhaoning Song, Nikolas J. Podraza, Adam B. Phillips, Randy J. Ellingson, Matthew O. Reese. All data associated with each figure in the manuscript and supplementary should be available in this dataset. A readme file is also included to provide some guidance. Abstract: Deployment of photovoltaics in space requires devices that combine high-efficiency, low areal mass, and resilience to harsh environments. Historically, high-efficiency multijunction III–V materials have dominated space power systems; however, their high cost and limited manufacturing throughput motivate the exploration of scalable alternatives. While CdTe-based thin-film photovoltaics offer an attractive option, their performance on non-conventional substrates can suffer from front-contact instability under higher-temperature processing. Here, the role of front-contact chemistry in limiting cell performance is investigated using CdTe-based devices fabricated on 150 μm thick Ceria-doped space-qualified 0214 Corning glass. A matrix of four transparent conducting oxides (TCOs: CTO, AZO, ITO, IZO) combined with two n-type emitters (MZO, IGO) reveals chemical stability at the front interface—rather than absorber composition alone—governs recombination losses, voltage deficits, and device reproducibility. Chemically stable front-contact combinations suppress elemental diffusion and interfacial degradation, resulting in significantly improved carrier lifetimes and junction quality. These insights are validated through record-certified Cd(Se,Te) cell efficiencies of 18.4% under AM1.5G and 16.2% under AM0 illumination on ultra-thin glass. Beyond CdTe, this work provides a general framework for the rational selection of TCO/emitter interfaces in superstrate thin-film photovoltaics, including emerging technologies like metal halide perovskites, while enabling high-efficiency, lightweight photovoltaics for space applications.
14 SOLAR ENERGY↗
Planned Steady State Irradiation of Characterized Instruments for Nuclear Thermal Rockets Using In-Pile Experiment Apparatus
The development of nuclear rocket technology is critical for the further exploration of extraterrestrial bodies. Nuclear rockets are capable of providing various advantages over current chemical rockets. However, the harsh environment provides a number of challenges regarding instrument performance. Temperature extremes, radiation (reactor and space), and the inability to conduct traditional maintenance activities can lead to a severe degradation in instrument performance. To better understand the effects of radiation on instrumentation, an irradiation campaign has been designed to test a set of instruments provided by a collaborator in the aerospace industry. Details concerning pre-irradiation performance are provided for a future comparison to the irradiated performance. Additionally, the design of the irradiation test is described in detail.
Floyd, Dan↗
Influence on Structural Loading of a Wave Energy Converter by Controlling Variable-Geometry Components and the Power Take-Off: Preprint
Oceans are a harsh environment and can impose significant loads on deployed structures. Deployment of wave energy converters (WECs) faces a design challenge with apparently contradictory goals. A WEC should be designed to maximize the energy absorbed while ensuring the operating wave condition does not exceed the failure limits of the device itself. Therefore, the loads endured by the support structure are a design constraint for the system. Adaptability to different sea states is, therefore, highly desirable. This work uses a WEC-Sim model of a Variable Geometry Oscillating Wave Energy Converter (VGOSWEC) mounted on a support structure simulated under different wave scenarios. A VGOSWEC resembles a paddle pitching about a fixed hinge perpendicular to the incoming waves-fronts. Therefore, the hinge experiences loads perpendicular to its axis as it maintains its position. The geometry of the VGOSWEC was varied by opening a series of controllable flaps on the pitching paddle when the structure experiences threshold loads. Since opening the flaps lets the waves transmit through the paddle, it is hypothesized that opening the flaps should result in load shedding at the base of the support structure. This load shedding is achieved by reducing the moments about the hinge axis. This work compares the hydrodynamic coefficients, natural periods, and Response Amplitude Operators (RAOs) from completely closed to completely open configurations of the controllable flaps. These comparisons quantify the effects of letting the waves transmit through the VGOSWEC. This work shows that the completely open configuration can reduce the pitch and surge loads on the base of the support structure by as much as 80%. It was observed that at the paddle's resonance frequency, the loads on the structure increased substantially. This increase in loads can be mitigated by a rotational Power Take-off (PTO) damping about the hinge axis. Changing the rotational PTO damping was identified as an additional design parameter that can be used to control the loads experienced by the WEC's support structure.
fixed and floating structures↗
INVESTIGATION OF TURBULENT JETS, SPRAYS, AND SUPERCRITICAL MIXING BY TIME RESOLVED RAINBOW SCHLIEREN DEFLECTOMETRY
As technological advancements have enabled higher efficiency compression ignition (CI) engines (diesel engines) by operating at higher pressures and temperatures, the mechanisms of fuel-air mixing are postulated to change. Thus, there is a greater need for experimental data to develop and verify new phenomena. However, the fast time scales and harsh environments associated with CI engines present many experimental difficulties and requires high quality non-intrusive diagnostics to obtain useful data. The diagnostics itself must be validated prior to its implementation in an engine environment. The purpose of this research is to advance rainbow schlieren deflectometry (RSD) to study turbulent fuel sprays including the effects of supercritical mixing in CI engine environments. This objective is met by developing and applying quantitative RSD, for the first time, to three separate aspects of fuel sprays: 1) turbulent mixing, 2) phase boundaries, and 3) non-ideal gas mixing. First, quantitative RSD is demonstrated for turbulent mixing in a canonical helium jet. Rayleigh scattering data in the literature is used to validate the concentration measurements obtained by RSD. The results also provide explanations for phenomena occurring in the helium jet and provide data not yet present in the literature. Second, RSD is applied to high pressure multi-phase fuel sprays and new methodologies are developed to distinguish the liquid region from the vapor region and to quantify the in-between region on a probabilistic basis. Isolating liquid and vapor regions generally requires two separate diagnostics, e.g., Mie scattering (liquid region) and Rayleigh scattering (vapor region). However, the results of this study demonstrate that RSD can be used as a single diagnostic to measure both liquid and vapor boundaries. Third, the optical-to-thermodynamic relations associated with refrac-tometry are investigated under non-ideal gas mixing conditions to develop a generalized relationship valid for both ideal or non-ideal gas mixing. The last part of this research develops the theoretical tools to understand and experimentally realize supercritical mixing at diesel conditions. Guided by the theoretical analysis, RSD is applied to compare supercritical versus transcritical mixing at CI conditions using a constant pressure test rig. It is found that while fully supercritical mixing ers benefits in diesel engines, i.e, faster mixing times (50% higher velocities), the absence of droplets which cause high levels of particulate emissions, etc., it would be difficult to achieve in practice because of the requirements of fuels with low critical temperature and/or substantial fuel preheating.
02 PETROLEUM↗
Photovoltaic array for a power-by-light system
A hybrid-integrated series/parallel-connected photovoltaic diode array employs 10s-to-100s of single-wavelength III-V compound semiconductor photodiodes in an array bonded onto a transparent optical plate through which the array is illuminated by monochromatic light. The power-by-light system receiver enables high-voltage, up to 1000s of volts, optical transmission of power to remote electrical systems in harsh environments.
Vawter, Gregory A.↗
Sub-nanosecond RF synchronization for MIMO software defined radio sensor networks
This disclosure presents distributed and decentralized synchronization for wireless transceivers. The disclosed system, device, and method achieve sub-nanosecond synchronization using low-cost commercial off the shelf software defined radios. By providing a decentralized mechanism that does not rely on a hierarchical master-slave structure, networks constructed as disclosed are robust to sensor drop-out in contested or harsh environments. Such networks may be used to create phased array radars and communication systems without requiring wired connections to distribute a common clock or local oscillator reference.
Moghaddam, Mahta↗
Inaugural Molten Salt Technologies Workshop Powering the Future
The inaugural “Molten Salt Technologies – Powering the Future” Workshop marked a significant convergence of minds from diverse industries, each harnessing molten-salt technologies in innovative ways. Participants from sectors such as solar, geothermal, and advanced nuclear energy, as well as those involved in cutting-edge applications like thermal transport and rare-earth metals extraction, gathered to discuss their shared technical challenges and opportunities. Industry leaders in metal extraction and recycling, alongside experts in high-temperature sensor technology and advanced material manufacturing, also brought their unique perspectives to the table. This workshop served as a crucial platform for these varied industries to delve into the engineering intricacies that molten salt technologies entail. Common challenges such as understanding the thermophysical properties of salts, tackling corrosion mechanisms in harsh environments, and enhancing material resilience under extreme conditions were at the forefront of discussions. These technical sessions highlighted the critical need for cross-industry collaboration to address issues like salt life-cycle process engineering, impurity mitigation, and the development of durable, high-performance materials. By bringing together academia, industry, and representatives from national laboratories and the U.S. Department of Energy (DOE), the workshop facilitated a rich exchange of knowledge and experiences. This interaction not only fostered new partnerships but also strengthened the network among existing collaborators, setting the stage for joint solutions to the complex problems faced by all sectors using molten salt technologies. The event underscored the importance of collaborative efforts in overcoming common engineering challenges and advancing the application of molten-salt technologies across various industries. The workshop not only provided an essential forum for networking and idea exchange but also highlighted the collective drive towards innovative solutions that could benefit multiple fields.
Department of Energy↗
Inaugural Molten Salt Technologies Workshop Powering the Future
The inaugural “Molten Salt Technologies – Powering the Future” Workshop marked a significant convergence of minds from diverse industries, each harnessing molten-salt technologies in innovative ways. Participants from sectors such as solar, geothermal, and advanced nuclear energy, as well as those involved in cutting-edge applications like thermal transport and rare-earth metals extraction, gathered to discuss their shared technical challenges and opportunities. Industry leaders in metal extraction and recycling, alongside experts in high-temperature sensor technology and advanced material manufacturing, also brought their unique perspectives to the table. This workshop served as a crucial platform for these varied industries to delve into the engineering intricacies that molten salt technologies entail. Common challenges such as understanding the thermophysical properties of salts, tackling corrosion mechanisms in harsh environments, and enhancing material resilience under extreme conditions were at the forefront of discussions. These technical sessions highlighted the critical need for cross-industry collaboration to address issues like salt life-cycle process engineering, impurity mitigation, and the development of durable, high-performance materials. By bringing together academia, industry, and representatives from national laboratories and the U.S. Department of Energy (DOE), the workshop facilitated a rich exchange of knowledge and experiences. This interaction not only fostered new partnerships but also strengthened the network among existing collaborators, setting the stage for joint solutions to the complex problems faced by all sectors using molten salt technologies. The event underscored the importance of collaborative efforts in overcoming common engineering challenges and advancing the application of molten-salt technologies across various industries. The workshop not only provided an essential forum for networking and idea exchange but also highlighted the collective drive towards innovative solutions that could benefit multiple fields.
Department of Energy↗
Novel Design and Fabrication of a High Frequency Transient Heat Flux Sensor for Use in an RDE
Rotating detonation engine (RDE) combustion systems have been a topic of interest in the pressure gain combustion community for their benefits over traditional gas turbine engine combustors. However, cooling requirements for these engines are significantly higher and less predictable than non-detonating engines. To understand the high-speed heat transfer dynamics inside an RDE, a novel, high-frequency heat flux gage is presented. This study aims to design a robust, single-sided sensor that can withstand the high temperature and harsh environment of an RDE for extended durations. Sensor bench testing is performed using a hot plate as a heat source, and the sensor response is compared to a finite-element analysis (FEA) model. The sensor response is then tested inside a water-cooled RDE and the wall heat flux is compared to calorimetry data.
rotating detonation engines↗
Non-Destructive Plutonium Assay in Pyroprocessing Bulk Materials with a 3D Boron-Coated-Straw Detector Array
Assessment of plutonium content through all the processing steps is needed and is a challenging task. While several destructive assay methods have been developed for nuclear material accountability, a nondestructive assay (NDA) system for the assessment of plutonium in bulk materials is still needed. This system should withstand pyroprocessing harsh environments and have consistent sensitivity and accuracy despite different fuel form factors. We aim to enable the accurate assessment of the plutonium content of nuclear material during pyroprocessing to improve the separation process and enhance its proliferation resistance. We plan to achieve this goal by developing and demonstrating a new 3D boron-coated-straw neutron detector array (3D-BCSDA) with high efficiency and spatial resolution.
11 - NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗
Harnessing Quantum Information Science for Enhancing Sensors in Harsh Fossil Energy Environments
The main goals of this project are to utilize real-time quantum dynamics simulations and quantum optimal control algorithms to (1) harness near-surface nitrogen vacancy (NV) centers to detect chemical analytes in harsh fossil energy environments, and (2) design optimally constructed electromagnetic fields for initializing these near-surface NV center spins for efficient sensor performance and detectivity.
20 FOSSIL-FUELED POWER PLANTS↗
Behavior of copper‐containing high‐entropy alloys in harsh metal‐dusting environments
Abstract Metal dusting is still an unresolved issue at high temperatures. Currently, two material‐related strategies to mitigate metal dusting are described in the literature. On the one hand, highly alloyed materials are used, which contain large amounts of protective oxide‐forming elements, such as Cr, Al, and Si. The second mitigation strategy is based on inhibiting the catalytic effect of Fe, Ni, and Co. These elements all strongly catalyze the formation of solid carbon from the gas phase. Combining the catalytic protection of Cu alloying for metal dusting with protection by a classical alumina/chromia barrier is a native feature that high‐entropy alloys (HEAs) can offer. In this study, the behavior of different equiatomic HEAs with and without Al and/or Cu are studied when exposed at 620°C in a highly aggressive metal‐dusting environment.
36 MATERIALS SCIENCE↗
Improved Manufacturing Techniques Waveguide Temperature Sensors for Measurements in Harsh and Corrosive Environments -Phase I Final Report
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03 NATURAL GAS↗
Optical Fiber Sensors Capable of Monitoring Hydrogen in the Subsurface Hydrogen Storage Environment
Subsurface hydrogen storage is a cost-effective and environmentally friendly storage option in a large quantity. Hydrogen would be stored in subsurface storage reservoirs at high temperature/pressure under very humid condition. Monitoring hydrogen concentration in those harsh storage environments is crucial to ensure the integrity and safety of the hydrogen storage infrastructure. Thus, this project focuses on the development of optical fiber hydrogen sensors capable of monitoring hydrogen in the harsh environments that are representative of underground storage conditions. The optical fiber hydrogen sensor developed at NETL consists of a palladium-based sensing film with a filter layer which minimizes the environmental impacts on hydrogen sensing. The developed sensor has demonstrated significant improvement on hydrogen sensing at 80℃ under high humidity condition (99% RH) without the baseline drift. The hydrogen sensor also showed negligible cross-sensitivity to CO2 and CH4 which would be present as a cushion gas inside the underground hydrogen storage reservoir. Moreover, the sensor has demonstrated the stable monitoring of hydrogen concentration at high pressure (1000 psi) and 80 ℃ in the presence of biological samples. The optical fiber hydrogen sensor developed would enable reliable monitoring of hydrogen concentration in subsurface hydrogen storage facilities.
Kim, Daejin↗