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At least 289 records · Page 16
All sourcesNASA NTRSDOE OSTI
NASA NTRS1979

Adherence of sputtered titanium carbides

Sputtered coatings of the refractory metal carbides are of great interest for applications where hard wear-resistant materials are desired. The usefulness of sputtered refractory carbides is often limited, in practice, by spalling or interfacial separation. In this work improvements in the adherence of refractory carbides on iron, nickel and titanium based alloys were obtained by using oxidation, reactive sputtering or sputtered interlayers to alter the coating-substrate interfacial region. X-ray photoelectron spectroscopy and argon ion etching were used to characterize the interfacial regions, and an attempt was made to correlate adherence as measured in wear tests with the chemical nature of the interface.

Brainard, W. A.↗
NASA NTRS1980

Improved adhesion of sputtered refractory carbides to metal substrates

Sputtered coatings of the refractory metal carbides are of great interest for applications where hard wear-resistant materials are desired. The usefulness of sputtered refractory carbides is often limited in practice by spalling or interfacial separation. In this work improvements in the adherence of refractory carbides on iron, nickel and titanium base alloys were obtained by using oxidation, reactive sputtering or sputtered interlayers to alter the coating-substrate interfacial region. X-ray photoelectron spectroscopy and argon ion etching were used to characterize the interfacial regions, and an attempt was made to correlate adherence as measured in wear tests with the chemical nature of the interface.

Wheeler, D. R.↗
NASA NTRS1976

Observations of A0620-00 by SAS-3

The transient X-ray source A0620-00 was observed by the SAS-3 group with the SAS-3 X-ray observatory. At maximum X-ray luminosity limits of 2% were placed on periodic variations from 0.2 ms - 2,000 sec. A precise position was obtained with the rotating modulation collimator. This led directly to radio and optical identification by groups at the NRAO, Arecibo, and McGraw Hill Observatories. The low energy (0.15-0.9 keV) system was pointed at the source, and a spectrum was derived. Hardness ratios are presented, as well as detailed light curves.

Bradt, H.↗
NASA NTRS1977

Friction and wear properties of three hard refractory coatings applied by radiofrequency sputtering

The adherence, friction, and wear properties of thin hard refractory compound coatings applied to 440C bearing steel by radiofrequency sputtering were investigated. Friction and wear tests were done with nonconforming pin on disk specimens. The compounds examined were chromium carbide, molybdenum silicide, and titanium carbide. The adherence, friction, and wear were markedly improved by the application of a bias voltage to the bearing steel substrate during coating deposition. Analysis by X-ray photoelectron spectroscopy indicated that the improvement may be due to a reduction in impurities in bias deposited coatings. A fivefold reduction in oxygen concentration in MoSi2 coating by biasing was noted. Chromium carbide was not effective as an antiwear coating. Molybdenum silicide provided some reduction in both friction and wear. Titanium carbide exhibited excellent friction and antiwear properties at light loads. Plastic flow and transfer of the coating material onto the pin specimen appears to be important in achieving low friction and wear.

Brainard, W. A.↗
NASA NTRS1976

An alpha particle instrument with alpha, proton, and X-ray modes for planetary chemical analyses

The interaction of alpha particles with matter is employed in a compact instrument that could provide rather complete in-situ chemical analyses of surfaces and thin atmospheres of extraterrestrial bodies. The instrument is a miniaturized and improved version of the Surveyor lunar instrument. The backscattering of alpha particles and (alpha, p) reactions provide analytical data on the light elements (carbon-iron). An X-ray mode that detects the photons produced by the alpha sources provides sensitivity and resolution for the chemical elements heavier than about silicon. The X-rays are detected by semiconductor detectors having a resolution between 150 and 250 eV at 5.9 keV. Such an instrument can identify and determine with good accuracy 99 percent of the atoms (except hydrogen) in rocks. For many trace elements, the detecting sensitivity is a few ppm. Auxiliary sources could be used to enhance the sensitivities for elements of special interest. The instrument could probably withstand the acceleration involved in semi-hard landings.

Economou, T. E.↗
NASA NTRS1976

The transient periodic X-ray source in Taurus, A0535+26

Eighteen X-ray light curves of the 104-sec periodicity in the Taurus X-ray nova A 0535+26 are analyzed which were obtained by SAS-3 in six energy intervals between 1 and 35 keV during the period from May 30 to June 2, 1975. It is shown that the pulse structure is relatively simple at energies above 19 keV, but develops a complex series of five irregularly spaced maxima at lower energies. The energy spectrum averaged over the 104-sec period is found to be extremely hard, with a best-fit temperature of about 30 keV for the exponential spectrum, an excess at about 15 keV, and a steepening above 20 keV. It is suggested that A 0535+26 may be a compact object in a binary system containing the peculiar Be star HDE 245770. The transient behavior could arise due to episodic mass loss by the primary or because the compact object is in a highly eccentric orbit about the companion, with appreciable mass transfer occurring only at periastron.

Bradt, H.↗
NASA NTRS1980

X-ray spectroscopy of late-type stars

The solid state spectrometer on the Einstein Observatory determined .4 - 4.5 keV spectra for Capella, Algol and 6 RS CVn binaries. All show evidence for a bimodal distribution of emission measure with temperature with one component approximately 7 million degrees and one approximately 40 million degrees. The spread in values of both luminosity and emission measure is 10 for the low temperature component and approximately 500 for the high temperature component. Line emission due to Fe can be identified in most of them and abundances of Si, S and Fe are consistent with approximately solar values in all cases. Estimates indicate dimensions of the emitting regions are on the order of the stellar size and the binary separation for the low and high temperature components, respectively, unless the pressures are high. Variations in the flux were observed, mostly in the hard component for the RS CVn binaries, in the soft component for Capella. A flare was observed during primary eclipse of Algol. The possibility is discussed that the other variations could all be due to intrinsic variability with a time scale of hours-days rather than eclipse or modulation with photometric phase.

Swank, J. H.↗
NASA NTRS1974

TRIIG - Time-lapse reproduction of images through interactive graphics

Description of the hardware and software implementing the system of time-lapse reproduction of images through interactive graphics (TRIIG). The system produces a quality hard copy of processed images in a fast and inexpensive manner. This capability allows for optimal development of processing software through the rapid viewing of many image frames in an interactive mode. Three critical optical devices are used to reproduce an image: an Optronics photo reader/writer, the Adage Graphics Terminal, and Polaroid Type 57 high speed film. Typical sources of digitized images are observation satellites, such as ERTS or Mariner, computer coupled electron microscopes for high-magnification studies, or computer coupled X-ray devices for medical research.

Buckner, J. D.↗
NASA NTRS1977

X-ray bursts from MXB 1837+05

Results are reported for SAS 3 observations of 22 bursts from the X-ray source designated MXB 1837+05. Assuming that all the bursts come from one source, the source position is determined to be right ascension (1950) 18 hr 37.9 min, declination (1950) 5 deg 4.2 min. Integrated burst intensities are listed along with ratios of counts in different energy channels, and it is found that there are significant variations in these ratios from burst to burst. The bursts are also shown to exhibit a variety of temporal structures (including double peaks) and changes in spectral hardness. No regularity was detected in the burst occurrence times during one observing period, but four bursts during another period seemed to recur at regular intervals of about 6.3 hr. It is concluded that an intensity-interval correlation similar to that for a rapid burster does not exist for MXB 1837+05 and that this source is probably identical with the relatively strong and steady source Ser X.1.

Li, F. K.↗
NASA NTRS1974

The hard start phenomena in hypergolic engines. Volume 3: Physical and combustion characteristics of engine residuals

An investigation was conducted to determine the cause of starting problems in the hypergolic rocket engines of the Apollo reaction control (RCS) engines. The scope of the investigation was as follows: (1) to establish that chemical reactions occurred during the preignition and post combustion periods, (2) to identify the chemical species of the products of preignition and post combustion reaction, and (3) to determine the explosive nature of the identified species. The methods used in identifying the chemical products are described species. The infrared spectra, X-ray spectra, and other signatures of the compounds are presented. The physical and explosion characteristics of various hypergolic agents are reported.

Miron, Y.↗
NASA NTRS1980

Microstructure and mechanical properties of bulk and plasma-sprayed y2O3-partially stabilized zirconia

Bulk 8.0 weight percent yttria partially stabilied zirconia (PSZ) was studied by light microscopy, transmission electron microscopy, X-ray analysis, microhardness testing, and fracture toughness testing. The as received PSZ contained spheroidal and grain boundary precipitates up to 4 micrometers in size. Spheroids up to 1.26 micrometers were metastable tetragonal; large spheroids were monoclinic. Grinding the PSZ into powder did not cause a significant amount of tetragonal to transform to monoclinic. This indicates that transformation toughness is not a significant mechanism in PSZ. Aging the PSZ at 1500 C caused the fine tetragonal precipitates to grow from 0.06 to 0.12 micrometers, in 250 minutes. A peak hardness of 1400 kg/sq mm was attained after 50 minutes. Solution annealing and quenching the as received PSZ eliminated the large precipitates, but fine tetragonal precipitates reformed on quenching. Aging at 1500 C caused the fine 0.02 micrometers tetragonal precipitates to grow into plates about 0.10 by 0.50 micrometers. A peak hardness of 1517 kg/sq mm was obtained after 250 minutes. On further aging, monoclinic percipitates formed along grain boundaries. The fracture toughness of the aged and unaged solution annealed and quenched PSZ was found to be between 2 and 3 MN /square root of m cubed. This range of fracture toughness is consistent with PSZ's that do not undergo transformation toughening.

Valentine, P. G.↗
NASA NTRS1959

Measurements of Total Hemispherical Emissivity of Several Stably Oxidized Nickel-Titanium Carbide Cemented Hard Metals from 600 F to 1,600 F

The total hemispherical emissivity of several nickel-titanium carbide cemented hard metals have been measured over a temperature range from 600 F to l,600 F. A variety of cemented hard metals were obtained from the Kennametal Corporation. A brief discussion of the apparatus employed and the procedures used for this investigation is included. The results of the tests of specimens in the as-received and polished states indicate a nearly constant emissivity for each material tested over the temperature range considered and only slight differences in emissivity values for the different materials. Values obtained on the stably oxidized specimens range from 0.90 to 0.94 at 6000 F and o.88 to 0.92 at 1,600 F for the as-received specimens and from 0.82 to 0.89 at 600 F and 0.85 to 0.87 at 1,600 F for the polished specimens. The surface analysis of the oxidized materials as obtained by X-ray diffraction methods and metallographic techniques are presented as an aid to reproducing the surface on which these measurements were made.

Wade, William R.↗
NASA NTRS1974

Observation of a cosmic gamma-ray burst on Apollo 16. I - Temporal variability and energy spectrum

A cosmic gamma-ray event occurring April 27, 1972 at 10.68 UT was observed by gamma-ray and X-ray spectrometers on Apollo 16 as well as by Vela 6A. Analysis has yielded a detailed time profile of the entire event, an energy spectrum covering three order of magnitude (2.0 to 7.9 KeV and 0.067 to 5.1 MeV) and a source location. A well-defined onset prior to the main impulse period and a probable precursor are reported. The total energy of the event over the observed range was 2 x 10 to the minus 4th power ergs/sq cm. The data indicate the presence of a hard component which persists during the entire event, with a softer variable component becoming dominant during the most explosive burst portion.

Metzger, A. E.↗
NASA NTRS1975

Upper limits of hard gamma-ray emission from six X-ray sources

The Cornell 100-inch gamma-ray telescope has been used to set upper limits for the gamma-ray flux above 400 MeV from the X-ray sources Cyg X-1, Cyg X-2, Cyg X-3, Cas A, Cas B, and Per X-1. An upper limit for the diffuse flux of the galactic disk was set which is consistent with OSO-3 and SAS-2 data. A new measurement of the atmospheric gamma-ray generation rate is presented.

Campbell, M.↗
NASA NTRS1976

Absorption dips at low X-ray energies in Cygnus X-1

Absorbing material in Cygnus X-1 jitters near the line joining the two stars, out of the orbital plane is described. Three looks with the Copernicus satellite at Cygnus X-1 have produced four examples of absorption dips (decreases in the 2 to 7 keV flux from Cygnus X-1 with an increase of spectral hardness consistent with photoelectric absorption).

Murdin, P. G.↗
NASA NTRS1978

Possible X-ray counterparts of gamma-ray sources

The results are presented of a survey regarding the X-ray source positions which fall within the error boxes of 10 unidentified gamma-ray sources observed with the aid of the COS-B satellite. In three cases, including CG 135-1, CG 312-1, and CG 327-0, an X-ray source was found within the gamma-ray error box. However, because of the large uncertainty regarding the gamma-ray source positions, the positional coincidence is not necessarily conclusive. It is, therefore, necessary to take into account additional information on the spectral or temporal characteristics of the X-ray sources. It is found that the X-ray source 4U 02416 plus 1 is a possible candidate as the X-ray-counterpart of CG 135 plus 1 in connection with both spectral hardness characteristics and positional coincidence.

Maraschi, L.↗
NASA NTRS1980

Gamma-ray burst observations from the UCB/LASL experiment of ISEE-3

The University of California at Berkeley (UCB)/Los Alamos Scientific Laboratory (LASL) gamma-ray burst experiment on board ISEE-3 is described and initial results of the experiment are presented. The instrument consists of an X-ray spectrometer originally designed to monitor solar emission continuously over the energy range 4.8-1264 keV with additional electronics to record data from the intense, short-lived gamma ray bursts at a very high rate and with good timing accuracy. Since the launch of ISEE-3 into a heliocentric orbit at the inner Lagrangian point in August, 1978, the UCB/LASL experiment has detected and recorded 12 gamma-ray bursts, including the unusually intense burst of November 4, 1978, which exhibited most of the classical gamma-ray burst characteristics, the intense burst of November 19, 1978, with an atypical time history and an unusually hard spectrum, and the extended burst of March 7, 1979. The spectral and temporal data demonstrate the diverse nature of the gamma-ray burst phenomenon, and are currently being combined with those of the Pioneer Venus Orbiter and Venera 11 and 12 to obtain accurate burst locations.

Evans, W. D.↗