Total emittance measurements of thin metallic films at cryogenic temperatures
Calorimetric measurements determining total hemispheric emittance of thin gold films as function of temperature, demonstrating film thickness effect
Armaly, B. F.↗
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Results for “Cryogenic temperatures”
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Effects of surface contamination on the infrared emissivity and visible-light scattering of highly reflective surfaces at cryogenic temperatures
A technique is described for the simultaneous in situ measurement of film thickness, refractive index, total normal emissivity, visible-light scattering, and reflectance of contaminant films on a highly reflective liquid-nitrogen cooled, stainless steel substrate. Emissivities and scattering data are obtained for films of water, carbon dioxide, silicone oil, and a number of aromatic and aliphatic hydrocarbons as a function of film thickness between zero and 20 microns. Of the contaminants investigated, water has by far the greatest effect on emissivity, followed by silicone oil, aliphatic hydrocarbons, aromatic hydrocarbons, and carbon dioxide. The emissivity increases more rapidly with film thickness between zero and 2.5 microns than at thicknesses greater than 2.5 microns. Scattering of visible light changes very little below 2 microns thickness but increases rapidly with thickness beyond 2 to 3 microns. The effect of contaminant films on passive radiation coolers is discussed.
Viehmann, W.↗
Effects of surface contamination on the infrared emissivity and visible-light scattering of highly reflective surfaces at cryogenic temperatures
A technique is described for the simultaneous in situ measurement of film thickness, refractive index, total normal emissivity, visible light scattering, and reflectance of contaminant films on a highly reflective liquid nitrogen-cooled, stainless steel substrate. Emissivities and scattering data were obtained for films of water, carbon dioxide, silicone oil, and a number of aromatic and aliphatic hydrocarbons as a function of film thickness between zero and 20 microns. Water had the greatest effect on emissivity, followed by silicone oil, aliphatic hydrocarbons, aromatic hydrocarbons, and carbon dioxide. Emissivity increased more rapidly with film thickness between zero and 2.5 microns, than at thickness greater than 2.5 microns. Scattering of visible light changed little below 2-microns thickness but increased rapidly with thickness beyond 2 to 3 microns. The effect of contaminant films on passive radiation coolers is discussed.
Viehmann, W.↗
Flaw growth behavior in thick welded plates of 2219-T87 aluminum at room and cryogenic temperatures
Axial load fatigue and fracture tests were conducted on thick welded plates of 2219-T87 aluminum alloy to determine the tensile strength properties and the flaw growth behavior in electron beam, gas metal arc, and pulse current gas tungsten arc welds for plates 6.35 centimeters (2.5 in.) thick. The tests were conducted in room temperature air and in liquid nitrogen environments. Specimens were tested in both the as-welded and the aged after welding conditions. The experimental crack growth rate were correlated with theoretical crack growth rate predictions for semielliptical surface flaws.
Forman, R. G.↗
NERVA irradiation program. GTR 23, volume 1: Combined effects of reactor radiation and cryogenic temperature on NERVA structural materials
Specimens fabricated from structural materials that were candidates for certain NERVA applications were irradiated in liquid nitrogen (LN2), liquid hydrogen (LH2), water, and air. The specimens irradiated in LN2 were stored in LN2 and finally tested in LN2, or at some higher temperature in a few instances. The specimens irradiated in LH2 underwent an unplanned warmup while in storage so this portion of the test was lost; some specimens were tested in LN2 but none were tested in LH2. The Ground Test Reactor was the radiation source. The test specimens consisted mainly of tensile and fracture toughness specimens of several different materials, but other types of specimens such as tear, flexure, springs, and lubricant were also irradiated. Materials tested include Hastelloy X, Al, Ni steel, steel, Be, ZrC, Ti-6Al-4V, CuB, and Ti-5Al-2.5Sn.
Mcdaniel, R. H.↗
Transport properties of N2 gas at cryogenic temperatures
The viscosity and thermal conductivity of nitrogen gas for the temperature range 5 K - 135 K have been computed from the second Chapman-Enskog approximation. Quantum effects, which become appreciable at the lower temperatures, are included by utilizing collision integrals based on quantum theory. A Lennard-Jones (12-6) potential was assumed. The computations yield viscosities about 20 percent lower than those predicted for the high end of this temperature range by the method of corresponding states, but the agreement is excellent when the computed values are compared with existing experimental data.
Pearson, W. E.↗
Crack-growth behavior in thick welded plates of Inconel 718 at room and cryogenic temperatures
Results of mechanical-properties and axial-load fatigue and fracture tests performed on thick welded plates of Inconel 718 superalloy are presented. The test objectives were to determine the tensile strength properties and the crack-growth behavior in electron-beam, plasma-arc, and gas tungsten are welds for plates 1.90 cm (0.75 in) thick. Base-metal specimens were also tested to determine the flaw-growth behavior. The tests were performed in room-temperature-air and liquid nitrogen environments. The experimental crack-growth-rate data are correlated with theoretical crack-growth-rate predictions for semielliptical surface flaws.
Forman, R. G.↗
Measurement component technology. Volume 3: Cryogenic temperature measurement and high temperature strain gage technology
For abstract, see N74-27185.
Hayakawa, K. K.↗
Increasing terminal strip efficiency at cryogenic temperatures
Single-crystal sapphire and quartz have been used to fabricate termally shorting, electrically insulating terminal boards for incorporation in metal heat-sink blocks.
Holdeman, L. B.↗
Effect of viscosity on rolling-element fatigue life at cryogenic temperature with fluorinated ether lubricants
Rolling-element fatigue tests were conducted with 12.7-mm-(1/2-in.-) diameter AISI 52100 steel balls in the NASA five-ball fatigue tester, with a maximum hertz stress of 5500 mN/m2 (800 000 psi), a shaft speed of 4750 rpm, lubricant temperature of 200 K (360 R), a contact angle of 20 deg, using four fluorinated ether lubricants of varying viscosities. No statistically significant differences in rolling-element fatigue life occurred using the four viscosity levels. Elastohydrodynamic calculations indicate that values of the lubricant film parameter were approximately 2 or greater.
Dietrich, M. W.↗
Plasma-sprayed, self-lubricating coatings for use from cryogenic temperatures to 870 deg C (1600 deg F)
A plasma-sprayed coating is described with good lubricating properties over a wide temperature range. The coating, designated NASA LUBE PS101, contains silver, nichrome, calcium fluoride, and an oxidation protective glass. Oscillating tests were conducted of self-aligning, plain cylindrical bearings, in which the bore was lined with 0.025 cm (0.010 in.) thick coatings of PS101; these were conducted at a radial load of 3.5 x 10 to the 7th power N/sq m (5000 psi) in nitrogen gas at -107 C (-160 F), in vacuum at room temperature, and in air from room temperature to 870 C (1600 F). Friction coefficients were less than 0.25 in all cases and wear rates were low. The coating is not brittle, and it has adequate oxidation resistance in air to at least 870 C.
Sliney, H. E.↗
Investigation of the fracture mechanism in Ti-5Al-2.5Sn at cryogenic temperatures
The influence of microstructure on the fracture mechanism and plane-strain fracture toughness of Ti-5Al-2.5Sn was studied through the use of fractography and metallographic sectioning techniques. One-inch thick plates of extra low interstitial (ELI) and normal interstitial Ti-5Al-2.5Sn were mill annealed at 815 C followed by either air or furnace cooling. These variations in composition and cooling rate resulted in differences in the volume fraction and internal structure of the iron-stabilized phase, and in the crystallographic texture and ordering of the alpha matrix. The tensile properties of these plates were determined at 20 K, 77 K, and 295 K. The air-cooled ELI plate was the toughest material evaluated.
Vanstone, R. H.↗
Investigation of the fracture mechanism of Ti-5Al-2.5Sn at cryogenic temperatures
Fractography and metallographic sectioning were used to investigate the influence of microstructure on the fracture mechanism and fracture toughness (KIC) of normal interstitial and extra low interstitial (ELI) Ti-5Al-25Sn at 20 K (-423 F) and 77 K (-320 F). Plates of each grade were mill annealed at 815 C followed by either air or furnace cooling. These variations in composition and cooling rate resulted in differences in the volume fraction and internal structure of the dispersed beta phase and in the ordering of the alpha matrix. The ELI alloys were tougher than the normal interstitial plates. KIC of the furnace-cooled ELI plate was 25% lower than that of the air-cooled ELI material. Variations in cooling rate had no influence of KIC of the normal interstitial alloys. Fractography showed that a large portion of the fracture surfaces were covered with elongated dimples. Metallographic sections of specimens deformed at 77 K showed that these features form at the intersections of slip bands or deformation twins with grain or twin boundaries. Ordering and higher interstitial levels increase the local strain in slip bands resulting in void nucleation at lower macroscopic strains and lower KIC values.
Van Stone, R. H.↗
Development of flightweight static face seals for 75.84 MPa /11 000 psi/ pressure and cryogenic temperatures
The development of a static seal configuration to meet the lightweight low-leakage requirements of the Space Shuttle Main Engine (pressure carrying capability of up to 75.84 MPa) is discussed. The design features, fabrication methods, lab testing, and performance of seal are examined. Flange and bolt details of the joint assembly are considered with attention to an ultrasonic technique for measuring preload in the bolts. Methods used for leak testing in the laboratory and in the field are described; the practicality of the procedures is considered. Attention is directed to hydrogen-environment embrittlement and its influence on seal and joint design.
Daniels, C. M.↗
Graphite/polyimide tension tests at elevated and cryogenic temperatures
Interim results for characterizing tension properties of graphite/polyimide laminates are reported. Existing test procedures for resin-matrix composites were evaluated for use through the extreme temperature range indicated above. Of particular concern was the performance of resistance strain gages at the elevated temperatures and tests were carried out to compare their performance against that of a capacitive strain gage. Limited design data are reported for graphite/polyimide laminates which are being produced through the CASTS Project.
Chapman, A. J.↗
Influence of composition, annealing treatment, and texture on the fracture toughness of Ti-5Al-2.5Sn plate at cryogenic temperatures
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Van Stone, R. H.↗
A study of optically contacted quartz at cryogenic temperatures
Optical contacting as a method of joining the quartz components of the instruments for the Gravity Probe-B experiment is evaluated. The strength of the bond between optically contacted fused quartz surfaces at liquid helium temperature was investigated. A test apparatus which can be used for making measurements of the tensile strength of these bonds was designed. Results of the tensile pull tests are given and the reliability of such bonds analyzed.
Payne, L. L.↗
Ambient and cryogenic temperature testing of a 32-channel CMOS multiplexer
A 32 channel CMOS multiplexer was tested at room temperature and at liquid helium temperature (4.9 K). Voltage gain of the FET input stage, leakage current, electrical crosstalk, and noise as a function of clock frequency were measured. The voltage gain measured at 4.9 K was slightly higher than that measured at 300 K and was independent of clock frequency at both operating temperatures. The off channel leakage current was 0.23 pA/channel at 4.9 K. Electrical crosstalk between adjacent channels (one on, one off) was quite low. The spot noise at 10 Hz, of the CMOS multiplexer operating in the static mode did not vary significantly with operating temperature. In the dynamic mode (3.2 kHz clock) at room temperature, the spot noise at 10 Hz was substantially higher than that measured in the static mode.
Lee, J. H.↗