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At least 271 records · Page 15
All sourcesNASA NTRSDOE OSTI
DOE OSTI2026

New perspectives on materials and device dynamics using time-resolved full-field diffraction X-ray imaging

Understanding how materials evolve during synthesis, processing, or device operation requires experimental access to structural dynamics across wide ranges of length and time scales, often in bulk samples or even within packaged devices. Time-resolved full-field diffraction X-ray microscopy has recently emerged as a powerful way to meet this need by combining the penetration and structural sensitivity of X-ray diffraction with objective-lens-based magnification, sensitive high-resolution X-ray imaging detectors, and pump-probe and real-time imaging strategies. Advances in full-field X-ray diffraction microscopy, often termed dark-field X-ray microscopy (DFXM), enable simultaneous imaging of extended fields of view while retaining crystallographic selectivity. Time-resolved DFXM promises to enable advances in materials processing and dynamics, electrochemical and photochemical processes, and the design of electronic devices. This Perspective summarizes the key instrumental concepts that define the performance of these methods, including the choice of imaging optics, detector considerations, and the impact of source time structure at synchrotron light sources and X-ray free-electron lasers (XFELs). We discuss the simultaneous use of complementary imaging modes that are increasingly used in practice. The early demonstrations of the potential of time-resolved DFXM include real-time defect and grain-boundary dynamics during metal annealing, stroboscopic imaging of functional devices with high strain sensitivity, and ultrafast pump-probe implementations at XFELs that directly visualize acoustic-wave propagation and energy dissipation in bulk crystals.

Dark-field X-ray microscopy↗
DOE OSTI2025

Theory of terahertz pulse transmission through ferroelectric nanomembranes

An analytical model is developed to predict the temporal evolution of the lattice polarization in ferroelectric nanomembranes upon the excitation by a terahertz (THz) electromagnetic pulse of an arbitrary waveform and the concurrent transmission of the THz pulse in both linear and nonlinear regimes. It involves the use of the perturbation method to solve the equation of motion for the lattice polarization in both unclamped and strained ferroelectric nanomembranes within the framework of Landau-Ginzburg-Devonshire theory. The model is applicable to perovskite oxides such as BaTiO 3 and SrTiO 3 , wurtzite Al 1−𝑥 ⁢Sc 𝑥 ⁢N, and trigonal LiNbO 3 . Our analytical model provides a theoretical basis for determining the thermodynamic and kinetic parameters of ferroelectric materials through a THz transmission experiment. The calculation results also suggest an approach to reversing the chirality of a circularly polarized THz pulse by harnessing the resonant polarization-photon coupling in ferroelectrics. This capability of chirality reversal, along with the high tunability from a strain applied along any arbitrarily oriented in-plane axis, provides new opportunities for THz wave modulation without relying on complex metasurface designs.

36 MATERIALS SCIENCE↗
DOE OSTI2022

Self-Induced Curvature in an Internally Loaded Peridynamic Fiber

A straight fiber with nonlocal forces that are independent of bond strain is considered. These internal loads can either stabilize or destabilize the straight configuration. Transverse waves with long wavelength have unstable dispersion properties for certain combinations of nonlocal kernels and internal loads. When these unstable waves occur, deformation of the straight fiber into a circular arc can lower its potential energy in equilibrium. The equilibrium value of the radius of curvature is computed explicitly.

36 MATERIALS SCIENCE↗
DOE OSTI2021

Strongly Anisotropic Thermomechanical Response to Shock Wave Loading in Oriented Samples of the Triclinic Molecular Crystal 1,3,5-Triamino-2,4,6-trinitrobenzene

All-atom molecular dynamics (MD) simulations were used to study shock wave loading in oriented single crystals of the highly anisotropic triclinic molecular crystal 1,3,5-triamino-2,4,6-trinitrobenzene (TATB). The crystal structure consists of planar hydrogen-bonded sheets of individually planar TATB molecules that stack into graphitic-like layers. Shocks were studied for seven systematically prepared crystal orientations with limiting cases that correspond to shock propagation exactly perpendicular and exactly parallel to the graphitic-like layers. The simulations were performed for initially defect-free crystals using a reverse-ballistic configuration that generates explicit, supported shocks. Final longitudinal stress components are between ≈8.5 and ≈10.5 GPa for the 1.0 km s –1 impact speed studied. Orientation-dependent properties are reported including shock speeds, stresses, temperatures, compression ratios, and local material strain rates. Spatiotemporal maps of the temperature, stress tensor, material flow, and molecular orientations reveal complicated processes that arise for specific shock directions. Furthermore, the results indicate that TATB shock response is highly sensitive to crystal orientation, with significant qualitative differences for the time evolution of the stress tensor and temperature, elastic/inelastic compression response, defect formation and growth, critical von Mises stress, and strain rates during shock rise that span nearly an order of magnitude. A variety of inelastic deformation mechanisms are identified, ranging from crumpling of graphitic-like layers to dislocation-mediated plasticity to intense shear strain localization. To our knowledge, these are the first systematic MD simulations and analysis of explicit shock wave propagation along nontrivial crystal directions in a triclinic molecular crystal.

36 MATERIALS SCIENCE↗
NASA NTRS1977

Perturbation of a discontinuous transonic flow

The main difficulty in perturbing a discontinuous transonic flow is in the representation of the shift in the location of the discontinuity (shock wave). Herein presented is a method of overcoming this difficulty by using a distorted airfoil as the initial case rather than the real physical airfoil; the distortion is chosen such that the shock location is unchanged by the perturbation. The distorted airfoil is obtained by the use of a strained coordinate system. A direct consequence of the theory is the derivation of an algebraic similarity relation between related airfoils with shock waves at differing locations. Results for simple examples are shown.

Nixon, D.↗
DOE OSTI2023

Modeling shock-induced void collapse in single-crystal Ta systems at the mesoscales

Understanding the role of microstructural heterogeneities on the shock wave propagation and defect evolution behavior is essential to predicting the dynamic response of metals. Heterogeneities, such as voids, provide challenges to understanding the wave propagation behavior as the shock-void interaction can collapse the void and result in large plastic strains and significant heating (hot spot formation) in the metal. Accurate modeling of this phenomenon requires predicting the void collapse mechanisms and the related heat generation and dissipation mechanisms (hotspot formation) that determine the microstructure evolution. While molecular dynamics (MD) simulations can model the void collapse behavior, the time/length scale capabilities pose a challenge to connect with continuum models or the experimental scales. Here, this study presents the capability of the newly developed quasi-coarse-grained dynamics (QCGD) method that extends the MD simulations to larger system sizes and longer times to model this phenomenon. This study uses QCGD simulations to investigate the mechanisms of shock wave interactions with pre-existing voids in single-crystal Ta microstructures for variations in shock pressures, void size, and loading orientations. For a given orientation, the plasticity contributions and rates of void collapse are observed to vary with shock pressures and void size. The larger void sizes and higher pressures result in increased temperatures (hot spots) and faster void collapse rates and unravel the variations in the plasticity contributions. In addition, QCGD simulations investigate the post-collapse microstructure evolution as a release wave travels through the hot spot region. The simulations reveal that the reduction in temperatures due to heat dissipation initiates the dynamic recrystallization behavior in the hotspot regions.

36 MATERIALS SCIENCE↗
NASA NTRS2015

Experimental Investigation on Acousto-Ultrasonic Sensing Using Polarization-Maintaining Fiber Bragg Gratings

This report discusses the guided Lamb wave sensing using polarization-maintaining (PM) fiber Bragg grating (PM-FBG) sensor. The goal is to apply the PM-FBG sensor system to composite structural health monitoring (SHM) applications in order to realize directivity and multi-axis strain sensing capabilities while using reduced number of sensors. Comprehensive experiments were conducted to evaluate the performance of the PM-FBG sensor in a composite panel structure under different actuation frequencies and locations. Three Macro-Fiber-Composite (MFC) piezoelectric actuators were used to generate guided Lamb waves and they are oriented at 0, 45, and 90 degrees with respect to PM-FBG axial direction, respectively. The actuation frequency was varied from 20kHz to 200kHz. It is shown that the PM-FBG sensor system is able to detect high-speed ultrasound waves and capture the characteristics under different actuation conditions. Both longitudinal and lateral strain components in the order of nano-strain were determined based on the reflective intensity measurement data from fast and slow axis of the PM fiber. It must be emphasized that this is the first attempt to investigate acousto-ultrasonic sensing using PM-FBG sensor. This could lead to a new sensing approach in the SHM applications.

Wang, Gang↗
DOE OSTI2022

Phase transitions in Zr at sub-nanosecond time scales

Here solid-solid phase transitions are investigated in Zr thin films using shock compression induced by a short laser pulse (<1 ns). Shock wave profiles are measured at free surfaces for films of different thicknesses (a few micrometers) using chirped-pulse line velocimetry with 10 ps time resolution. Experiments are performed at pressures up to ~50 GPa, which is sufficient to reach the ω and β phases under equilibrium conditions. The shock wave structures are analyzed using a general Lagrangian analysis method, which allows for the calculation of stress–strain paths and assessments of phase transition behavior. In agreement with recent short laser pulse experiments using ultra-fast x-ray diffraction, we do not find any clear evidence of the α–ω transition, though this would be expected from the phase diagram. Instead, we infer a direct transformation to a metastable β-phase at lower shock pressures (<20 GPa) and equilibrium β at higher pressures. Through the velocimetry analysis, we find α–β transformation onset times of less than ~100 ps and completion times of less than ~200 ps.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
NASA NTRS2016

Experimental Investigation on Acousto-ultrasonic Sensing Using Polarization-Maintaining Fiber Bragg Gratings

This report discusses the guided Lamb wave sensing using polarization-maintaining (PM) fiber Bragg grating (PM-FBG) sensor. The goal is to apply the PM-FBG sensor system to composite structural health monitoring (SHM) applications in order to realize directivity and multi-axis strain sensing capabilities while reducing the number of sensors. Comprehensive experiments were conducted to evaluate the performance of the PM-FBG sensor attached to a composite panel structure under different actuation frequencies and locations. Three Macro-Fiber-Composite (MFC) piezoelectric actuators were used to generate guided Lamb waves that were oriented at 0, 45, and 90 degrees with respect to PM-FBG axial direction, respectively. The actuation frequency was varied from 20kHz to 200kHz. It was shown that the PM-FBG sensor system was able to detect high-speed ultrasound waves and capture the characteristics under different actuation conditions. Both longitudinal and lateral strain components in the order of nano-strain were determined based on the reflective intensity measurement data from fast and slow axis of the PM fiber. It must be emphasized that this is the first attempt to investigate acouto-ultrasonic sensing using PM-FBG sensor. This could lead to a new sensing approach in the SHM applications. Nomenclature.

Wang, Gag↗
NASA NTRS1977

A CW ultrasonic bolt-strain monitor

There exists a need for a relatively inexpensive system for measuring strain in bolts. The torque wrench is one technique for straining bolts which has been widely applied. Unfortunately, friction in the bolt threads and between the nut and the work tend to make such a simple system inaccurate. In practice, a torque wrench is unacceptable for many situations where strain is critical. In this article, an ultrasonic technique is described which can indicate changes in bolt strain to better than one part in 10,000. The technique is based on the one-dimensional propagating-ultrasonic-wave model and uses a new ultrasonic instrument called a Reflection Oscillator Ultrasonic Spectrometer which is a closed-loop feedback marginal-oscillator system that frequency locks the device to the peak of a mechanical resonance in the bolt. The instrument indicates a shift in the bolt resonance frequency due to elongation and changes in velocity of sound due to strain. Data are presented comparing a standard torque wrench to the ultrasonic monitor for different measured stresses on the bolt as well as for different bolt conditions. The strain instrument can be used to monitor changing stresses, to measure material properties and may be applied as a strain gage or load cell.

Heyman, J. S.↗
NASA NTRS1940

An Investigation of Sheet-stiffener Panels Subjected to Compression Loads with Particular Reference to Torsionally Weak Stiffeners

A total of 183 panel specimens of 24ST aluminum alloy with nominal thickness of 0.020, and 0.040 inch with extruded bulb-angle sections of 12 shapes spaced 4 and 5 inches as stiffeners were tested to obtain the buckling stress and the amplitude of the maximum wave when buckled. Bulb angles from 3 to 27 1/2 inches long were tested as pin-end columns. The experimental data are presented as stress-strain and column curves and in tabular form. Some comparisons with theoretical results are presented. Analytical methods are developed that make it possible for the designer to predict with reasonable accuracy the buckling stress and the maximum-wave amplitude of the sheet in stiffened-panel combinations. The scope of the tests was insufficient to formulate general design criteria but the results are presented as a guide for design and an indication of the type of theoretical and experimental work that is needed.

LOADS - COLUMNS↗
NASA NTRS2004

A Novel Inter Core-Cladding Lithium Niobate Thin Film Coated Fiber Modulator/Sensor

A fiber modulator/sensor has been fabricated by depositing a lithium niobate sol-gel thin film between the core and cladding of a fiber preform. The preform is then drawn into 125 micron fiber. The proposed design of lithium niobate cylinder fibers can enhance the existing methodology for detecting sound waves under water utilizing the acoustooptic properties of lithium niobate. Upon application of a stress or strain, light propagating inside the core, according to the principle of total internal reflection, escapes, into the cladding because of the photoelastic boundary layer of lithium niobate. Test results of the lithium niobate fiber reveal a reduction in the 1550 nm, 4mW source with applied tension. The source power from an ordinary quartz fiber under the same stress condition remained invariant to applied tension.

Jamison, Tracee L.↗
DOE OSTI2026

Towards the Ultimate Strength of Medium‐Entropy Alloys Through Pulsed Lasers

The tensile strength of metals at extreme strain rates is a key predictor of their performance in ballistic and structural impact applications. An important experimental method to reach these extreme strain rates is the use of high-amplitude, short-duration pulsed lasers. The Jupiter Laser Facility at the Lawrence Livermore National Laboratory enabled probing for the first time the mechanical response of several promising High Entropy Alloys at times on the order of nanoseconds (strain rates of ∼10 7 and ∼10 9 s −1 ). The measured strength is in the range of 6 to 10 GPa, ten times the quasistatic value. The mechanisms of plastic deformation and failure were identified and quantified through analysis and molecular dynamics simulation. The reflected wave amplitudes, obtained by VISAR, were used to determine the tensile (spall) stress. The high tensile strength obtained is due to two factors: the strain-rate dependence of plastic flow and the kinetics of void nucleation, growth, and coalescence. The experimental results are compared with an analytical prediction considering both grain-interior and grain-boundary void initiation. Molecular dynamics simulations, conducted at strain rates of 10 8 and 10 9 s −1 , rationalize the experimental results. In conclusion, they provide valuable information about the process of failure evolution, and reveal that grain boundary separation plays a pivotal role in spalling.

Materials science↗
NASA NTRS2003

Possible Stick-Slip Mechanism for Whillans Ice Stream

Tidally-induced stick-slip motion in the mouth of Whillans Ice Stream provides a unique natural experiment in ice-stream response behavior and fiom which we might learn a great deal about subglacial till properties and sub-ice-stream conditions. At the IGS Symposium on Fast Glacier Flow (Yakutat, 2002), we reported our observations of stick- slip motion and demonstrated its synchronicity with tidal forcing. Recently, we have completed additional processing of our GPS data in differential mode. It reveals more details of the stick-slip events and illustrates that within 30 seconds, the temporal interval of our data, the ice stream accelerates to a speed corresponding to a completely lubricated bed. While details of individual events vary, there seems to be strong evidence of an elastic rebound on the time scale of one hour following most events. This suggests the event involves the release of stored elastic strain energy in the ice. The similar displacements of events suggest further that till or subglacial hydrologic properties limit the amount of elastic strain released in any single event. We follow a line of reasoning that dilatant strengthening limits the slip displacement and present model of the stick-slip process. To match the observed delay between the peak ocean tide and stick-slip events, our model includes a propagating pressure wave in the subglacial hydrologic system between the grounding line, where the rising tide first increases the subglacial water pressure and regions upstream where stored elastic strain increases the basal shear stress. This high-tide event is released when the increased water pressure reaches the region of increased shear stress. Dilatant strengthening stops the event by increasing pore volume and lowering the water pressure. Following this event, falling tide increases the normal forces, compresses the till and increases pore pressure again, leading to the second falling-tide event we observe every tidal cycle.

Bindschadler, Robert↗
NASA NTRS2003

Possible Stick-Slip Mechanism for Whillans Ice Stream

Tidally-induced stick-slip motion in the mouth of Whillans Ice Stream provides a unique natural experiment in ice-stream response behavior and from which we might learn a great deal about subglacial till properties and sub-ice-stream conditions. At the IGS Symposium on Fast Glacier Flow (Yakutat, 2002), we reported our observations of stick- slip motion and demonstrated its synchronicity with tidal forcing. Recently, we have completed additional processing of our GPS data in differential mode. It reveals more details of the stick-slip events and illustrates that within 30 seconds, the temporal interval of our data, the ice stream accelerates to a speed corresponding to a completely lubricated bed. While details of individual events vary, there seems to be strong evidence of an elastic rebound on the time scale of one hour following most events. This suggests the event involves the release of stored elastic strain energy in the ice. The similar displacements of events suggest further that till or subglacial hydrologic properties limit the amount of elastic strain released in any single event. We follow a line of reasoning that dilatant strengthening limits the slip displacement and present model of the stick-slip process. To match the observed delay between the peak ocean tide and stick-slip events, our model includes a propagating pressure wave in the subglacial hydrologic system between the grounding line, where the rising tide first increases the subglacial water pressure and regions upstream where stored elastic strain increases the basal shear stress. This high-tide event is released when the increased water pressure reaches the region of increased shear stress. Dilatant strengthening stops the event by increasing pore volume and lowering the water pressure. Following this event, falling tide increases the normal forces, compresses the till and increases pore pressure again, leading to the second falling-tide event we observe every tidal cycle.

Bindschadler, Robert↗
DOE OSTI2024

Shallow Soil Response to a Buried Chemical Explosion With Geophones and Distributed Acoustic Sensing

Abstract Shallow sediments can respond non‐linearly to large dynamic strains and undergo a subsequent healing phase as the material gradually recovers following the passing of seismic waves. This study focuses on the physical changes in the subsurface caused by the shaking from a buried chemical explosion detonated in a borehole in Nevada, USA, as a part of the Source Physics Experiment Phase II. The explosion damaged the shallow subsurface and modified the frequency content recorded by 491 geophones and 2240 Distributed Acoustic Sensing (DAS) channels within 2.5 km from surface ground zero. We observe a gradual shift of resonance frequencies in the 10–25 Hz frequency band in the hours following the explosion and develop a method to characterize the related logarithm‐type healing process of the shallow (i.e., upper ∼25 m) subsurface. We find that stronger levels of ground motion increase the relative degree of damage and duration of the subsurface healing; with the spall region exhibiting the largest degree of damage and longest healing recovery time. We observe coherent spatial patterns of damage with the region located to the southeast of the explosion exhibiting more damage than the southwest region. This study demonstrates that both DAS and co‐located geophones capture similar temporal changes associated with the physical processes occurring in the subsurface, with the high‐density sampling of DAS measurements enabling a new capability to monitor the fine‐scale changes of the Earth's shallow subsurface following the detonation of a buried explosion.

Viens, Loïc↗
NASA NTRS1972

Attenuation of stress waves in single and multi-layered structures

Analytical and experimental studies were made of the attenuation of the stress waves during passage through single and multilayer structures. The investigation included studies on elastic and plastic stress wave propagation in the composites and those on shock mitigating material characteristics such as dynamic stress-strain relations and energy absorbing properties. The results of the studies are applied to methods for reducing the stresses imposed on a spacecraft during planetary or ocean landings.

Yang, J. C. S.↗