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At least 271 records · Page 15

Open aperture flow cells for on-line optical analysis of process fluids

A flow cell system includes a vessel and a fluid located in the vessel. A fluid surface of the fluid can be vented to a first gas pressure. The fluid surface can have a first cross-sectional area. The flow cell system includes a conduit in fluid communication with the vessel and positioned downstream of the vessel. The conduit can have a region that includes one or more orifices and has a second cross-sectional area. The second cross-sectional area can be less than the first cross-sectional area. The one or more orifices can be vented to a second gas pressure. The second gas pressure can be equal to or greater than the first gas pressure. Methods for analyzing a process fluid can include characterizing the fluid in the conduit.

Launiere, Cari A.↗

Influence of argon flow rate on structural and optical properties of transparent Nb{sub 2}O{sub 5} thin films

Transparent niobium pentoxide (Nb{sub 2}O{sub 5}) thin films deposited on glass substrates by RF sputtering at different argon (Ar) flow rate were contrastively studied. Analytical methods such as X-ray fluorescence, Fourier-transform infrared spectroscopy and field emission scanning electron microscope were utilized to investigate the morphological surface and structural properties of Nb{sub 2}O{sub 5} thin films deposited at different Ar flow rate. UV–Vis–NIR and photoluminescence (PL) spectroscopy were used to explore the optical properties of Nb{sub 2}O{sub 5} thin films deposited at different Ar flow rate. The allowed optical band gap (E{sub g}{sup d}) of the Nb{sub 2}O{sub 5} thin films varies from 3.88 to 3.80 eV with increasing Ar flow rate from 30 to 90 sccm. The PL of the Nb{sub 2}O{sub 5} thin films showed strong emission peak around 400 nm. The real values of the refractive index are increase with increasing Ar flow rate. Optical quantities related to the optical constants of Nb{sub 2}O{sub 5} thin films thin films such as single oscillator parameters and third-order nonlinear susceptibility were assessed.

36 MATERIALS SCIENCE↗

Optical Measurement of Mass Flow of a Two-Phase Fluid

An optoelectronic system utilizes wavelength-dependent scattering of light for measuring the density and mass flow of a two-phase fluid in a pipe. The apparatus was invented for original use in measuring the mass flow of a two-phase cryogenic fluid (e.g., liquid hydrogen containing bubbles of hydrogen gas), but underlying principles of operation can readily be adapted to non-cryogenic two-phase fluids. The system (see figure) includes a laser module, which contains two or more laser diodes, each operating at a different wavelength. The laser module also contains beam splitters that combine the beams at the various wavelengths so as to produce two output beams, each containing all of the wavelengths. One of the multiwavelength output beams is sent, via a multimode fiberoptic cable, to a transmitting optical coupler. The other multiwavelength output beam is sent, via another multimode fiber-optic cable, to a reference detector module, wherein fiber-optic splitters split the light into several multiwavelength beams, each going to a photodiode having a spectral response that is known and that differs from the spectral responses of the other photodiodes. The outputs of these photodiodes are digitized and fed to a processor, which executes an algorithm that utilizes the known spectral responses to convert the photodiode outputs to obtain reference laser-power levels for the various wavelengths. The transmitting optical coupler is mounted in (and sealed to) a hole in the pipe and is oriented at a slant with respect to the axis of the pipe. The transmitting optical coupler contains a collimating lens and a cylindrical lens that form the light emerging from the end of the fiber-optic cable into a fan-shaped beam in a meridional plane of the pipe. Receiving optical couplers similar to the transmitting optical couplers are mounted in the same meridional plane at various longitudinal positions on the opposite side of the pipe, approximately facing the transmitting optical coupler along the same slant. Light collected by each receiving optical coupler is sent, via a multimode fiber-optic cable, to a detector module similar to the reference detector module. The outputs of the photodiodes in each detector module are digitized and processed, similarly to those of the reference detector module, to obtain indications of the amounts of light of each wavelength scattered to the corresponding receiving position. The value for each wavelength at each position is also normalized to the reference laser-power level for that wavelength. From these normalized values, the density and the mass flow rate of the fluid are estimated.

Wiley, John↗

Reconfigurable acquisition system with integrated optics for a portable flow cytometer

Portable and inexpensive scientific instruments that are capable of performing point of care diagnostics are needed for applications such as disease detection and diagnosis in resource-poor settings, for water quality and food supply monitoring, and for biosurveillance activities in autonomous vehicles. In this paper, we describe the development of a compact flow cytometer built from three separate, customizable, and interchangeable modules. The instrument as configured in this work is being developed specifically for the detection of selected Centers for Disease Control (CDC) category B biothreat agents through a bead-based assay: E. coli O157:H7, Salmonella, Listeria, and Shigella. It has two-color excitation, three-color fluorescence and light scattering detection, embedded electronics, and capillary based flow. However, these attributes can be easily modified for other applications such as cluster of differentiation 4 (CD4) counting. Proof of concept is demonstrated through a 6-plex bead assay with the results compared to a commercially available benchtop-sized instrument.

60 APPLIED LIFE SCIENCES↗

Accretion flows onto supermassive black holes

The radiative and hydrodynamic properties of an angular momentum-dominated accretion flow onto a supermassive black hole depend largely on the ratio of the accretion rate to the Eddington accretion rate. High values of this ratio favor optically thick flows which produce largely thermal radiation, while optically thin 'two-temperature' flows may be present in systems with small values of this ratio. Observations of some AGN suggest that thermal and nonthermal sources of radiation may be of comparable importance in the 'central engine'. Consideration is given to the possibilities for coexistence of different modes of accretion in a single flow. One intriguing possibility is that runaway pair production may cause an optically thick 'accretion annulus' to form at the center of a two-temperature inflow.

Begelman, Mitchell C.↗

Application of reference-free natural background–oriented schlieren photography for visualizing leakage sites in building walls

Air leakage in buildings can cause health and comfort concerns for occupants and can contribute to mold growth on building materials, or in extreme conditions, rot of building materials. Unwanted air leakage through the building envelope also contributes to approximately 4 quadrillion Btu (1172 TWh) of energy consumption per year in the building sector in the United States. Locating and sealing leakage sites can improve the energy efficiency, comfort, air quality, and moisture durability of the building stock. Typical methods of finding leakage sites, such as infrared imaging and smoke tracing, rely on concurrent blower door operation, which can also measure the total leakage rate of the building. Smoke tracing can be disruptive to occupants, and infrared imaging and smoke tracing cannot measure the contribution of individual leaks to prioritize sealing efforts. Here, an optical fluid flow imaging technique, reference-free natural background–oriented schlieren imaging, was adapted to visualize air exfiltration. This is the first step in developing a method to noninvasively locate and measure exfiltration or infiltration sites so that sealing efforts can be prioritized. Experimental results of this technique are presented, demonstrating the method's applicability to visualizing exfiltration through three common building claddings in an outdoor environment. Key variables impacting the performance of this technique when applied to building leakage are also discussed.

29 ENERGY PLANNING, POLICY, AND ECONOMY↗

Doppler mapping of an alternating-sign flow with complex geometry using optical coherence tomography

The method of sign-sensitive mapping of the given range of velocities in a flow with complex geometry based on the principles of optical coherence tomography is described. To produce an alternating-sign flow, the 1% aqueous intralipid solution and the tilted capillary entry with the contraction coefficient 4:1 are used. The mapping is controlled using two parameters, the value of one specific velocity (OSV) for mapping and the accuracy of its determination. The structure image and two OSV images (for positive and negative direction of motion) are obtained as a result of selecting and processing the relevant parts of the signal spectrum. The final image is a result of summing these three images and can be used as a Doppler equivelocity contour map. (radiation scattering)

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

Application of optical interferometry in compressible flows

Interferometry methods were applied to the investigation of steady and unsteady flows in large scale transonic wind tunnels. Holographic interferometry was demonstrated to provide reliable flow visualization and quantitative results for a number of two-dimensional flows. These conclusions were based on extensive comparisons with results obtained by other means. Data obtained on a NACA 64A010 airfoil with an oscillating flap installed in the Ames 11-foot transonic tunnel are presented. Interferograms were recorded at a free stream Mach number of 0.8, flap frequency of 30 Hertz and chord Reynolds numbers of 6.6 x 10 to the 6th and 12.3 x 10 to the 6th. The interferometric results were reduced to dynamic surface pressures, Mach contours and wake flow profiles. A new interferometry method that is capable of providing real-time interferometry data is also discussed.

Bachalo, W. D.↗

Optical manifestations of mass outflows from young stars - At atlas of CCD images of Herbig-Haro objects

An attempt is made to provide deep CCD images suitable for tracing the shock-excited and scattered-light components characterizing extended Herbig-Haro complexes. Tabular data include astrometric positions for all stars, shock-excited emission knots, prominent scattered-light patches, as well as an identification for all H-alpha emission objects within the CCD images. It is concluded that: (1) optical outflows are not always accompanied by molecular flows, (2) optical outflows show a higher degree of collimation than their molecular counterparts, and (3) the Herbig-Haro phenomenon is not restricted to low-mass young stellar objects.

Strom, K. M.↗

Theoretical investigation of non-equilibrium chemistry and optical radiation in hypersonic flow fields

Future space vehicles returning from distant missions or high earth orbits may enter the upper regions of the atmosphere and use aerodynamic drag to reduce their velocity before they skip out of the atmosphere and enter low earth orbit. The Aeroassist Flight Experiment (AFE) is designed to explore the special problems encountered in such entries. A computer code was developed to calculate the radiative transport along line-or-sight in the general 3-D flow field about an arbitrary entry vehicle, if the temperatures and species concentrations along the line-of-sight are known. The radiative heating calculation at the stagnation point of the AFE vehicle along the entry trajectory was performed, including a detailed line-by-line accounting of the radiative transport in the vacuum ultraviolet (below 200 nm) by the atomic N and O lines. A method was developed for making measurements of the haze particles in the Titan atmosphere above 200 km altitude. Several other tasks of a continuing nature, to improve the technical ability to calculate the nonequilibrium gas dynamic flow field and radiative heating of entry vehicles, were completed or advanced.

Whiting, Ellis E.↗

A photoionization model for the optical line emission from cooling flows

The detailed predictions of a photoionization model previously outlined in Voit and Donahue (1990) to explain the optical line emission associated with cooling flows in X-ray emitting clusters of galaxies are presented. In this model, EUV/soft X-ray radiation from condensing gas photoionizes clouds that have already cooled. The energetics and specific consequences of such a model, as compared to other models put forth in the literature is discussed. Also discussed are the consequences of magnetic fields and cloud-cloud shielding. The results illustrate how varying the individual column densities of the ionized clouds can reproduce the range of line ratios observed and strongly suggest that the emission-line nebulae are self-irradiated condensing regions at the centers of cooling flows.

Donahue, Megan↗

Fiber-Based Multi-Resolution Imaging and Multidimensional X-ray Diagnostics for Ejecta Dynamics in Plume Surface Interactions

The interaction of a rocket exhaust plume with a particulate-laden surface creates a complex, multiphase flow field that can destabilize the vehicle and damage nearby equipment. This study investigates two methods for capturing the particulate dynamics of plume-surface interaction (PSI): optical fiber-based multi-resolution Mie scattering and multi-dimensional X-ray radiography. Mie scattering was used to track PSI-interacted particles, trace their paths, and measure velocities. While effective for the jet periphery and early PSI stages, the technique becomes limited as the scattering cross-section increases over time due to particle displacement from the soil bed, causing the core to become optically dense and appear as a luminous, opaque region. To address this, X-ray radiography was explored as a complementary method for visualizing the optically dense core. PSI experiments were conducted with both reacting and non-reacting jets to evaluate these approaches across a range of optical and flow parameters. The results demonstrated the capability of the fiber-based multi-resolution imaging system to capture simultaneous fields of view at varying magnifications (1x, 2x, 4x), and the ability of X-ray imaging to penetrate the optically dense plume, revealing flow structures that would otherwise be obscured in scattering-based methods. Data were collected for various PSI parameters, including three different heights above the surface, to analyze the ejecta properties and the plume’s temporal evolution. These results provide the first imaging strategy capable of resolving flow structures over a wide spatial dynamic range while also offering the first visualization of the optically dense core.

Ejecta↗

Local measurements in turbulent flows through cross correlation of optical signals

Crossed beam correlation method measures turbulent fluctuations in transonic and supersonic flows. Two collimated beams of radiation are crossed at the point of interest in the flow, and the power loss of each beam is measured with two independent photodetectors, which yield information about the turbulent properties.

Fisher, M. J.↗

Fiber optic-based laser vapor screen flow visualization systems for aerodynamic research in larger-scale subsonic and transonic wind tunnels

The design, installation, and application of the NASA laser vapor screen (LVS) flow visualization systems developed by 10-foot high speed tunnel and 8-foot transonic pressure tunnel are discussed. Sufficient quantity of water is injected into the wind tunnel diffuser section to increase the relative humidity and promote condensation of the water vapor in the flow field about the model. Vortex-dominated flows are illuminated with an intense sheet of laser light. Fiber optics are used to deliver the laser beam through the plenum shell that surrounds the test section of each facility and to the light sheet-generating optics positioned in the ceiling window of the test section. Operational experience indicates that fiber optic-based systems are safe, reliable, and capable of proving high-quality off-surface flow visualization in larger scale subsonic and transonic wind tunnels.

Erickson, Gary E.↗

A high sensitivity fiber optic macro-bend based gas flow rate transducer for low flow rates: Theory, working principle, and static calibration

A novel fiber optic macro-bend based gas flowmeter for low flow rates is presented. Theoretical analysis of the sensor working principle, design, and static calibration were performed. The measuring system consists of: an optical fiber, a light emitting diode (LED), a Quadrant position sensitive Detector (QD), and an analog electronic circuit for signal processing. The fiber tip undergoes a deflection in the flow, acting like a cantilever. The consequent displacement of light spot center is monitored by the QD generating four unbalanced photocurrents which are function of fiber tip position. The analog electronic circuit processes the photocurrents providing voltage signal proportional to light spot position. A circular target was placed on the fiber in order to increase the sensing surface. Sensor, tested in the measurement range up to 10 l min{sup -1}, shows a discrimination threshold of 2 l min{sup -1}, extremely low fluid dynamic resistance (0.17 Pa min l{sup -1}), and high sensitivity, also at low flow rates (i.e., 33 mV min l{sup -1} up to 4 l min{sup -1} and 98 mV min l{sup -1} from 4 l min{sup -1} up to 10 l min{sup -1}). Experimental results agree with the theoretical predictions. The high sensitivity, along with the reduced dimension and negligible pressure drop, makes the proposed transducer suitable for medical applications in neonatal ventilation.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Measuring retinal blood flow in rats using Doppler optical coherence tomography without knowing eyeball axial length

Purpose: Doppler optical coherence tomography (OCT) is widely used for measuring retinal blood flow. Existing Doppler OCT methods require the eyeball axial length, in which empirical values are usually used. However, variations in the axial length can create a bias unaccounted for in the retinal blood flow measurement. The authors plan to develop a Doppler OCT method that can measure the total retinal blood flow rate without requiring the eyeball axial length. Methods: The authors measured the retinal blood flow rate using a dual-ring scanning protocol. The small and large scanning rings entered the eye at different incident angles (small ring: 4°; large ring: 6°), focused on different locations on the retina, and detected the projected velocities/phase shifts along the probing beams. The authors calculated the ratio of the projected velocities between the two rings, and then used this ratio to estimate absolute flow velocity. The authors tested this method in both Intralipid phantoms and in vivo rats. Results: In the Intralipid flow phantom experiments, the preset and measured flow rates were consistent with the coefficient of determination as 0.97. Linear fitting between preset and measured flow rates determined the fitting slope as 1.07 and the intercept as −0.28. In in vivo rat experiments, the measured average total retinal blood flow was 7.02 ± 0.31μl/min among four wild-type rats. The authors’ measured flow rates were consistent with results in the literature. Conclusions: By using a dual-ring scanning protocol with carefully controlled incident angle difference between the two scanning rings in Doppler OCT, the authors demonstrated that it is feasible to measure the absolute retinal blood flow without knowing the eyeball axial length.

60 APPLIED LIFE SCIENCES↗