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At least 271 records · Page 15
All sourcesNASA NTRSDOE OSTI
DOE OSTI2020

Mitigating Damage to Hybrid Perovskites Using Pulsed-Beam TEM

Using a pulsed-beam transmission electron microscope, we discover a reduction in damage to methylammonium lead iodide (MAPbI3) as compared to conventional beams delivered at the same dose rates. For rates as low as 0.001 e·Å –2 ·s –1 , we find up to a 17% reduction in damage at a total dose of 10 e·Å –2 . We systematically study the effects of number of electrons in each pulse and the duration between pulse arrival. Damage increases for both, though the number of electrons per pulse has a larger effect. A crossover is identified, where a pulsed beam causes more damage than a conventional one. Although qualitatively similar to previous findings, the degree to which damage is reduced in MAPbI3 is less than that observed for other materials (e.g., C36H74), supporting the hypothesis that the effects are material- and damage-mechanism-dependent. Despite this, the observation here of damage reduction for relatively large electron packets (up to 200 electrons per pulse) suggests that MAPbI3 is in fact less susceptible to irradiation than C36H74, which may be related to reported self-healing effects. This work provides insights into damage processes and durability in hybrid perovskites and also illustrates the viability of using pulsed-beam TEM to explore the associated molecular-level routes to degradation, analogous to laser-accelerated energetic pulsed electron beams and the study of damage to biomolecules, cells, and tissues in radiobiology.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2021

Investigation of UV, ns-laser damage resistance of hafnia films produced by electron beam evaporation and ion beam sputtering deposition methods

Laser-induced damage in coating materials with a high index of refraction, such as hafnia, limits the performance of high power and high energy laser systems. Understanding the underlying physics responsible for laser damage holds the key for developing damage-resistant optical films. Previous studies have reported a substantial difference in laser damage onset for hafnia films produced by different deposition methods, yet the underlying mechanisms for the observed difference remain elusive. We combined laser damage testing with analytical characterizations and theoretical simulations to investigate the response of hafnia films produced by electron (e-) beam evaporation vs ion beam sputtering (IBS) methods upon UV ns-laser exposure. We found that e-beam produced hafnia films were overall more damage resistant; in addition, we observed a polarization anisotropy associated with the onset of damage in the e-beam films, while this effect was absent in the latter films. The observed differences can be attributed to the stark contrast in the pressure inside the pores inherent in both films. The high pressure inside the IBS-induced nanobubbles has been shown to reduce the threshold for laser-induced plasma breakdown leading to film damage. The polarization effects in the e-beam coatings can be related to the asymmetric electric field intensification induced by the columnar void structure. Our findings provide a fundamental basis for developing strategies to produce laser damage-resistant coatings for UV pulsed laser applications.

36 MATERIALS SCIENCE↗
DOE OSTI2025

Laser damage of crazed electron-beam high-reflectors following infrared and ultraviolet irradiation in the nanosecond pulse regime

Laser damage of optical components can be a limiting factor in scaling the energetics of high-peak and average power laser systems. Specifically for optical coatings, damage under nanosecond pulsed irradiation is initiated by pre-existing defects in the coating layers, including those that cause discontinuities in the structure, like craze lines. Crazing or cracking in a multilayer dielectric optical coating is induced when the overall coating stress is sufficiently tensile, and is an occasionally observed issue when employing more porous deposition techniques like electron-beam evaporation. Here, in this study, electron-beam high-reflectors were fabricated utilizing process parameters that are known to induce crazing based on prior processing history to systematically evaluate the impact of crazing on reflector damage performance for 1064 and 355 nm lasers. The crazing that was observed was apparently nucleated at nodular defects. When the cross-section of these nodules was investigated, it was observed that there were cracks into the fused silica substrate of approximately 5 µm in depth. The craze lines were irradiated with 1064 and 355 nm light at fluences slightly above the onset of damage initiation fluence of the coating. The 1064 nm irradiated sub-apertures exhibit laser damage but with no spatial correlation with the craze line, whereas the 355 nm irradiated area exhibited many damage sites along the craze line. Finite-difference time-domain electric-field simulations were conducted, and ∼2× field amplification in hafnia was observed for the 355 nm wavelength case. The laser damage can be attributed to a slight electric-field intensification coincidental with an area where UV damage-prone precursors are known to occur. The 355 nm laser damage in uncoated fused silica substrates has been previously correlated to initiate through localized UV absorption at the broken silica bonds in the tips of fractures.

Harthcock, Colin [Lawrence Livermore National Labo↗
DOE OSTI2016

Optical damage performance of conductive widegap semiconductors: spatial, temporal, and lifetime modeling

The optical damage performance of electrically conductive gallium nitride (GaN) and indium tin oxide (ITO) films is addressed using large area, high power laser beam exposures at 1064 nm sub-bandgap wavelength. Analysis of the laser damage process assumes that onset of damage (threshold) is determined by the absorption and heating of a nanoscale region of a characteristic size reaching a critical temperature. We use this model to rationalize semi-quantitatively the pulse width scaling of the damage threshold from picosecond to nanosecond timescales, along with the pulse width dependence of the damage threshold probability derived by fitting large beam damage density data. Multi-shot exposures were used to address lifetime performance degradation described by an empirical expression based on the single exposure damage model. A damage threshold degradation of at least 50% was observed for both materials. Overall, the GaN films tested had 5-10 × higher optical damage thresholds than the ITO films tested for comparable transmission and electrical conductivity. This route to optically robust, large aperture transparent electrodes and power optoelectronics may thus involve use of next generation widegap semiconductors such as GaN.

36 MATERIALS SCIENCE↗
DOE OSTI2020

Large-Scale Image Analysis for Investigating Spatio-Temporal Changes in Nuclear DNA Damage Caused by Nitrogen Atmospheric Pressure Plasma Jets

The effective clinical application of atmospheric pressure plasma jet (APPJ) treatments requires a well-founded methodology that can describe the interactions between the plasma jet and a treated sample and the temporal and spatial changes that result from the treatment. In this study, we developed a large-scale image analysis method to identify the cell-cycle stage and quantify damage to nuclear DNA in single cells. The method was then tested and used to examine spatio-temporal distributions of nuclear DNA damage in two cell lines from the same anatomic location, namely the oral cavity, after treatment with a nitrogen APPJ. One cell line was malignant, and the other, nonmalignant. The results showed that DNA damage in cancer cells was maximized at the plasma jet treatment region, where the APPJ directly contacted the sample, and declined radially outward. As incubation continued, DNA damage in cancer cells decreased slightly over the first 4 h before rapidly decreasing by approximately 60% at 8 h post-treatment. In nonmalignant cells, no damage was observed within 1 h after treatment, but damage was detected 2 h after treatment. Notably, the damage was 5-fold less than that detected in irradiated cancer cells. Moreover, examining damage with respect to the cell cycle showed that S phase cells were more susceptible to DNA damage than either G1 or G2 phase cells. The proposed methodology for large-scale image analysis is not limited to APPJ post-treatment applications and can be utilized to evaluate biological samples affected by any type of radiation, and, more so, the cell-cycle classification can be used on any cell type with any nuclear DNA staining.

cellular imaging↗
NASA NTRS1976

Effect of Low Velocity Impact Damage on the Compressive Strength of Graphite/Epoxy Hat-Stiffened Panels

Low velocity impact damage on the compressive strength of graphite/epoxy hat stiffened panels is studied. Fourteen panels, representative of minimum-mass designs for two compression load levels were tested. Eight panels were damaged by impact and the effect on compressive strength was evaluated by comparing the results with data for undamaged panels. The impact tests consisted of firing 1.27 cm diameter aluminum projectiles normal to the plane of the panel at a velocity of approximately 55 m/sec to simulate impact from runway debris. The results of this investigation indicate that impact damage in the panels designed for 0.53 MN/m was contained locally and the damaged panels were capable of carrying the design load. The panels designed for 1.58 MN/m failed between 50 and 58 percent of the design load due to impact damage in the high axial stiffness region. The extent of damage in the high axial stiffness region of both panel designs increased with the magnitude of applied axial load. Damage in this region was the most significant factor in reducing panel strength. Limited damage that was not visually detectable reduced ultimate strength as much as extensive visible damage.

Rhodes, M. D.↗
NASA NTRS1992

A procedure for utilization of a damage-dependent constitutive model for laminated composites

Described here is the procedure for utilizing a damage constitutive model to predict progressive damage growth in laminated composites. In this model, the effects of the internal damage are represented by strain-like second order tensorial damage variables and enter the analysis through damage dependent ply level and laminate level constitutive equations. The growth of matrix cracks due to fatigue loading is predicted by an experimentally based damage evolutionary relationship. This model is incorporated into a computer code called FLAMSTR. This code is capable of predicting the constitutive response and matrix crack damage accumulation in fatigue loaded laminated composites. The structure and usage of FLAMSTR are presented along with sample input and output files to assist the code user. As an example problem, an analysis of crossply laminates subjected to two stage fatigue loading was conducted and the resulting damage accumulation and stress redistribution were examined to determine the effect of variations in fatigue load amplitude applied during the first stage of the load history. It was found that the model predicts a significant loading history effect on damage evolution.

Lo, David C.↗
NASA NTRS1993

Micromechanical simulation of damage progression in carbon phenolic composites

Carbon/phenolic composites are used extensively as ablative insulating materials in the nozzle region of solid rocket motors. The current solid rocket motor (RSRM) on the space shuttle is fabricated from woven rayon cloth which is carbonized and then impregnated with the phenolic resin. These plies are layed up in the desired configuration and cured to form the finished part. During firing, the surface of the carbon/phenolic insulation is exposed to 5000 F gases from the rocket exhaust. The resin pyrolizes and the material chars to a depth which progresses with time. The rate of charring and erosion are generally predictable, and the insulation depth is designed to allow adequate safety margins over the firing time of the motor. However, anomalies in the properties and response of the carbon/phenolic materials can lead to severe material damage which may decrease safety margins to unacceptable levels. Three macro damage modes which were observed in fired nozzles are: ply lift, 'wedge out', and pocketing erosion. Ply lift occurs in materials with plies oriented nearly parallel to the surface. The damage occurs in a region below the charred material where material temperatures are relatively low - about 500 F. Wedge out occurs at the intersection of nozzle components whose plies are oriented at about 45 deg. The corner of the block of material breaks off along a ply interface. Pocketing erosion occurs in material with plies oriented normal to the surface. Thermal expansion is restrained in two directions resulting in large tensile strains and material failure normal to the surface. When a large section of material is removed as a result of damage, the insulation thickness is reduced which may lead to failure of the nozzle due to excessive heating of critical components. If these damage events cannot be prevented with certainty, the designer must increase the thickness of the insulator thus adding to both weight and cost. One of the difficulties in developing a full understanding of these macro damage mechanisms is that the loading environment and the material response to that environment are extremely complex. These types of damage are usually only observed in actual motor firings. Therefore, it is difficult and expensive to evaluate the reliability of new materials. Standard material tests which measure mechanical and thermal properties of test specimens can only provide a partial picture of how the material will respond in the service environment. The development of the ANALOG test procedure which can combine high heating rates and mechanical loads on a specimen will improve the understanding of the interactive effects of the various loads on the system. But a mechanistic model of material response which can account for the heterogeneity of the material, the progression of various micromechanical damage mechanisms, and the interaction of mechanical and thermal stresses on the material is required to accurately correlate material tests with response to service environments. A model based on fundamental damage mechanisms which is calibrated and verified under a variety of loading conditions will provide a general tool for predicting the response of rocket nozzles. The development of a micromechanical simulation technique was initiated and demonstrated to be effective for studying across-ply tensile failure of carbon/phenolic composites.

Slattery, Kerry T.↗
NASA NTRS1999

An Experimental Investigation of Damaged Arresting Gear Tapes for the Langley Aircraft Landing Dynamics Facility

An experimental investigation was performed on damaged arresting gear tapes at the Langley Aircraft Landing Dynamics Facility. The arrestment system uses five pairs of tapes to bring the test carriage to a halt. The procedure used to determine when to replace the tapes consists of a close evaluation of each of the 10 tapes after each run. During this evaluation, each tape is examined thoroughly and any damage observed on the tape is recorded. If the damaged tape does not pass the inspection, the tape is replaced with a new one. For the past 13 years, the most commonly seen damage types are edge fray damage and transverse damage. Tests were conducted to determine the maximum tensile strength of a damaged arresting gear tape specimen. The data indicate that tapes exhibiting transverse damage can withstand higher loads than tapes with edge fray damage.

Mason, Angela J.↗
NASA NTRS2000

Clustered DNA damages induced in isolated DNA and in human cells by low doses of ionizing radiation

Clustered DNA damages-two or more closely spaced damages (strand breaks, abasic sites, or oxidized bases) on opposing strands-are suspects as critical lesions producing lethal and mutagenic effects of ionizing radiation. However, as a result of the lack of methods for measuring damage clusters induced by ionizing radiation in genomic DNA, neither the frequencies of their production by physiological doses of radiation, nor their repairability, nor their biological effects are known. On the basis of methods that we developed for quantitating damages in large DNAs, we have devised and validated a way of measuring ionizing radiation-induced clustered lesions in genomic DNA, including DNA from human cells. DNA is treated with an endonuclease that induces a single-strand cleavage at an oxidized base or abasic site. If there are two closely spaced damages on opposing strands, such cleavage will reduce the size of the DNA on a nondenaturing gel. We show that ionizing radiation does induce clustered DNA damages containing abasic sites, oxidized purines, or oxidized pyrimidines. Further, the frequency of each of these cluster classes is comparable to that of frank double-strand breaks; among all complex damages induced by ionizing radiation, double-strand breaks are only about 20%, with other clustered damage constituting some 80%. We also show that even low doses (0.1-1 Gy) of high linear energy transfer ionizing radiation induce clustered damages in human cells.

NASA Discipline Radiation Health↗
NASA NTRS2011

Full-Scale Test and Analysis of a PRSEUS Fuselage Panel to Assess Damage-Containment Features

Stitched composite technology has the potential to substantially decrease structural weight through enhanced damage containment capabilities. The most recent generation of stitched composite technology, the Pultruded Rod Stitched Efficient Unitized Structure (PRSEUS) concept, has been shown to successfully arrest damage at the sub-component level through tension testing of a three stringer panel with damage in the form of a two-bay notch. In a joint effort undertaken by the National Aeronautics and Space Administration (NASA), the Federal Aviation Administration (FAA), and the Boeing Company, further studies are being conducted to characterize the damage containment features of the PRSEUS concept. A full-scale residual strength test will be performed on a fuselage panel to determine if the load capacity will meet strength, deformation, and damage tolerance requirements. A curved panel was designed, fabricated, and prepared for residual strength testing. A pre-test Finite Element Model (FEM) was developed using design allowables from previous test programs to predict test panel deformation characteristics and margins of safety. Three phases of testing with increasing damage severity include: (1) as manufactured; (2) barely visible impact damage (BVID) and visible impact damage (VID); and (3) discrete source damage (DSD) where the panel will be loaded to catastrophic failure. This paper presents the background information, test plan, and experimental procedure. This paper is the first of several future articles reporting the test preparations, results, and analysis conducted in the test program.

Bergan, Andrew↗
NASA NTRS2010

Micromechanics Modeling of Composites Subjected to Multiaxial Progressive Damage in the Constituents

The high-fidelity generalized method of cells composite micromechanics model is extended to include constituent-scale progressive damage via a proposed damage model. The damage model assumes that all material nonlinearity is due to damage in the form of reduced stiffness, and it uses six scalar damage variables (three for tension and three for compression) to track the damage. Damage strains are introduced that account for interaction among the strain components and that also allow the development of the damage evolution equations based on the constituent material uniaxial stress strain response. Local final-failure criteria are also proposed based on mode-specific strain energy release rates and total dissipated strain energy. The coupled micromechanics-damage model described herein is applied to a unidirectional E-glass/epoxy composite and a proprietary polymer matrix composite. Results illustrate the capability of the coupled model to capture the vastly different character of the monolithic (neat) resin matrix and the composite in response to far-field tension, compression, and shear loading.

Bednarcyk, Brett A.↗
NASA NTRS2013

Automated 3D Damaged Cavity Model Builder for Lower Surface Acreage Tile on Orbiter

The 3D Automated Thermal Tool for Damaged Acreage Tile Math Model builder was developed to perform quickly and accurately 3D thermal analyses on damaged lower surface acreage tiles and structures beneath the damaged locations on a Space Shuttle Orbiter. The 3D model builder created both TRASYS geometric math models (GMMs) and SINDA thermal math models (TMMs) to simulate an idealized damaged cavity in the damaged tile(s). The GMMs are processed in TRASYS to generate radiation conductors between the surfaces in the cavity. The radiation conductors are inserted into the TMMs, which are processed in SINDA to generate temperature histories for all of the nodes on each layer of the TMM. The invention allows a thermal analyst to create quickly and accurately a 3D model of a damaged lower surface tile on the orbiter. The 3D model builder can generate a GMM and the correspond ing TMM in one or two minutes, with the damaged cavity included in the tile material. A separate program creates a configuration file, which would take a couple of minutes to edit. This configuration file is read by the model builder program to determine the location of the damage, the correct tile type, tile thickness, structure thickness, and SIP thickness of the damage, so that the model builder program can build an accurate model at the specified location. Once the models are built, they are processed by the TRASYS and SINDA.

Belknap, Shannon↗
NASA NTRS2014

MMOD Impact Damage to ISS

Paper will describe micrometeoroid and orbital debris (MMOD) damage that has been observed on the International Space Station (ISS). Several hundred documented MMOD damage sites on ISS have been identified through imagery from the windows of ISS modules or docked vehicles. Sites that are observable from ISS or shuttle windows exhibiting distinct features of hypervelocity impact damage are usually greater than 5mm in diameter. Many smaller features are revealed in on-orbit imagery are typically less distinct and difficult to characterize but could be MMOD damage. Additional images of on-orbit damage features have been collected by astronauts during extra vehicular activities. Ground inspection of returned ISS hardware has also contributed to the database of ISS MMOD impact damage. A handful of orbital replacement units (ORU) from the ISS active thermal control and electrical power subsystems were swapped out and returned during the Space Shuttle program. In addition, a reusable logistics module was deployed on ISS for a total 59.4 days on 11 shuttle missions between 2001 and 2011 and then brought back in the shuttle payload bay. All of this returned hardware was subjected to detailed post-flight inspections for MMOD damage, and a database with nearly 1000 impact records has been collected. A description of the largest observed damages will be provided in the paper. In addition, a discussion of significant MMOD impact sites with operational or design aspects will be presented. Some of the ISS modules/subsystems damaged by MMOD to be included in the discussion are (1) Solar Arrays, (2) US and Russian windows, (3) EVA handrails, (4) Radiators, and (5) Russian FGB module.

Hyde, James L.↗
NASA NTRS2018

Investigations of Hail Damage Swaths Using Various Satellite Remote Sensing Platforms

Severe thunderstorms that bring damaging winds and large hail can cause significant damage to agricultural crops. Severe thunderstorms can cause upwards of several hundreds of millions of dollars in damage to agricultural areas. Formal ground surveys are not conducted on these areas of damage, like they are for suspected tornado damaged areas. IF ground surveys were conducted, they would likely be time and resources consuming due to their large spatial extent. Satellite remote sensing has been frequently used in identification and analysis of these hail damage swaths. Previous analysis have looked at the simple change in damaged vegetation to looking at the damage areas in satellite imagery with varying spatial resolutions. One study has even looked at the impacts that these damage swaths can have on the land surface, associated fluxes and how they affect numerical weather prediction. Previous studies have focused on using optical remote (VIS, NIR, SWIR) sensing instruments and derived indices, such as Normalized Difference Vegetation Index (NDVI) for analysis. NDVI is used to monitor the health (greenness) of the vegetation. Optical sensors however are limited by sky conditions over the areas they are imaging and certain bands are further limited by the diurnal cycle. These limitations can lead to sometimes upwards of 7 to 10 day gaps of the surface not being imaged, especially during the height of summer convection. One way to obtain more views of the surface, regardless of the sky conditions or time of day is through the use of synthetic aperture radar (SAR). SAR sensors are active instruments that transmit in the microwave portion of the EM spectrum. The surface and its characteristics will determine the amount of energy scattered back to the sensor. The SAR sensors then measure amplitude and phase of wavelength coming back from surface.

Bell, Jordan R.↗
NASA NTRS2018

Detection of Damage During Quasi-Static Loading of a Single Stringer Panel Using Passive Thermography and Acoustic Emission

The purpose of this paper is to describe the methodology of measuring damage onset and growth in a composite structure during quasi-static loading using passive thermography and acoustic emission. The early detection and measurement of damage progression is important to understand failure modes. A single stringer panel was subjected to quasi-static loading to induce deformation which resulted in the formation of damage between the stiffener flange and skin. The loading was stopped when damage growth was detected. Passive thermography and acoustic emission were used to detect damage in real-time as a function of the applied load. Of particular interest are the small transient thermographic signals resulting from damage formation which can be challenging to detect, as compared to the persistent passive thermography indications of cyclic fatigue loading. We describe a custom developed thermal inspection system for detection of composite damage during quasi-static loading. The thermal results are compared to a two-dimensional multi-layered thermal simulation based on the quadrupole method. Acoustic emission is used to further characterize the damage by comparing the acoustic emission events with the thermal imagery. Results are compared to ultrasonic measurements to document the damage through-the-thickness.

Zalameda, Joseph N.↗
NASA NTRS2019

Observations of MMOD Impact Damage to the ISS

This paper describes meteoroid and orbital debris (MMOD) damage observations on the International Space Station (ISS). Several hundred MMOD damage sites on ISS have been documented using imagery taken from ISS windows. MMOD damage sites visible from ISS windows are typically larger – approximately 5mm diameter and greater – due to the larger viewer-to-surface distance. Closer inspection of these surfaces by astronauts during spacewalks reveals many smaller features that are typically less distinct. Characterization of these features as MMOD or non- MMOD is difficult, but can be partially accomplished by matching physical characteristics of the damage against typical MMOD impact damage observed on ground-based impact tests. Numerous pieces of space-exposed ISS hardware were returned during space shuttle missions. Subsequent ground inspection of this hardware has also contributed to the database of ISS MMOD impact damage. A handful of orbital replacement units (ORUs) from the ISS active thermal control and electrical power subsystems were swapped out and returned during the Space Shuttle program. In addition, a reusable logistics module was deployed on ISS for a total 59.4 days on 11 shuttle missions between 2001 and 2011 and then brought back in the shuttle payload bay. All of this returned hardware was subjected to detailed post-flight inspections for MMOD damage, and a database with over 1,400 impact records has been collected. A description of the largest observed damage features is provided in the paper. In addition, a discussion of significant MMOD impact sites with operational or design aspects is presented. MMOD impact damage to the following ISS modules/subsystems is described: (1) Solar Arrays, (2) US and Russian windows, (3) Extravehicular Activity (EVA) handrails, (4) Radiators, and (5) Russian Functional Cargo Block (FGB) module.

Hyde, James L.↗
NASA NTRSDate not supplied

Understanding Variability in Mechanical Behavior of Adhesively Bonded Sandwich Joints due to Stochastic Material Damage

A mesoscale progressive damage analysis was applied to the analysis of recently tested adhesively bonded sandwich panels, in which ten nominally identical tension loaded panels failed in three different failure modes, with peakloads ranging from 13.0 –16.1 kips. A parametric finite element model for progressive damage analysis of an adhesively bonded joint (ABJ) considering matrix and fiber damage, and delamination cracks in unidirectional and fabric composite sections of the joint, as well as core crushing, and adhesive fracture was developed. The model was developed using Abaqus/Explicit and utilized continuum damage mechanics material models for intralaminar damage in the facesheet and doubler plies, cohesive elements for delamination and adhesive debonding, and discretized cells considering plasticity to model crushing of the aluminum honeycomb core. Analysis predictions obtained with a pristine model agreed well with the average experimental peak load, strain in the joint, and post-test damage states. Then, various methods to incorporate stochastic material variability into ABJ model were evaluated. These methods included simulation of pre-existing matrix damage, pre-existing adhesive porosity, and uniform modification of adhesive properties. These material and manufacturing defects changed the damage mode predictions in some cases. The analysis of stochastic strength due to the considered defects revealed unintuitive damage mode interaction in the ABJ, explaining some structure-property relationships observed experimentally.

Richard Larson↗