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At least 271 records · Page 15

Dimensional stability

The temporal stability of glass and glass-ceramic materials is important to the success of a large diffraction-limited telescope. The results are presented of an experimental study of the dimensional stability of glasses and glass ceramics being considered for substrates of massive diffraction-limited mirrors designed for several years of service in earth orbit. The purpose of the study was to measure the relative change in length of the candidate substrate materials, to the order of 5 parts in 10 to the 8th power, as a function of several years time. The development of monolithic test etalons, the development and improvement of two types of ultra-high precision interferometers, and certain aspects of tests data presently achieved are discussed.

Hocken, R.↗

Ceramic Propellant Injectors Designed and Fabricated

Ceramic propellant injectors offer the potential for order-of-magnitude weight reductions in comparison to conventional metallic injectors and may enable some NASA missions. Injectors constructed of ceramic materials have the inherent advantages of being lighter weight, more erosion resistant, and capable of higher temperature operation than current metallic designs. The use of ceramics may facilitate new designs for a broad range of combustion devices in aero and space applications. In a joint project involving NASA Glenn Research Center's Ceramics and Combustion branches and Case Western Reserve University, a rocket propellant injector faceplate was designed and fabricated using laminated object manufacturing and standard ceramic processing. A number of faceplates have been successfully hot-fire bench tested.

Eckel, Andrew J.↗

Characterization and Glass Formation of JSC-1 Lunar and Martian Soil Simulants

The space exploration mission of NASA requires long duration presence of human being beyond the low earth orbit (LEO), especially on Moon and Mars. Developing a human habitat or colony on these planets would require a diverse range of materials, whose applications would range from structural foundations, (human) life support, (electric) power generation to components for scientific instrumentation. A reasonable and cost-effective approach for fabricating the materials needed for establishing a self-sufficient human outpost would be to primarily use local (in situ) resources on these planets. Since ancient times, glass and ceramics have been playing a vital role on human civilization. A long term project on studying the feasibility of developing glass and ceramic materials using Lunar and Martian soil simulants (JSC-1) as developed by Johnson Space Center has been undertaken. The first step in this on-going project requires developing a data base on results that fully characterize the simulants to be used for further investigations. The present paper reports characterization data of both JSC-1 Lunar and JSC Mars-1 simulants obtained up to this time via x-ray diffraction analysis, scanning electron microscopy, thermal analysis (DTA, TGA) and chemical analysis. The critical cooling rate for glass formation for the melts of the simulants was also measured in order to quantitatively assess the glass forming tendency of these melts. The importance of the glasses and ceramics developed using in-situ resources for constructing human habitats on Moon or Mars is discussed.

Sen, Subhayu↗

Investigation of Ceramic, Graphite, and Chrome-plated Graphite Nozzles on Rocket Engine

The use of ceramic material for rocket nozzles and the effectiveness of preventing oxidation and erosion of graphite nozzles by chrome-plating the internal surface were investigated. A supported ceramic nozzle, cracked by initial operation, was operated a second time without further cracking or damage. Chrome-plating the internal surface of graphite nozzles effectively prevented oxidation and erosion that occurred during operation with unprotected graphite.

CERAMICS↗

Flow Duct Data for Validation of Acoustic Liner Codes for Impedance Eduction

The objective of the study reported here was to acquire acoustic and flow data with hard and lined duct wall duct sections for validation of a liner prediction code being developed at NASA LaRC. Both the mean flowfield and acoustic flowfields were determined in a cross-plane of the rectangular duct. A flow duct facility with acoustic drivers connected to a rectangular (4.7 x 2.0 inch) source section and a linear acoustic liner mounted downstream of the source section was used in this study. The liner section was designed to allow liner materials to be placed on all 4 walls of the duct. The test liner was of the locally-reacting type and was made from a ceramic material. The material, consisting of a tubular structure, was provided by NASA LaRC. The liner was approximately 8.89 cm (3.5 inches) thick. For the current study, only the two "short" sides of the duct were lined with liner material. The other two sides were hard walls. Two especially built instrumentation sections were attached on either sides of the liner section to allow acoustic and flow measurements to be made upstream and downstream of the liner. The two instrumentation duct sections were built to allow measurement of acoustic and flow properties at planes perpendicular to flow upstream and downstream of the liner section. The instrumentation section was also designed to provide a streamwise gradient in acoustic (complex) pressure from which the acoustic particle velocity, needed for the model validation, can be computed. Flow measurements included pressure, temperature, and velocity profiles upstream of the liner section. The in-flow sound pressure levels and phases were obtained with a microphone probe equipped with a nose cone in two cross planes upstream of the liner and two cross plane downstream of the liner. In addition to the acoustic measurements at the cross planes. axial centerline acoustic data was acquired using an axially traversing microphone probe which was traversed from a location upstream of the liner to some distance downstream of the liner. All probes used here had to be calibrated with respect to a standard microphone equipped with a nose cone to allow for the effects of flow.

Ahuja, K. K.↗

Carbon Nanotubes for Human Space Flight

Single-wall carbon nanotubes offer the promise of a new class of revolutionary materials for space applications. The Carbon Nanotube Project at NASA Johnson Space Center has been actively researching this new technology by investigating nanotube production methods (arc, laser, and HiPCO) and gaining a comprehensive understanding of raw and purified material using a wide range of characterization techniques. After production and purification, single wall carbon nanotubes are processed into composites for the enhancement of mechanical, electrical, and thermal properties. This "cradle-to-grave" approach to nanotube composites has given our team unique insights into the impact of post-production processing and dispersion on the resulting material properties. We are applying our experience and lessons-learned to developing new approaches toward nanotube material characterization, structural composite fabrication, and are also making advances in developing thermal management materials and electrically conductive materials in various polymer-nanotube systems. Some initial work has also been conducted with the goal of using carbon nanotubes in the creation of new ceramic materials for high temperature applications in thermal protection systems. Human space flight applications such as advanced life support and fuel cell technologies are also being investigated. This discussion will focus on the variety of applications under investigation.

Scott, Carl D.↗

Acousto-ultrasonic evaluation of ceramic matrix composite materials

Acousto-ultrasonic nondestructive evaluation of ceramic composite specimens with a lithium-alumino-silicate glass matrix reinforced with unidirectional silicon carbide (NICALON) fibers was conducted to evaluate their reserve of strength. Ceramic composite specimens with different amount of damage were prepared by four-point cyclic fatigue loading of the specimens at 500 C for a different number of cycles. The reserve of strength of the specimens was measured as the maximum bending stress recorded during four-pointed bending test with the load monotonically increased until failure occurs. It was observed that the reserve of strength did not correlate with the number of fatigue cycles. However, it was also observed that higher values of the stress wave factor measurements correspond to higher values of the reserve of strength test data. Therefore, these results show that the acousto-ultrasonic approach has the potential of being used to monitor damage and to estimate the reserve of strength of ceramic composites.

Dosreis, Henrique L. M.↗

Ceramics potential in automotive powerplants

The paper addresses the potential that ceramic materials can play an important role in future automotive powerplants - both advanced heat engines and advanced battery systems. A number of related experimental programs are reviewed including ceramics for gasoline and diesel piston engines, gas turbine and Stirling Engines and sodium-sulfur batteries. A strong integrated program to develop ceramics technology is recommended.

Mclean, A. F.↗

On the sintering of silicon carbide

This document deals with the sintering of silicon carbide using pressureless sintering. This technique makes it possible to sinter a primarily covalent material to usable densities up to over 98% thD without having to use a high amount of sinter additives as is the case with other non-oxide ceramic materials. The process takes place rapidly, and it is also possible to produce relatively thick-walled structural parts without major problems. This sheds more light on the true characteristics of silicon carbide in one structural part, since there is no second or nearly no second phase. Heat pressing has improved stability.

Gugel, E.↗

Development of superconducting YBa2Cu3O(x) wires with low resistance electrical contacts

Materials exhibiting superconductivity above liquid nitrogen temperatures (77 K) will enable new applications of this phenomena. One of the first commercial applications of this technology will be superconducting magnets for medical imaging. However, a large number of aerospace applications of the high temperature superconducting materials have also been identified. These include magnetic suspension and balance of models in wind tunnels and resistanceless leads to anemometers. The development of superconducting wires fabricated from the ceramic materials is critical for these applications. The progress in application of a patented fiber process developed by Clemson University for the fabrication of superconducting wires is reviewed. The effect of particle size and heat treatment on the quality of materials is discussed. Recent advances made at Christopher Newport College in the development of micro-ohm resistance electrical contacts which are capable of carrying the highest reported direct current to this material is presented.

Buoncristiani, A. M.↗

Processing of glass-ceramics from lunar resources

The goal is to fabricate useful ceramic materials from the by-products of lunar oxygen production processes. Specifically, the crystal nucleation and growth kinetics of ilmenite-extracted lunar regolith were studied in order to produce glass-ceramics with optimal mechanical, thermal, and abrasion resistant properties. In the initial year of the program, construction and calibration of a high temperature viscometer, used for determining the viscosity of simulated lunar glasses was finished. A series of lunar simulants were also prepared, and the viscosity of each was determined over a range of temperatures. It was found that an increase in the concentration of Fe2O3 decreases the viscosity of the glass. While this may be helpful in processing the glass, Fe2O3 concentrations greater than approximately 10 wt percent resulted in uncontrolled crystallization during viscosity measurements. Impurities (such as Na2O, MnO, and K2O) in the regolith appeared to decrease the viscosity of the parent glass. These effects, as well as those of TiO2 and SiO2 on the processability of the glass, however, remain to be quantified.

Fabes, B. D.↗

Ceramic insulation/multifoil composite for thermal protection of reentry spacecraft

A new type of insulation blanket called Composite Flexible Blanket Insulation is proposed for thermal protection of advanced spacecraft in regions where the maximum temperature is not excessive. The blanket is a composite of two proven insulation materials: ceramic insulation blankets from Space Shuttle technology and multilayer insulation blankets from spacecraft thermal control technology. A potential heatshield weight saving of up to 500 g/sq m is predicted. The concept is described; proof of concept experimental data are presented; and a spaceflight experiment to demonstrate its actual performance is discussed.

Pitts, W. C.↗

Uses of ceramics in microelectronics: A survey

The properties and behavior of ceramic materials used in components for electronic circuitry are examined to appraise the present and future directions for microelectronics, and to suggest further product development, and how innovations may be useful in other technologies. Ceramic and glass insulators, resistors, capacitors, and the use of ceramics and glasses in microcircuitry are discussed along with technology transfer to nonaerospace uses.

Bratschun, W. R.↗

Comparison of the Radiative Two-Flux and Diffusion Approximations

Approximate solutions are sometimes used to determine the heat transfer and temperatures in a semitransparent material in which conduction and thermal radiation are acting. A comparison of the Milne-Eddington two-flux approximation and the diffusion approximation for combined conduction and radiation heat transfer in a ceramic material was preformed to determine the accuracy of the diffusion solution. A plane gray semitransparent layer without a substrate and a non-gray semitransparent plane layer on an opaque substrate were considered. For the plane gray layer the material is semitransparent for all wavelengths and the scattering and absorption coefficients do not vary with wavelength. For the non-gray plane layer the material is semitransparent with constant absorption and scattering coefficients up to a specified wavelength. At higher wavelengths the non-gray plane layer is assumed to be opaque. The layers are heated on one side and cooled on the other by diffuse radiation and convection. The scattering and absorption coefficients were varied. The error in the diffusion approximation compared to the Milne-Eddington two flux approximation was obtained as a function of scattering coefficient and absorption coefficient. The percent difference in interface temperatures and heat flux through the layer obtained using the Milne-Eddington two-flux and diffusion approximations are presented as a function of scattering coefficient and absorption coefficient. The largest errors occur for high scattering and low absorption except for the back surface temperature of the plane gray layer where the error is also larger at low scattering and low absorption. It is shown that the accuracy of the diffusion approximation can be improved for some scattering and absorption conditions if a reflectance obtained from a Kubelka-Munk type two flux theory is used instead of a reflection obtained from the Fresnel equation. The Kubelka-Munk reflectance accounts for surface reflection and radiation scattered back by internal scattering sites while the Fresnel reflection only accounts for surface reflections.

Spuckler, Charles M.↗

Material for Fast Cutting

New material for cutting tools increases productivity of machining processes. Material, called Iscanite (or equivalent), based on silicon nitride contains more than 90 percent silicon. Combines impact resistance close to that of coated carbides with heat and wear resistance close to those of aluminum oxide ceramics. Material used for cutting on old or new machine tools and makes it possible to exploit fully power and speed of machine.

Perez, A.↗