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DOE OSTI2022

Investigation of Inverse Temperature Effects During Thermal-Radiation Aging of Semicrystalline Cable Insulation

Inverse temperature effects were observed for semi-crystalline polymers subjected to combined thermal and irradiation aging. The mechanical durability of materials aged at low temperatures degrades with dose faster than at high temperatures. In this paper, two crosslinked polyethylene (XLPE) and two ethylene propylene rubber (EPR) type nuclear cable insulations were exposed to thermal-radiation aging at 100Gy/h up to 30Mrad and three temperatures (26°C, 50°C, 90°C). Their mass change and color change after aging were analyzed.

Ni, Yelin↗

DOE OSTI2023

A genomic region associated with iteroparous spawning phenology is linked with age‐at‐maturity in female steelhead trout

Abstract Age‐at‐maturity and iteroparity are two life history variations of steelhead trout ( Oncorhynchus mykiss ) that are believed to increase population resilience and stability. While repeat‐spawning individuals are thought to have historically made up a substantial portion of the reproductive population in the Columbia River and the majority of females still attempt outmigration as kelts, return rates of repeat‐spawner are low throughout the basin and below 1% for the furthest migrating stocks. Notably, outmigrating adults exhibit variation in rematuration phenology, displaying either “consecutive” (reproduce immediately the following season) or “skip” (delay spawning for future seasons) spawning patterns. Here, we use low coverage whole genome sequencing of consecutive versus skip spawning female Columbia River steelhead from two populations to test for genomic differences between these two iteroparous phenotypes. We identified genomic regions on several chromosomes which were associated with the phenology of iteroparity, including a region on chromosome 25 containing two genes, estradiol receptor beta ( ER β) and glycoprotein hormone beta‐5 ( GPHB5 ), which, in mammals, are estrogen‐sensitive and expressed in reproductive tissues. Allele frequencies in this ER β/ GPHB5 region differed among female steelhead of different age at maturity, but not males. These genes also shared an island of linkage disequilibrium with the SIX6 gene, 600Kbp away on the same chromosome, a region of known association with age‐at‐maturity. These observations contribute to growing evidence that age‐at‐maturity and the phenology of iteroparity are determined by overlapping physiological processes and genetic pathways.

Willis, Stuart↗

DOE OSTI2021

A Modified Network Alteration Model to Predict Quasi-Static Behavior of the Cross-Linked Polymers During Hydrolytic Aging

Abstract The network alteration theory is utilized to capture the effects of hydrolytic aging on the mechanical integrity of the polymer matrix. Hydrolytic degradation generally considered as a result of two simultaneous chemical phenomena; (i) reduction of the cross-links, and (ii) active chain loss. Assuming the alteration of the chain density is identical to the change of the number average molecular weight along the aging trajectory, the strain energy of polymer matrix can be rewritten as a function of deformation, deformation history, storage time, and aging temperature. The proposed model includes only five physically inspired material parameters. Thus, while it is computationally efficient, it shows good agreement with own experimental data, which performed on various range of accelerated aging temperatures and times. With respect to its computational efficiency, simplicity, accuracy, and interpret-ability, the model is a good choice for advanced implementations in FE programs.

Bahrololoumi, Amir↗

DOE OSTI2022

A Micro-Mechanical Constitutive Model to Predict Hygrothermal Aging of Cross-Linked Polymers

Abstract A multi-physics material model is presented to describe the effects of temperature, oxygen, and humidity on the constitutive response of cross-linked polymers. The effect of hygrothermal damage on the mechanical integrity of the polymer matrix can be considered as the result of damage accumulation of two independent aging mechanism namely, i) thermo-oxidative, and ii) hydrolytic aging. In order to capture the mutual effects of thermo-oxidative and hydrolytic aging, an assumption has been made that each of the aging phenomenon can be superposed to each other. In fact, each of them works independently and as a result, they can compete with each other. Utilizing the theory of network decomposition, all phenomena and their correlation were modeled and thus, the strain energy function of the polymer matrix is written with respect to four independent mechanisms, i) the shrinking original matrix that has neither been attacked by water nor oxygen, ii) conversion of the first network to two new network due to the reduction and formation of cross-links, and iii) energy loss from network degradation due to attack of the water molecules to polymer active agents. Moreover, the proposed model is micro-mechanically based and is mainly relevant on thin samples due to our underlying assumption of homogeneous diffusion of oxygen and water throughout the matrix. The model has been validated against extensive data-sets obtained from experiments we specifically designed for concept validation.

Bahrololoumi, Amir↗

DOE OSTI2022

Perspective—On the Safety of Aged Lithium-Ion Batteries

Concerns about the safety of lithium-ion batteries have motivated numerous studies on the response of fresh cells to abusive, off-nominal conditions, but studies on aged cells are relatively rare. This perspective considers all open literature on the thermal, electrical, and mechanical abuse response of aged lithium-ion cells and modules to identify critical changes in their behavior relative to fresh cells. We outline data gaps in aged cell safety, including electrical and mechanical testing, and module-level experiments. Understanding how the abuse response of aged cells differs from fresh cells will enable the design of more effective energy storage failure mitigation systems.

25 ENERGY STORAGE↗

DOE OSTI2025

Physics-Based Analysis of Cell Imbalances and Aging in Lithium-Ion Battery Modules and Packs

Lithium-ion battery (LIB) packs are a key solution for grid-scale energy storage, enabling grid resilience and supporting critical infrastructure. LIB modules and packs experience current imbalances and uneven cell aging due to various design and operational factors, and require a battery management system (BMS) to continuously monitor and control. In this context, a physics-based modeling framework for LIB modules and packs (liionpack) was enhanced to identify design and control strategies that minimize current imbalance and improve module/pack operation. Simulations of an 8-cell parallel-connected module demonstrate that reducing current imbalance leads to more uniform cell aging and improved module/pack-level degradation predictions. The analysis shows that current imbalance are affected by the electrical resistances. Terminal location significantly affects imbalance, with opposite-end terminal connections at intermediate branches minimizing the imbalance, and the pack circuit construction influences the accuracy of physics-based analysis at the pack scale. This framework enables design optimization of modules and packs through a fast and easy evaluation of pack performance and aging, and supports the development of aging-informed balancing strategies compatible with BMS implementation. Thereby, offering practical pathways to improve reliability and cycle life predictions in large-scale battery energy storage systems.

Ayalasomayajula, Surya Mitra [Oak Ridge National L↗

DOE OSTI2025

Data for Soil Fertility Management for Sustainable Miscanthus × giganteus Production: Increased Tiller Weight from Nitrogen Management Explains Yield Gains in Aged Miscanthus

Aging-related yield decline in Miscanthus × giganteus (miscanthus) remains a major constraint to sustainable biomass production. This study evaluated how nitrogen (N) management and soil fertility influence yield-component traits and productivity in aging miscanthus. Trials were conducted at two sites established in 2008 at the University of Illinois Energy Farm, Urbana, IL. (i) The Sun Grant trial received 0, 60, and 120 kg N ha−1 annually until 2015. Starting 2021, half of each plot received 60 or 120 kg N ha−1, resulting in six legacy-contemporary treatments: 0N–0N, 0N–120N, 60N–0N, 60N–60N, 120N–0N, 120N–120N. (ii) The Energy Farm trial remained unfertilized until 2014, when one half of each plot received 56 kg N ha−1, forming two treatments: 0N–0N, 0N–56N. Sun Grant trial results showed N fertilization increased tiller density (tillers m−2) and tiller weight (g tiller−1) in juvenile to early-mature miscanthus (2011–2015). After N withdrawal, both traits declined (20 % and 40 %), though legacy effects persisted in tiller weight in the aging stands (2020–2023). Contemporary N had little effect on tiller density but increased tiller weight by 34 %–77 %, resulting in 23 %–106 % higher machine-harvested biomass yield in 0–120N, 60-60N, and 120-120N plots. At the Energy Farm trial, 0N–56N plots yielded 59 %–108 % more biomass than 0N–0N. Soil total N increased (Sun Grant: 47 % by 2020; Energy Farm: 58 % by 2023), while Mehlich-3 P (42 %–44 %) and K (21 %–46 %) declined. These findings identify tiller weight as a key determinant of biomass yield in aging miscanthus and highlight the need for P and K management for long-term productivity.

miscanthus↗

DOE OSTI2023

Structural aging of human neurons is opposite of the changes in schizophrenia

Human mentality develops with age and is altered in psychiatric disorders, though their underlying mechanism is unknown. In this study, we analyzed nanometer-scale three-dimensional structures of brain tissues of the anterior cingulate cortex from eight schizophrenia and eight control cases. The distribution profiles of neurite curvature of the control cases showed a trend depending on their age, resulting in an age-correlated decrease in the standard deviation of neurite curvature (Pearson’s r = -0.80, p = 0.018). In contrast to the control cases, the schizophrenia cases deviate upward from this correlation, exhibiting a 60% higher neurite curvature compared with the controls (p = 7.8 × 10 -4 ). The neurite curvature also showed a correlation with a hallucination score (Pearson’s r = 0.80, p = 1.8 × 10 -4 ), indicating that neurite structure is relevant to brain function. This report is based on our 3D analysis of human brain tissues over a decade and is unprecedented in terms of the number of cases. We suggest that neurite curvature plays a pivotal role in brain aging and can be used as a hallmark to exploit a novel treatment of schizophrenia.

59 BASIC BIOLOGICAL SCIENCES↗

DOE OSTI2022

Accelerated beta radiation aging of interlayer titanium nitride in gallium nitride contacts

Currently, there is no good way to determine the influence of the radiation on the aging of betavoltaic electrical contacts. Here, this work tested a method to accelerate the aging of the contacts inside a betavoltaic by enhancing energy deposition within the interfacial region of interest. An electrical contact of gold-titanium on gallium nitride was aged by exposure to tritium betas and electrons in a beamline. The interface stoichiometry was compared to the electrical performance of the contact. The method to age the betavoltaic component could help predict lifetime performance of the internal electrical contacts and provide assurance of deployment reliability.

36 MATERIALS SCIENCE↗

DOE OSTI2022

Photosynthesis in aging perennial and leaf nitrogen

Perennial energy grasses are a fundamental component of the emerging bioeconomy. While their yield dynamics and environmental services are being widely studied, little attention has been given to how the physiological changes associated with perenniality (e.g., nutrient cycling) that underpin yield and environmental services, change as a function of age. Across species, perennial grasses show a photosynthetic decline as a function of stand age, however, the physiological drivers of this age-related decline are poorly understood. In this manuscript we ask: by how much does nitrogen dilution in larger older plants contribute to this photosynthetic decline? Our results support the hypothesis that nitrogen dilution did not limit photosynthesis in mature stands. Compared per unit of area-based leaf nitrogen, photosynthesis of fertilized mature stands was still 26% lower than unfertilized juvenile stands. We hypothesize that the lack of late-season carbohydrate sinks may instead drive the age-related decline in photosynthesis.

Tejera, Mauricio↗

DOE OSTI2020

Mechanistic Understanding of Silver Sorbent Aging Processes in Off-Gas Treatment

The effect of aging in various off-gas streams including dry air, humid air, 1% NO/N 2 , 2% NO 2 /air, and a gas mixture consisting of 99.25% humid air (dew point: -15 °C), 0.25% NO/N 2 , and 0.5% NO 2 /air in terms of concentration on reduced silver exchanged mordenite (Ag 0 Z) and silver functionalized silica aerogel (Ag 0 -aerogel) were studied in this project. Utilizing simple and sophisticated experimental information combined with molecular and macroscopic mechanistic modeling, this project has significantly advanced the current understanding of aging for silver bearing adsorbents in nuclear-fuel-reprocessing off-gas streams. In addition, this project has produced models that can be utilized to predict the influence of adsorbent aging on the uptake kinetics and capacity of aged adsorbents for iodine and iodine-containing organic compounds. The results of the study have been published in the open literature, and can be used to help DOE better predict the removal of radioactive gases from nuclear-fuel-reprocessing off-gas streams.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗

DOE OSTI2022

Ageing Management for Extended Long-Term Dry Storage of Spent Nuclear Fuel and Transportation

The principal objectives of the Coordinated Research Project (CRP) and CRADA were to (1) investigate how ageing effects leading to degradation of materials used in the spent fuel dry storage systems could be managed by ageing management programs (AMPs) and (2) using existing AMPs as a basis, establish guidance on how to develop, generate, and maintain AMPs for dry storage systems of spent nuclear fuel (SNF) that can be accomplished in various ways. The PI (Dr. Liu) is an internationally recognized expert on ageing management for license renewal of nuclear power plants and independent spent fuel dry storage installations. Dr. Liu was invited by IAEA to participate in this CRP and served as Chair of the Working Group, supporting the IAEA CRP Lead, with other members from Argentina, the Czech Republic, France, Germany, Hungary, Japan, Pakistan, Spain, Switzerland, United Kingdom, and the United States of America. Argonne’s scope of work in the CRADA for the CRP included (1) ageing management guidance documents developed by Argonne for DOE and used by the Nuclear Regulatory Commission (NRC) and industry and (2) research leveraged from the DOE Office of Nuclear Energy on the mechanical properties of high-burnup fuel cladding and the ARG-US remote monitoring systems technology developed for the DOE Packaging Certification Program, Office of Packaging and Transportation, Office of Environmental Management.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

DOE OSTI2023

Role of n-phenyl-β-naphthylamine in the Acid-Nitroplasticizer Thermal Aging (ANTA) Experiment

A short-term aging study, which was named as Acid-Nitroplasticizer Thermal Aging (ANTA), was conducted to explore the complex chemistry between n-phenyl-β-naphthylamine (PBNA), HNO x , and nitroplasticizer (NP). Aging of NP with PBNA and acid treatments have demonstrated that PBNA is an effective antioxidant and an anti-hydrolytic agent (e.g., inhibits HNO 3 ) and have allowed the identification of nitroso-PBNA (PBNA-NO). The direct conversion of PBNA to PBNA-NO via scavenging of HONO, known as nitrosation, is a preceding event of PBNA nitration, which provides evidence to the HONO elimination as the key mechanism in the early stage of NP aging. Through the kinetics of both nitrosation and nitration, the accuracy of a prediction on PBNA consumption in NP degradation is further improved.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2023

A mathematical approach to survey electrochemical impedance spectroscopy for aging in lithium-ion batteries

Electrochemical impedance spectroscopy (EIS) is a valuable technique to detect the health status and aging phenomena in lithium-ion batteries (LiB). Equivalent circuit modeling (ECM) is conventionally used when interpreting EIS data and gaining physical insights into the aging mechanisms. However, performing ECM is resource intensive and expert-level of knowledge is usually required to select suitable models and fitting parameters. This article presents a quick and user-friendly data analysis algorithm as an alternative to ECM by mathematically fitting geometric features in Nyquist plots and obtaining the growth trends of the features. The evolving trends in the Nyquist plots, such as chord lengths of the arcs and interception points, are consistent with the growth of resistance components obtained using ECM with R 2 values from 0.67 to 0.99, and therefore can be used as indicators of battery aging. Our results show that the quick-fitting approach is suitable for analyzing a series of EIS data acquired during battery cycling and identifying the underlying aging mechanisms.

Chen, Bor-Rong↗

DOE OSTI2020

Clarissa Family Age from the Yarkovsky Effect Chronology

The Clarissa family is a small collisional family composed of primitive C-type asteroids. It is located in a dynamically stable zone of the inner asteroid belt. In this work we determine the formation age of the Clarissa family by modeling planetary perturbations as well as thermal drift of family members due to the Yarkovsky effect. Simulations were carried out using the SWIFT-RMVS4 integrator modified to account for the Yarkovsky and Yarkovsky–O’Keefe–Radzievskii–Paddack (YORP) effects. We ran multiple simulations starting with different ejection velocity fields of fragments, varying proportion of initially retrograde spins, and also tested different Yarkovsky/YORP models. Our goal was to match the observed orbital structure of the Clarissa family which is notably asymmetrical in the proper semimajor axis, a {sub p}. The best fits were obtained with the initial ejection velocities ≲20 m s{sup −1} of diameter D ≃ 2 km fragments, ∼4:1 preference for spin-up by YORP, and assuming that ≃80% of small family members initially had retrograde rotation. The age of the Clarissa family was found to be t {sub age} = 56 ± 6 Myr for the assumed asteroid density ρ = 1.5 g cm{sup −3}. Small variation of density to smaller or larger value would lead to slightly younger or older age estimates. This is the first case where the Yarkovsky effect chronology has been successfully applied to an asteroid family younger than 100 Myr.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2021

Two Young Planetary Systems around Field Stars with Ages between 20 and 320 Myr from TESS

Planets around young stars trace the early evolution of planetary systems. We report the discovery and validation of two planetary systems with ages ≲300 Myr from observations by the Transiting Exoplanet Survey Satellite (TESS). The 40--320 Myr old G star TOI-251 hosts a 2.74{sub −0.18}{sup +0.18} R{sub ⊕} mini-Neptune with a 4.94 day period. The 20--160 Myr old K star TOI-942 hosts a system of inflated Neptune-sized planets, with TOI-942b orbiting in a period of 4.32 days with a radius of 4.81{sub −0.20}{sup +0.20} R{sub ⊕} and TOI-942c orbiting in a period of 10.16 days with a radius of 5.79{sub −0.18}{sup +0.19} R{sub ⊕}. Though we cannot place either host star into a known stellar association or cluster, we can estimate their ages via their photometric and spectroscopic properties. Both stars exhibit significant photometric variability due to spot modulation, with measured rotation periods of ∼3.5 days. These stars also exhibit significant chromospheric activity, with age estimates from the chromospheric calcium emission lines and X-ray fluxes matching that estimated from gyrochronology. Both stars also exhibit significant lithium absorption, similar in equivalent width to well-characterized young cluster members. TESS has the potential to deliver a population of young planet-bearing field stars, contributing significantly to tracing the properties of planets as a function of their age.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2022

Synthesizing Stellar Populations in South Pole Telescope Galaxy Clusters. I. Ages of Quiescent Member Galaxies at 0.3 < $\textit{z}$ < 1.4

Using stellar population synthesis models to infer star formation histories (SFHs), we analyze photometry and spectroscopy of a large sample of quiescent galaxies that are members of Sunyaev–Zel'dovich (SZ)-selected galaxy clusters across a wide range of redshifts. We calculate stellar masses and mass-weighted ages for 837 quiescent cluster members at 0.3 < $\textit{z}$ < 1.4 using rest-frame optical spectra and the Python-based Prospector framework, from 61 clusters in the SPT-GMOS Spectroscopic Survey (0.3 < $\textit{z}$ < 0.9) and three clusters in the SPT Hi-z cluster sample (1.25 < $\textit{z}$ < 1.4). We analyze spectra of subpopulations divided into bins of redshift, stellar mass, cluster mass, and velocity-radius phase-space location, as well as by creating composite spectra of quiescent member galaxies. We find that quiescent galaxies in our data set sample a diversity of SFHs, with a median formation redshift (corresponding to the lookback time from the redshift of observation to when a galaxy forms 50% of its mass, $t_{50}$) of $\textit{z}$ = 2.8 ± 0.5, which is similar to or marginally higher than that of massive quiescent field and cluster galaxy studies. We also report median age–stellar mass relations for the full sample (age of the universe at $t_{50}$ (Gyr) = 2.52 (±0.04)–1.66 (±0.12) log$_{10}(M/10^{11}M_⊙$)) and recover downsizing trends across stellar mass; we find that massive galaxies in our cluster sample form on aggregate ~0.75 Gyr earlier than lower-mass galaxies. We also find marginally steeper age–mass relations at high redshifts, and report a bigger difference in formation redshifts across stellar mass for fixed environment, relative to formation redshifts across environment for fixed stellar mass.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2020

Evidence for Cosmic Acceleration Is Robust to Observed Correlations between Type Ia Supernova Luminosity and Stellar Age

Type Ia supernovae (SNe Ia) are powerful standardizable candles for constraining cosmological models and provided the first evidence of the accelerated expansion of the universe. Their precision derives from empirical correlations, now measured from >1000 SNe Ia, between their luminosities, light-curve shapes, colors, and most recently with the stellar mass of their host galaxy. As mass correlates with other galaxy properties, alternative parameters have been investigated to improve SN Ia standardization though none have been shown to significantly alter the determination of cosmological parameters. We re-examine a recent claim, based on 34 SN Ia in nearby passive host galaxies, of a 0.05 mag Gyr -1 dependence of standardized SN Ia luminosity on host age, which, if extrapolated to higher redshifts, would be a bias up to 0.25 mag, challenging the inference of dark energy. We reanalyze this sample of hosts using both the original method and a Bayesian hierarchical model and find after a fuller accounting of the uncertainties the significance of a dependence on age to be ≤2σ and ~1σ after the removal of a single poorly sampled SN Ia. Here, to test the claim that a trend seen in old stellar populations can be applied to younger ages, we extend our analysis to a larger sample that includes young hosts. We find the residual dependence of host age (after all standardization typically employed for cosmological measurements) to be consistent with zero for 254 SNe Ia from the Pantheon sample, ruling out the large but low significance trend seen in passive hosts.

79 ASTRONOMY AND ASTROPHYSICS↗