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NASA NTRS1982

Low-gravity fluid flows

The behavior of fluids in micro-gravity conditions is examined, with particular regard to applications in the growth of single crystals. The effects of gravity on fluid behavior are reviewed, and the advent of Shuttle flights are noted to offer extended time for experimentation and processing in a null-gravity environment, with accelerations resulting solely from maneuvering rockets. Buoyancy driven flows are considered for the cases stable-, unstable-, and mixed-mode convection. Further discussion is presented on g-jitter, surface-tension gradient, thermoacoustic, and phase-change convection. All the flows are present in both gravity and null gravity conditions, although the effects of buoyancy and g-jitter convection usually overshadow the other effects while in a gravity field. Further work is recommended on critical-state and sedimentation processes in microgravity conditions.

Ostrach, S.↗

NASA NTRS2001

Viscoplastic Model Development to Account for Strength Differential: Application to Aged Inconel 718 at Elevated Temperature

The magnitude of yield and flow stresses in aged Inconel 718 are observed to be different in tension and compression. This phenomenon, called the Strength differential (SD), contradicts the metal plasticity axiom that the second deviatoric stress invariant alone is sufficient for representing yield and flow. Apparently, at least one of the other two stress invariants is also significant. A unified viscoplastic model was developed that is able to account for the SD effect in aged Inconel 718. Building this model involved both theory and experiments. First, a general threshold function was proposed that depends on all three stress invariants and then the flow and evolution laws were developed using a potential-based thermodynamic framework. Judiciously chosen shear and axial tests were conducted to characterize the material. Shear tests involved monotonic loading, relaxation, and creep tests with different loading rates and load levels. The axial tests were tension and compression tests that resulted in sufficiently large inelastic strains. All tests were performed at 650 C. The viscoplastic material parameters were determined by optimizing the fit to the shear tests, during which the first and the third stress invariants remained zero. The threshold surface parameters were then fit to the tension and compression test data. An experimental procedure was established to quantify the effect of each stress invariant on inelastic deformation. This requires conducting tests with nonproportional three-dimensional load paths. Validation of the model was done using biaxial tests on tubular specimens of aged Inconel 718 using proportional and nonproportional axial-torsion loading. These biaxial tests also helped to determine the most appropriate form of the threshold function; that is, how to combine the stress invariants. Of the set of trial threshold functions, the ones that incorporated the third stress invariant give the best predictions. However, inclusion of the first stress invariant does not significantly improve the model predictions. The model shows excellent predictive capability for nonproportional load paths. Additionally, it reduces to the well-known models of Mises Drucker and Drucker-Prager. The requisite experiments involve reasonably simple load paths in the axial-shear stress plane and hence can be performed on a variety of different materials: be they metallic, geological. polymeric, ceramic or granular. The general form of the threshold function allows representation of inelastic deformation in a range of materials.

Iyer, Saiganesh↗

NASA NTRS1984

Ribbon Reduces Spiking in Electron-Beam Welding

Spiking in electron-beam welding reduced by placing high-vapor-pressure substance along path of electron beam. Strip of metal having vapor pressure higher than base metal at same temperature placed in slot machined along weld line. Strip vaporizes as beam strikes it, and vapor pressure keeps surface tension from closing off top of channel. Technique used successfully on nickel alloys and aluminum alloys and effective on steel and titanium.

Olson, R. E.↗

NASA NTRS1992

Heat transfer and fluid flow in floating-zone crystal growth with a mostly covered melt surface

Computer simulation was conducted to study a modified floating-zone crystal growth process, in which the melt surface is mostly covered with a heated ring. The growth of 6-mm diameter single crystals of NaNO3 was considered, and the effects of the following parameters were studied: (1) temperature of the ring, (2) growth rate, (3) surface tension-temperature coefficient of the melt, (4) thermal expansion coefficient of the melt, and (5) gravity. It was demonstrated that thermocapillary convection in the melt zone is reduced significantly in this modified process. The model was checked against the measured lengths of the meniscus near the growth front and axial temperature distribution in a growing crystal, and the agreement was good.

Lan, C. W.↗

NASA NTRS1992

Potential pressurized payloads: Fluid and thermal experiments

Space Station Freedom (SSF) presents the opportunity to perform long term fluid and thermal experiments in a microgravity environment. This presentation provides perspective on the need for fluids/thermal experimentation in a microgravity environment, addresses previous efforts, identifies possible experiments, and discusses the capabilities of a proposed fluid physics/dynamics test facility. Numerous spacecraft systems use fluids for their operation. Thermal control, propulsion, waste management, and various operational processes are examples of such systems. However, effective ground testing is very difficult. This is because the effect of gravity induced phenomena, such as hydrostatic pressure, buoyant convection, and stratification, overcome such forces as surface tension, diffusion, electric potential, etc., which normally dominate in a microgravity environment. Hence, space experimentation is necessary to develop and validate a new fluid based technology. Two broad types of experiments may be performed on SSF: basic research and applied research. Basic research might include experiments focusing on capillary phenomena (with or without thermal and/or solutal gradients), thermal/solutal convection, phase transitions, and multiphase flow. Representative examples of applied research might include two-phase pressure drop, two-phase flow instabilities, heat transfer coefficients, fluid tank fill/drain, tank slosh dynamics, condensate removal enhancement, and void formation within thermal energy storage materials. In order to better support such fluid/thermal experiments on board SSF, OSSA has developed a conceptual design for a proposed Fluid Physics/Dynamics Facility (FP/DF). The proposed facility consists of one facility rack permanently located on SSF and one experimenter rack which is changed out as needed to support specific experiments. This approach will minimize the on-board integration/deintegration required for specific experiments. The FP/DF will have acceleration/vibration compensation, power and thermal interfaces, computer command/data collection, a video imaging system, and a portable glove box for operations. This facility will allow real-time astronaut interaction with the testing.

Swanson, Theodore D.↗

NASA NTRS1999

Surface Tension Driven Convection Experiment-2 (STDCE-2)

Thermocapillary flows are known to become oscillatory (time-periodic), but how and when they become oscillatory in containers of unit-order aspect ratio are not yet fully understood. The present work is a part of our continuous effort to obtain a better understanding of the phenomenon. Thermocapillary flow experiments in normal gravity are limited to a narrow parametric range in order to minimize gravity and buoyancy effects, which is an important reason for our lack of full understanding of the oscillation phenomenon. One important unanswered question is what role, if any, free surface deformation plays in the oscillation mechanism. For that reason we performed thermocapillary flow experiments, called the Surface Tension Driven Convection Experiment-2 (STDCE-2), aboard the USML-2 Spacelab in 1995. The main objectives of the experiments were to investigate oscillatory thermocapillary flows in microgravity and to clarify the importance of free surface deformation in such flows. Steady and oscillatory thermocapillary flows were generated in cylindrical containers by employing two heating modes. A CO2 laser with adjustable power and beam diameter was used in the Constant Flux (CF) configuration to heat the free surface. The other configuration investigated in STDCE-2 was the Constant Temperature (CT) configuration in which a submerged cylindrical cartridge heater placed at the symmetry (axial) axis of the test container heated the fluid. Both heating modes cause non-uniform temperature distributions on the free surface, which generates thermocapillary flow. The flow field was investigated by flow visualization, and the temperature field was measured by thermistors and an infrared imager. The free surface shape and motion were measured by a Ronchi system. The hardware performed well and we were able to conduct more tests than originally planned. From the successful experiments a large amount of data was acquired. The analysis of the data is now nearly complete. Some important results are presented and discussed herein.

Masud, J.↗

NASA NTRS1974

SS/RCS surface tension propellant acquisition/expulsion tankage technology program

An evaluation of published propellant physical property data together with bubble point tests of fine-mesh screen in propellants, was conducted. The effort consisted of: (1) the collection and evaluation of pertinent physical property data for hydrazine (N2H4), monomethylhydrazine (MMH), and nitrogen tetroxide (N2O4); (2) testing to determine the effect of dissolved pressurant gas, temperature, purity, and system cleanliness or contamination on system bubble point, and (3) the compilation and publishing of both the literature and test results. The space shuttle reaction control system (SS/RCS) is a bipropellant system using N2O4 and MMH, while the auxiliary power system (SS/APU) employs monopropellant N2H4. Since both the RCS and the APU use a surface tension device for propellant acquisition, the propellant properties of interest are those which impact the design and operation of surface tension systems. Information on propellant density, viscosity, surface tension, and contact angle was collected, compiled, and evaluated.

Source record↗

NASA NTRS1992

Crack-mouth displacements for semielliptical surface cracks subjected to remote tension and bending loads

The exact analytical solution for an embedded elliptical crack in an infinite body subjected to arbitrary loading was used in conjunction with the finite element alternating method to obtain crack-mouth-opening displacements (CMOD) for surface cracks in finite plates subjected to remote tension. Identical surface-crack configurations were also analyzed with the finite element method using 20-noded element for plates subjected to both remote tension and bending. The CMODs from these two methods generally agreed within a few percent of each other. Comparisons made with experimental results obtained from surface cracks in welded aluminum alloy specimens subjected to tension also showed good agreement. Empirical equations were developed for CMOD for a wide range of surface-crack shapes and sizes subjected to tension and bending loads. These equations were obtained by modifying the Green-Sneddon exact solution for an elliptical crack in an infinite body to account for finite boundary effects. These equations should be useful in monitoring surface-crack growth in tests and in developing complete crack-face-displacement equations for use in three-dimensional weight-function methods.

Raju, Ivatury S.↗

NASA NTRS1998

Convective Instability of a Gravity Modulated Fluid Layer with Surface Tension Variation

Gravity modulation of an unbounded fluid layer with surface tension variations along its free surface is investigated. In parameter space of (wavenumber, Marangoni number) modulation has a destabilizing effect on the unmodulated neutral stability curve for large Prandtl number, Pr, and small modulation frequency, Omega, while a stabilizing effect is observed for small Pr and large Omega. As Omega yields infinity, the modulated neutral stability curves approach the unmodulated neutral stability curve. At certain values of Pr and L2 multiple minima are observed and the neutral stability curves become highly distorted. Closed regions of subharmonic instability are also observed. Alternating regions of synchronous and subharmonic instability separated by very thin stable regions are observed in (1/Omega,g(sub 1)) space for the singly diffusive cases. Quasiperiodic behavior in addition to the synchronous and subharmonic responses, are observed for the case of a double diffusive fluid layer. Minimum acceleration amplitudes were observed to closely correspond with a subharmonic response, Lambda(sub im) = Omega/2 .

Skarda, J. Raymond Lee↗

NASA NTRS1974

Effects of proof loads and combined mode loadings on fracture and flaw growth characteristics of aerospace alloys

This experimental program was undertaken to determine the effects of (1) combined tensile and bending loadings, (2) combined tensile and shear loadings, and (3) proof overloads on fracture and flaw growth characteristics of aerospace alloys. Tests were performed on four alloys: 2219-T87 aluminum, 5Al-2.5Sn (ELl) titanium, 6Al-4V beta STA titanium and high strength 4340 steel. Tests were conducted in room air, gaseous nitrogen at -200F (144K), liquid nitrogen and liquid hydrogen. Flat center cracked and surface flawed specimens, cracked tube specimens, circumferentially notched round bar and surface flawed cylindrical specimens were tested. The three-dimensional photoelastic technique of stress freezing and slicing was used to determine stress intensity factors for surface flawed cylindrical specimens subjected to tension or torsion. Results showed that proof load/temperature histories used in the tests have a small beneficial effect or no effect on subsequent fracture strength and flaw growth rates.

Shah, R. C.↗

NASA NTRS2001

Contact Angles and Surface Tension of Germanium-Silicon Melts

Precise knowledge of material parameters is more and more important for improving crystal growth processes. Two important parameters are the contact (wetting) angle and the surface tension, determining meniscus shapes and surface-tension driven flows in a variety of methods (Czochralski, EFG, floating-zone, detached Bridgman growth). The sessile drop technique allows the measurement of both parameters simultaneously and has been used to measure the contact angles and the surface tension of Ge(1-x)Si(x) (0 less than or equal to x less than or equal to 1.3) alloys on various substrate materials. Fused quartz, Sapphire, glassy carbon, graphite, SiC, carbon-based aerogel, pyrolytic boron nitride (pBN), AIN, Si3N4, and polycrystalline CVD diamond were used as substrate materials. In addition, the effect of different cleaning procedures and surface treatments on the wetting behavior were investigated. Measurements were performed both under dynamic vacuum and gas atmospheres (argon or forming gas), with temperatures up to 1100 C. In some experiments, the sample was processed for longer times, up to a week, to investigate any changes of the contact angle and/or surface tension due to slow reactions with the substrate. For pure Ge, stable contact angles were found for carbon-based substrates and for pBN, for Ge(1-x)Si(x) only for pBN. The highest wetting angles were found for pBN substrates with angles around 170deg. For the surface tension of Ge, the most reliable values resulted in gamma(T) = (591- 0.077 (T-T(sub m)) 10(exp -3)N/m. The temperature dependence of the surface tension showed similar values for Ge(1-x)Si(x), around -0.08 x 10(exp -3)N/m K, and a compositional dependence of 2.2 x 10(exp -3)N/m at%Si.

Croell, A.↗

NASA NTRS2004

Heat pipe systems using new working fluids

The performance of a heat pipe system is greatly improved by the use of a dilute aqueous solution of about 0.0005 and about 0.005 moles per liter of a long chain alcohol as the working fluid. The surface tension-temperature gradient of the long-chain alcohol solutions turns positive as the temperature exceeds a certain value, for example about 40.degree. C. for n-heptanol solutions. Consequently, the Marangoni effect does not impede, but rather aids in bubble departure from the heating surface. Thus, the bubble size at departure is substantially reduced at higher frequencies and, therefore, increases the boiling limit of heat pipes. This feature is useful in microgravity conditions. In addition to microgravity applications, the heat pipe system may be used for commercial, residential and vehicular air conditioning systems, micro heat pipes for electronic devices, refrigeration and heat exchangers, and chemistry and cryogenics.

Chao, David F.↗

NASA NTRS1974

Liquid phase sintered compacts in space

A model that will explain the effect of gravity on liquid phase sintering was developed. Wetting characteristics and density segregation which are the two important phenomena in liquid phase sintering are considered in the model development. Experiments were conducted on some selected material combinations to study the gravity effects on liquid phase sintering, and to verify the validity of the model. It is concluded that: (1) The surface tension forces acting on solid particles in a one-g environment are not appreciably different from those anticipated in a 0.00001g/g sub 0 (or lower) environment. (2) The capillary forces are dependent on the contact angle, the quantity of the liquid phase, and the distance between solid particles. (3) The pores (i.e., bubbles) do not appear to be driven to the surface by gravity-produced buoyancy forces. (4) The length of time to produce the same degree of settling in a low-gravity environment will be increased significantly. (5) A low gravity environment would appear to offer a unique means of satisfactorily infiltrating a larger and/or complex shaped compact.

Mookherji, T. K.↗

NASA NTRS1988

Growth of GaAs crystals from the melt in a partially confined configuration

The experimental approach was directed along two main goals: (1) the implementation of an approach to melt growth in a partially confined configuration; and (2) the investigation of point defect interaction and electronic characteristics as related to thermal treatment following solidification and stoichiometry. Significant progress was made along both fronts. Crystal growth of GaAs in triangular ampuls was already carried out successfully and consistent with the model. In fact, pronounced surface tension phenomena which cannot be observed in ordinary confinement system were identified and should premit the assessment of Maragoni effects prior to space processing. Regarding thermal treatment, it was discovered that the rate of cooling from elevated temperatures is primarily responsible for a whole class of defect interactions affecting the electronic characteristics of GaAs and that stoichiometry plays a critical role in the quality of GaAs.

Gatos, Harry C.↗

NASA NTRS1990

Surface-crack growth: Models, experiments, and structures; Proceedings of the Symposium, Sparks, NV, Apr. 25, 1988

The present volume on surface-crack growth modeling, experimental methods, and structures, discusses elastoplastic behavior, the fracture analysis of three-dimensional bodies with surface cracks, optical measurements of free-surface effects on natural surfaces and through cracks, an optical and finite-element investigation of a plastically deformed surface flaw under tension, fracture behavior prediction for rapidly loaded surface-cracked specimens, and surface cracks in thick laminated fiber composite plates. Also discussed are a novel study procedure for crack initiation and growth in thermal fatigue testing, the growth of surface cracks under fatigue and monotonically increasing load, the subcritical growth of a surface flaw, surface crack propagation in notched and unnotched rods, and theoretical and experimental analyses of surface cracks in weldments.

Reuter, Walter G.↗

NASA NTRS1992

An interface tracking method applied to morphological evolution during phase change

The focus of this work is the numerical simulation of interface motion during solidification of pure materials. First, the applicability of the oft-used quasi-stationary approximation for interface motion is assessed. It is seen that such an approximation results in poor accuracy for nontrivial Stefan numbers. Solution of the full set of equations including grid movement terms yields close agreement with analytical results. Next, a generic interface tracking procedure is designed, which overcomes restrictions of single-valuedness of the interface imposed by commonly used mapping methods. This method incorporates with ease interface phenomena involving curvature, which assume importance at the smaller scales of a deformed interface. The method is then applied to study the development of a morphologically unstable phase interface. The issue of appropriate scaling has been addressed. The Gibbs-Thomson effect for curved interfaces has been included. The evolution of the interface, with the competing mechanisms of undercooling and surface tension is found to culminate in tip-splitting, cusp formation and persistent cellular development.

Shyy, W.↗

NASA NTRS1986

Convective effects in float-zone and Czochralski melts

The hydrodynamics of crystal-growth melts is a relatively new research area. Numerical modeling of these processes is necessary. The work discussed herein is in two parts: numerical simulations of the flow in a Czochralski melt, and also of that in a float zone. In addition, for the float-zone case, energy stability theory will be used to determine stability bounds for the onset of oscillatory thermo-capillary flow. Convective effects in crystal-growth melts arise from a variety of mechanisms. Temperature gradients both in the direction of gravity and normal to it give rise to convection due to buoyancy effects. Rotation of the crucible and/or crystal causes a forced convection which may augment or oppose the buoyancy-driven flow. Finally, thermo-capillary forces (due to the variation of surface tension with temperature) drive surface motions which in turn generate convection in the bulk fluid. All of these mechanisms are present in either Czochralski or float-zone growth. The objective of the Czochralski modeling is to develop an accurate numerical simulation of the flow in a Czochralski silicon melt and to investigate the effects of various parameters on the flow properties. Like some earlier investigations, the intent is to simulate the effects of buoyancy, forced and thermo-capillary convection, including unsteady effects. Unlike earlier work, the aim is to include the effects of a variable free surface and freezing interface and, possibly incorporate nonaxisymmetric effects.

Neitzel, G. P.↗

NASA NTRS1971

Radial rib antenna surface deviation analysis program

A digital computer program was developed which analyzes any radial rib antenna with ribs radiating from a central hub. The program has the capability for calculating the antenna surface contour (reversed pillowing effect), the optimum rib shape for minimizing the rms surface error, and the actual rms surface error. Rib deflection due to mesh tension and catenary cable tension can also be compensated for, and the pattern from which the mesh gores are cut can be determined.

Coyner, J. V., Jr.↗