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At least 253 records · Page 14

Low cost Get-Away-Special (GAS) furnace

A simple and inexpensive Space Shuttle experimental apparatus to conduct microgravity melting and solidification is presented. A GAS space furnace was initially developed as a student design project at the USAF Academy and further refined at NASA Lewis. The experiment package consists of a melting chamber, battery power system, temperature data recording systems, and electronic controller. The melting chamber is a thin-walled tube wrapped by heating resistance wire. Thermocouples are used to record the specimen thermal history. Power is supplied by 2-V batteries wired to produce 360 W. The mV output of the thermocouples is amplified, cold-junction compensated, and converted to a frequency which is then recorded on an off-the-shelf cassette tape recorder. A backup data recording system which digitizes the amplified signal and records the data on EEPROMs has also been included. This experimental device demonstrates that basic science research can be kept simple and inexpensive.

Turner, Glon D.↗

Acoustical Measurement Of Furnace Temperatures

Simple probes withstand severe conditions, yet give spatially-resolved temperature readings. Prototype acoustical system developed to measure temperatures from ambient to 1,800 degree F in such structures as large industrial lime kilns and recovery-boiler furnaces. Pulses of sound reflected from obstructions in sensing tube. Speed of sound and temperature in each segment deduced from travel times of pulses.

Parthasarathy, Shakkottai↗

Modified Furnace Makes More Silicon Ribbon

Simple change in lid and heat shields makes faster growth rates possible. In modified furnace, slots in shields making up lid grow progressively wider from bottom to top of lid. Allows ribbon to cool faster by radiation. Result, crucible maintains at higher temperature, 5.8-cm-wide ribbon thicker, and ribbon is pulled faster. Used in pilot production line to demonstrate dendritic-web technology.

Piotrowski, Paul A.↗

Experimental observation of the influence of furnace temperature profile on convection and segregation in the vertical Bridgman crystal growth technique

Azulene-doped naphtalene was directionally solidified using the vertical Bridgman-Stockbarger technique. Doping homogeneity and convection are determined as a function of the temperature profile in the furnace and the freezing rate. Convective velocities are two orders of magnitude lower when the temperature increases with height. The cross sectional variation in azulene concentration tends to be asymmetric. Neither rotation of the ampoule nor deliberate introduction of thermal asymmetries during solidification had a significant influence on cross sectional variations in doping. It is predicted that slow directional solidification under microgravity conditions can produce greater inhomogeneities than on earth. Thus when low freezing rates are necessary in order to avoid constitutional supercooling, it may be necessary to combine microgravity and magnetic fields in order to achieve homogeneous crystals.

Neugebauer, G. T.↗

Crystal Growth Furnace - An overview of the system configuration and planned experiments on the first United States Microgravity Laboratory mission

Attention is given to the Crystal Growth Furnace (CGF) currently in the Level IV integration cycle at the Kennedy Space Center in preparation for its maiden flight on the first United States Microgravity Laboratory (USML-1) mission to be launched in May 1992. CGF was developed for NASA under the Microgravity Science and Application division programs at NASA Headquarters. An overview of the CGF system and the system configuration for the USML-1 mission are presented, and the planned on-orbit experiments are described. The four important scientific experiments selected from industry and educational institutions for the CGF USML-1 mission will enable a better understanding of the complex phenomena inherent in materials processing that will lead to the ultimate improvement of both processes and materials. Crystal growth by chemical vapor transport has resulted in improved growth conditions with crystal morphology, lower defect densities, and higher growth rates than terrestrially observed.

Srinivas, R.↗

Crystal Growth Furnace - An overview of the system configuration and planned experiments on the First United States Microgravity Laboratory mission

The Crystal Growth Furnace (CGF) system configuration for the First United States Microgravity Laboratory (USML-1) mission is reviewed, and the planned on-orbit experiments are briefly described. The CGF is configured to accommodate four scientific experiments involving crystal growth which are based on the classical Bridgman method and CVT method, including vapor transport crystal growth of mercury cadmium telluride; crystal growth of mercury zinc telluride by directional solidification; seeded Bridgman growth of zinc-doped cadmium telluride; and Bridgman growth of selenium-doped gallium arsenide.

Srinivas, R.↗

Moving-Temperature-Gradient Heat-Pipe Furnace Element

In improved apparatus, ampoule of material directionally solidified mounted in central hole of annular heat pipe, at suitable axial position between heated and cooled ends. Heated end held in fixed position in single-element furnace; other end left in ambient air or else actively cooled. Gradient of temperature made to move along heat pipe by changing pressure of noncondensable gas. In comparison with prior crystal-growing apparatuses, this one simpler, smaller, and more efficient.

Gillies, Donald C.↗

Experimental observation of the influence of furnace temperature profile on convection and segregation in the vertical Bridgman crystal growth technique

Azulene-doped naphthalene was directionally solidified during the vertical Bridgman-Stockbarger technique. Doping homogeneity and convection were determined as a function of the temperature profile in the furnace and the freezing rate. Convection velocities were two orders of magnitude lower when the temperature increased with height. Rarely was the convection pattern axisymmetric, even though the temperature varied less than 0.1 K around the circumference of the growth ampoule. Correspondingly the cross sectional variation in azulene concentration tended to be asymmetric, especially when the temperature increased with height. This cross sectional variation changed dramatically along the ingot, reflecting changes in convection presumably due to the decreasing height of the melt. Although there was large scatter and irreproducibility in the cross sectional variation in doping, this variation tended to be least when the growth rate was low and the convection was vigorous. It is expected that compositional variations would also be small at high growth rates with weak convection and flat interfaces, although this was not investigated in the present experiments. Neither rotation of the ampoule nor deliberate introduction of thermal asymmetries during solidification had a significant influence on cross sectional variations in doping. It is predicted that slow directional solidification under microgravity conditions could produce greater inhomogeneities than on Earth. Combined use of microgravity and magnetic fields would be required to achieve homogeneity when it is necessary to freeze slowly in order to avoid constitutional supercooling.

Neugebauer, G. T.↗

Optical/thermal analysis methodology for a space-qualifiable RTP furnace

A methodology to predict the coupled optical/thermal performance of a reflective cavity heating system was developed and a laboratory test to verify the method was carried out. The procedure was utilized to design a rapid thermal processing (RTP) furnace for the Robot-Operated Material Processing in Space (ROMPS) Program which is a planned STS HH-G canister experiment involving robotics and material processing in microgravity. The laboratory test employed a tungsten-halogen reflector/lamp to heat thin, p-type silicon wafers. Measurements instrumentation consisted of 5-mil Pt/Pt-Rh thermocouples and an optical pyrometer. The predicted results, utilizing an optical ray-tracing program and a lumped-capacitance thermal analyzer, showed good agreement with the measured data for temperatures exceeding 1300 C.

Bugby, D.↗

Space Station Furnace Facility. Volume 2: Appendix 1: Contract End Item specification (CEI), part 1

This specification establishes the performance, design, development, and verification requirements for the Space Station Furnace Facility (SSFF) Core. The definition of the SSFF Core and its interfaces, specifies requirements for the SSFF Core performance, specifies requirements for the SSFF Core design, and construction are presented, and the verification requirements are established.

Seabrook, Craig↗

Space Station Furnace Facility. Volume 2: Requirements Definition and Conceptual Design Study. Appendix 3: Environment Analysis

A Preliminary Safety Analysis (PSA) is being accomplished as part of the Space Station Furnace Facility (SSFF) contract. This analysis is intended to support SSFF activities by analyzing concepts and designs as they mature to develop essential safety requirements for inclusion in the appropriate specifications, and designs, as early as possible. In addition, the analysis identifies significant safety concerns that may warrant specific trade studies or design definition, etc. The analysis activity to date concentrated on hazard and hazard cause identification and requirements development with the goal of developing a baseline set of detailed requirements to support trade study, specifications development, and preliminary design activities. The analysis activity will continue as the design and concepts mature. Section 2 defines what was analyzed, but it is likely that the SSFF definitions will undergo further changes. The safety analysis activity will reflect these changes as they occur. The analysis provides the foundation for later safety activities. The hazards identified will in most cases have Preliminary Design Review (PDR) applicability. The requirements and recommendations developed for each hazard will be tracked to ensure proper and early resolution of safety concerns.

Source record↗

Space Station Furnace Facility. Volume 3: Program cost estimate

The approach used to estimate costs for the Space Station Furnace Facility (SSFF) is based on a computer program developed internally at Teledyne Brown Engineering (TBE). The program produces time-phased estimates of cost elements for each hardware component, based on experience with similar components. Engineering estimates of the degree of similarity or difference between the current project and the historical data is then used to adjust the computer-produced cost estimate and to fit it to the current project Work Breakdown Structure (WBS). The SSFF Concept as presented at the Requirements Definition Review (RDR) was used as the base configuration for the cost estimate. This program incorporates data on costs of previous projects and the allocation of those costs to the components of one of three, time-phased, generic WBS's. Input consists of a list of similar components for which cost data exist, number of interfaces with their type and complexity, identification of the extent to which previous designs are applicable, and programmatic data concerning schedules and miscellaneous data (travel, off-site assignments). Output is program cost in labor hours and material dollars, for each component, broken down by generic WBS task and program schedule phase.

Source record↗

System performance and on-orbit operations of the Crystal Growth Furnace (CGF) on the first United States microgravity laboratory mission

The paper discusses the design, the performance, and on-orbit operations of the Crystal Growth Furnace (CGF) system flown for the first time aboard the Orbiter Columbia on STS-50. Four experiments were carried out: (1) crystal growth of (Hg,Zn)Te by chemical vapor transport, (2) seeded Bridgman growth of Zn-doped CdTe, (3) Bridgman growth of Se-doped GaAs, and (4) crystal growth of (Hg,Zn)Te by directional solidification. The results of a system performance data analysis demonstrate that all the elements of the CGF system functioned flawlessly. Seven out of eight samples carried on board yielded the best possible science return to date, surpassing previous microgravity material processing experiments in space.

Srinivas, R.↗

Data acquisition from a crystal growth furnace

Digital acquisition from a furnace for growing the lead tin telluride crystal based on Asyst software is described. It is shown that the use of Asyst for the acquisition of experimental data makes it possible to handle large amounts of data and to drastically reduce the time required for displaying the data from several hours to less than 5 minutes.

Woodell, Glenn A.↗

High Temperature Calibration Furnace System user's guide

The High Temperature Calibration Furnace System (HTCFS) was developed by Summitec Corporation. It is a high precision instrument providing a constant temperature which can be used to calibrate high temperature thermocouples. Incorporating the many recent technological advances from the fields of optical fiber thermometry, material science, computer systems interfacing, and process control, the engineers at Summitec Corporation have been able to create a system that can reach a steady operating temperature of 1700 C. The precision for the system requires the measurement of temperature to be within 1 C in two hours and within 2 C in 24 hours. As documented, the experimental result shows that this system has been able to stay within .5 C in 5 hours. No other systems commercially available have been able to achieve such high temperature precision. This manual provides an overview of the system design, instructions for instrument setup, and operation procedures. Also included are a vendor list and the source codes for the custom-designed software.

Source record↗

A new containerless image furnace with electro-static positioning device

A new containerless image furnace with a microwave discharge plasma lamp and electrostatic positioning device was developed for the use of the microgravity experiment on the Japanese experimental module (JEM). The electrostatic positioning system was tested under the reduced gravity environment in the MU-300 aircraft. Solid specimens (maximum weight is 1.3 gr and 10 mm in diameter) and water drops (maximum weight is 0.11 gr and 6 mm in diameter) were successfully controlled under the 0.02G environment. Rotation control of the dielectric specimen was also possible by means of supplying a rotating electric field while the specimen is levitating. The measured rotation speed of the glass shell specimen (0.08 gr, 10 mm) was up to 110 rpm, when the rotating field frequency was 6Hz.

Yamawaki, Toshihiko↗

Redesigned Electron-Beam Furnace Boosts Productivity

Redesigned electron-beam furnace features carousel of greater capacity so more experiments conducted per loading, and time spent on reloading and vacuum pump-down reduced. Common mounting plate for electron source and carousel simplifies installation and reduces vibration.

Williams, Gary A.↗