Tensile failure of fiber composites.
Composite tensile-failure modes, discussing failure load prediction, experimental data and statistical analysis of stress concentration effects
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Composite tensile-failure modes, discussing failure load prediction, experimental data and statistical analysis of stress concentration effects
Residual stresses arising from fabrication processes in laminates
Structural application of advanced composite filamentary materials requires lamination of the basic orthotropic plies into angle-ply laminates. The resulting elastic and strength properties depend on the pattern of orientation and are influenced by inevitable errors and inaccuracy in placement of the angle plies. Reviewed is the effect on elastic properties of orientation dispersion. The conventional constitutive relations are recast in a homologous form to account for orientation dispersion by addition of a single parameter. Graphical results are presented to show the behavior of the most important advanced composite materials. The results are directly useful for estimating effects of manufacturing inaccuracy and for design of partially oriented reinforced structures.
The application of polyimide resin as a matrix for glass filament-wound thin metal-lined pressure vessels was studied over a temperature range of (minus) 320 to 600 F. Keramid 601 polyimide was found to perform quite well over the entire range of temperature. Hoop stress values of 425 ksi were determined at 75 F which is equivalent to epoxy resin in similar structures. At -320 and 600 F, 125 and 80% of this strength was retained. Thermal ageing at 500 F for up to 50 hours was studied with severe reduction in strength, but there is evidence that this reduction could be improved. Another polyimide resin studied was P10PA which was found to have processing characteristics inappropriate for filament-winding. NOL ring tensile and shear data was determined from both resins with S-glass. Pressure vessel design, fabrication and test procedures are described in detail.
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An experimental investigation was conducted to determine the magnitude of lamination residual stresses in angle-ply composites and to evaluate their effects on composite structural integrity. The materials investigated were boron/epoxy, boron/polyimide, graphite/low modulus epoxy, graphite/high modulus epoxy, graphite/polyimide and s-glass/epoxy. These materials were fully characterized. Static properties of laminates were also determined. Experimental techniques using embedded strain gages were developed and used to measure residual strains during curing. The extent of relaxation of lamination residual stresses was investigated. It was concluded that the degree of such relaxation is low. The behavior of angle-ply laminates subjected to thermal cycling, tensile load cycling, and combined thermal cycling with tensile load was investigated. In most cases these cycling programs did not have any measurable influence on residual strength and stiffness of the laminates. In the tensile load cycling tests, the graphite/polyimide shows the highest endurance with 10 million cycle runouts at loads up to 90 percent of the static strength.
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A combined theoretical and experimental investigation was conducted to assess the suitability of the 10 deg off-axis tensile test specimen for the intralaminar shear characterization of unidirectional composites. Composite mechanics, a combined-stress failure criterion, and a finite element analysis were used to determine theoretically the stress-strain variation across the specimen width and the relative stress and strain magnitudes at the 10 deg plane. Strain gages were used to measure the strain variation across the specimen width at specimen midlength and near the end tabs. Specimens from Mod-I/epoxy, T-300/epoxy, and S-glass/epoxy were used in the experimental program. It was found that the 10 deg off-axis tensile test specimen is suitable for intralaminar shear characterization and it is recommended that it should be considered as a possible standard test specimen for such a characterization.
Graphite-epoxy laminates were thermally cycled to determine the effects of thermal cycles on tensile properties and thermal expansion coefficients of the laminates. Three 12-ply laminate configurations were subjected to up to 5,000 thermal cycles. The cumulative effect of the thermal cycles was determined by destructive inspection (electron micrographs and tensile tests) of samples after progressively larger numbers of cycles. After thermal cycling, the materials' tensile strengths, moduli, and thermal expansion coefficients were significantly lower than for the materials as fabricated. Most of the degradation of properties occurred after only a few cycles. The property degradation was attributed primarily to the progressive development of matrix cracks whose locations depended upon the layup orientation of the laminate.
The improved foreign object damage resistance of a metal matrix advanced composite fan blade was demonstrated. The fabrication, whirl impact test and subsequent evaluation of nine advanced composite fan blades of the "QCSEE" type design were performed. The blades were designed to operate at a tip speed of 282 m/sec. The blade design was the spar/shell type, consisting of a titanium spar and boron/aluminum composite airfoils. The blade retention was designed to rock on impact with large birds, thereby reducing the blade bending stresses. The program demonstrated the ability of the blades to sustain impacts with up to 681 g slices of birds at 0.38 rad with little damage (only 1.4 percent max weight loss) and 788 g slices of birds at 0.56 rad with only 3.2 percent max weight loss. Unbonding did not exceed 1.1 percent of the post-test blade area during any of the tests. All blades in the post-test condition were judged capable of operation in accordance with the FAA guidelines for medium and large bird impacts.
Resin matrix composites having improved resistance to foreign object damage in gas turbine engine fan blade applications were developed. Materials evaluated include epoxy matrix graphite/glass and boron/glass hybrids, thermoplastic matrix boron/glass hybrids, and superhybrids consisting of graphite/epoxy, boron/aluminum, and titanium alloy sheets. Static, pendulum impact, and ballistic impact test results are reported for all materials. Superhybrid blade like specimens are shown to be capable of withstanding relatively severe ballistic impacts from gelatin spheres without fracture. The effects of ply configuration and projectile angle of incidence on impact behavior are described. Predictions of surface strains during ballistic impact are presented and shown to be in reasonable agreement with experimental measurements.
Some effects of post-cure time and temperature on the physicomechanical properties of a phenolic-asbestos and a phenolic-glass composite are studied. The molding and post-curing procedures are discussed along with physical and mechanical test results. It is found that the specific gravity of the panels tested decreased slightly but the hardness always increased with post cure, and that the mechanical properties had different patterns of response to increasing post-cure time and temperature. For tensile properties, strength decreased, modulus increased, and elongation at break exhibited little change. In general, the phenolic-asbestos showed more positive response to post cure than did the phenolic-glass. Mold venting is found to impart better properties to the composites concerned.
The analytical/experimental correlation study was performed to develop an understanding of the behavior of notched Boron/epoxy laminates subjected to tension/tension fatigue loading. It is postulated that the fatigue induced property changes (stiffness as well as strength) of the laminate can be obtained from the lamina fatigue properties. To that end, the Boron/epoxy lamina static and fatigue data (lifetime, residual stiffness and strength) were obtained initially. The longitudinal and transverse tension data were determined from the (0) and (90) laminate tests while the in-plane shear data were obtained from the (+ or - 45) sub s laminates. The static tests obtained the notched strength and mode of failure while the fatigue tests determined lifetime, damage propagation and residual strength. The failure in static tension occurred in a transverse crack propagation mode.
The results of a 20-month program, designed to investigate parameters which effect the foreign object damage resulting from ingestion of birds into fan blades are described. Work performed on this program included the design, fabrication, and impact testing of QCSEE fan blades to demonstrate improvement in resistance relative to existing blades and also the design and demonstration of a pin root attachment concept.
The results of an experimental study of damage extension and failure in glass and graphite/epoxy laminates containing partially through-thickness surface cracks are presented. The laminates studied are divided between those containing four plies, 90/0/0/90, 15/-15/-15/15, and 45/-45/-45/45, and those containing 12-16 plies of the general configurations 0/90, + or - 45, and 0/+ or - 60. Most of the results are for surface cracks of various lengths and several depths. Stable damage extension in laminates containing surface cracks is predominantly delamination between plies, and tends to be much more extensive prior to failure than is the case with through-thickness cracks, resulting in approximately notch-insensitive behavior in most cases. A greater tendency for notch-sensitive behavior is found for 0/90 graphite/epoxy laminates for which stable damage extension is more limited. The rate of damage extension with increasing applied stress depends upon the composite system and ply configuration as well as the crack length and depth. An approximate semiempirical method is presented for estimating the growth rate of large damage-regions.
A combined theoretical and experimental investigation was conducted to assess the suitability of the 10 deg off-axis tensile test specimen for the intralaminar shear characterization of unidirectional composites. Composite mechanics, a combined-stress failure criterion, and a finite variation across the specimen width and the relative stress and strain magnitudes at the 10 deg plane. Strain gages were used to measure the strain variation across the specimen width at specimen midlength and near the end tabs. Specimens from Mod-I/epoxy, T-300/epoxy, and S-glass/epoxy were used in the experimental program. It was found that the 10 deg off-axis tensile test specimen is suitable for intralaminar shear characterization, and it is recommended that it should be considered as a possible standard test specimen for such a characterization.
A combined theoretical and experimental investigation was conducted to assess the suitability of the 10-deg off-axis tensile test specimen for the intralaminar shear characterization of unidirectional composites. Composite mechanics, a combined-stress failure criterion, and a finite-element analysis were used to determine theoretically the stress-strain variation across the specimen width and the relative stress and strain magnitudes at the 10-deg plane. Strain gages were employed to measure the strain variation across the specimen width at specimen midlength and near the end tabs. Specimens from Mod-I/epoxy, T-300/epoxy, and S-glass/epoxy were used in the experimental program. It was found that the 10-deg off-axis tensile test specimen is suitable for intralaminar shear characterization, and it is recommended that it should be considered as a possible standard test specimen for such a characterization.