Spontaneous Phase Balancing in Delta-Connected Single-Phase Droop-Controlled Inverters
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Engineering↗
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Grain boundary widening controls siderite (FeCO3) replacement of limestone (CaCO3)
Abstract The microstructure of minerals and rocks can significantly alter reaction rates. This study focuses on identifying transport paths in low porosity rocks based on the hypothesis that grain boundary widening accelerates reactions in which one mineral is replaced by another (replacement reaction). We conducted a time series of replacement experiments of three limestones (CaCO 3 ) of different microstructures and solid impurity contents using FeCl 2 . Reacted solids were analyzed using chemical imaging, small angle X-ray and neutron scattering and Raman spectroscopy. In high porosity limestones replacement is reaction controlled and complete replacement was observed within 2 days. In low porosity limestones that contain 1–2% dolomite impurities and are dominated by grain boundaries, a reaction rim was observed whose width did not change with reaction time. Siderite (FeCO 3 ) nucleation was observed in all parts of the rock cores indicating the percolation of the solution throughout the complete core. Dolomite impurities were identified to act as nucleation sites leading to growth of crystals that exert force on the CaCO 3 grains. Widening of grain boundaries beyond what is expected based on dissolution and thermal grain expansion was observed in the low porosity marble containing dolomite impurities. This leads to a self-perpetuating cycle of grain boundary widening and reaction acceleration instead of reaction front propagation.
37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
A Step Towards Machine Learning-based Coherent Generator Grouping for Emergency Control Applications in Modern Power Grid
A dynamic neural network (NN) based multi-class classifier is proposed for improving online prediction of coherent generator groups (CGGs), following the occurrences of various contingencies in the power grid. This is motivated by the increasing availability of the measurements from phasor measurement units (PMUs) and the number of grouping schemes is limited. The proposed method consists of three steps. First, by performing offline simulations, a library of system dynamic responses characterized by post-contingency rotor angles and speeds of individual generators is obtained. To generate sufficient data, up to N-2 contingencies and the uncertain parameters associated with the power grid including type and location of disturbance and fault clearing times are modeled. Secondly, the training data-set is produced by generating labels for individual contingencies using a hierarchical clustering method based on rotor angle and speed data. Lastly, the dynamic NN models are trained for online applications such as emergency controls and controlled islanding. The proposed method is tested on the standard 16-generator 68-bus system to demonstrate its performance. Furthermore, the impact of the sample data lengths on the CGG numbers is evaluated. It is interesting to observe that the time domain stability behaviors can be determined by examining the changes in the CGG numbers.
29 ENERGY PLANNING, POLICY, AND ECONOMY↗
Rotated-Droop Control for Enhanced Stability and Power Decoupling in Microgrids With Complex Line Impedances
Classical droop control in microgrids predominantly assumes inductive line impedance, which simplifies implementation but causes power coupling and steady-state errors in systems with resistive and inductive lines. This paper proposes a rotated-droop control strategy for grid-forming inverters that reformulates the power equations by incorporating the magnitude and angle of the line impedance within a rotated reference frame. This method enhances the decoupling of active and reactive power dynamics without increasing complexity or requiring communication links. A small-signal state-space model was created to capture the dynamic behavior of the system under varying impedance parameters, preserving the original droop gains by rotating the power control structure. This allows eigenvalue-based stability analysis and enhances damping and transient performance. Simulation and experimental results validated the improved power-sharing performance, faster response, and robustness of the proposed method under different impedance conditions. This approach maintains the decentralized structure of the conventional droop control while enabling greater adaptability and scalability, making it suitable for modern inverter-based microgrids with dynamic topologies.
Campo-Ossa, Daniel Dario [Univ. of Puerto Rico, Ag↗
Revealing transient powder-gas interaction in laser powder bed fusion process through multi-physics modeling and high-speed synchrotron x-ray imaging
Laser powder bed fusion (LPBF) is an emerging metal additive manufacturing process. The gas-driven powder motions in laser powder bed fusion have significant influence on the build quality. However, the transient powder-gas interaction has not been well understood due to the challenges in quantitative experiment measurements. In this work, the powder-gas interaction for a single pulse laser illuminating on the powder bed is studied. We establish a multi-physics model to simulate the complex liquid/gas flow as well as the gas-driven powder motions, which is substantiated by high-speed synchrotron x-ray imaging. We identify and quantify four characteristic modes of powder-gas interaction in LPBF. The motion of a powder is controlled by one or multiple interaction modes collectively. As revealed by simulations and confirmed by experiments, powders can merge into the molten pool from its rim, be ejected at different divergence angles (powder spattering), or dive into the molten pool to cause significant molten pool fluctuation. Overall, our results provide insights toward the driving forces controlling the dynamic powder behavior, which pave the way for reducing structure defects during the build process.
36 MATERIALS SCIENCE↗
Dynamic motion trajectory control with nanoradian accuracy for multi-element X-ray optical systems via laser interferometry
The past decades have witnessed the development of new X-ray beam sources with brightness growing at a rate surpassing Moore’s law. Current and upcoming diffraction limited and fully coherent X-ray beam sources, including multi-bend achromat based synchrotron sources and high repetition rate X-ray free electron lasers, puts increasingly stringent requirements on stability and accuracy of X-ray optics systems. Parasitic motion errors at sub-micro radian scale in beam transport and beam conditioning optics can lead to significant loss of coherence and brightness delivered from source to experiment. To address this challenge, we incorporated optical metrology based on interferometric length and angle sensing and real-time correction as part of the X-ray optics motion control system. A prototype X-ray optics system was constructed following the optical layout of a tunable X-ray cavity. On-line interferometric metrology enabled dynamical feedback to a motion control system to track and compensate for motion errors. The system achieved sub-microradian scale performance, as multiple optical elements are synchronously and continuously adjusted. This first proof of principle measurement demonstrated both the potential and necessity of incorporating optical metrology as part of the motion control architecture for large scale X-ray optical systems such as monochromators, delay lines, and in particular, X-ray cavity systems to enable the next generation cavity-based X-ray free electron lasers.
47 OTHER INSTRUMENTATION↗
Dative Epitaxy of Commensurate Monocrystalline Covalent van der Waals Moiré Supercrystal
Realizing van der Waals (vdW) epitaxy in the 1980s represents a breakthrough that circumvents the stringent lattice matching and processing compatibility requirements in conventional covalent heteroepitaxy. However, due to the weak vdW interactions, there is little control over film qualities by the substrate. Typically, discrete domains with a spread of misorientation angles are formed, limiting the applicability of vdW epitaxy. In this study, the epitaxial growth of monocrystalline, covalent Cr 5 Te 8 2D crystals on monolayer vdW WSe 2 by chemical vapor deposition is reported, driven by interfacial dative bond formation. The lattice of Cr 5 Te 8 , with a lateral dimension of a few tens of micrometers, is fully commensurate with that of WSe 2 via 3 × 3 (Cr 5 Te 8 )/7 × 7 (WSe 2 ) supercell matching, forming a single-crystalline moiré superlattice. This work establishes a conceptually distinct paradigm of thin-film epitaxy, termed “dative epitaxy”, which takes full advantage of covalent epitaxy with chemical bonding for fixing the atomic registry and crystal orientation, while circumventing its stringent lattice matching and processing compatibility requirements; conversely, it ensures the full flexibility of vdW epitaxy, while avoiding its poor orientation control. Cr 5 Te 8 2D crystals grown by dative epitaxy exhibit square magnetic hysteresis, suggesting minimized interfacial defects that can serve as pinning sites.
36 MATERIALS SCIENCE↗
Edge-localized mode mitigation enabled by active control of pedestal density gradient with new EAST tokamak divertor
Mitigation of large edge-localized modes (ELMs) has been achieved by actively reducing the pedestal density gradient with the EAST new right-angled lower divertor through changing the strike point position from the vertical target to the horizontal target. A series of dedicated experiments in the 2021–2024 EAST campaigns demonstrate that this ELM control solution is highly reproducible in a broad parameter space of edge safety factor q 95 = 4.7–7.1, heating power P total = 2.3–5 MW, and pedestal collisionality $ν_{e,ped}^{*}$ = 1–6, under both favorable and unfavorable magnetic configurations. Higher plasma density could facilitate the achievement of this ELM control solution. Statistical results indicate that the ELM mitigation effect can be observed at relatively larger Greenwald density fraction of f GW > 0.47. In addition, this ELM mitigation effect can be achieved with both lithium-coated and boronized metal walls. The pedestal density gradient is systematically lower in the horizontal target case than that of the vertical target case when the ELM mitigation effect can be observed. SOLPS-ITER simulation results indicate that the pedestal fueling from divertor recycling is significantly lower in the horizontal target case. This could contribute to the formation of a flattened pedestal density profile with small ELMs.
70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
Lifetime fatigue response due to wake steering on a pair of utility-scale wind turbines
Quantifying the impacts on turbine loads during wind farm control is an important consideration in assessing power production benefits. Wake steering controls aim to improve total wind farm performance by coordinating the control actions of individual turbines, wherein an upstream turbine is intentionally yawed at an offset angle from the measured wind direction. Consequently, this redirects its wake for improved power production and potentially reduces fatigue loads of the downstream turbines. This paper studies the lifetime fatigue loads associated with wake steering by using utility-scale wind turbine experimental data to conduct an analysis on a pair of wind turbines. This study was part of a large field experiment in which a group of five GE 1.5-MW SLE CWE turbines were selected as targets for conducting wake steering research. A standard loads instrumentation package and data acquisition system were installed on two turbines within the cluster to measure turbine fundamental loads. The time-series databases were used to calculate loads statistics as well as short-term and lifetime damage equivalent loads. Fatigue calculations followed the guidance in Annex H of the International Electrotechnical Commission standard 61400-1, Edition 4. Lifetime fatigue calculation results are presented in this analysis; three methods of assessing lifetime fatigue were used to determine percent difference for blade root moments, main shaft moments, main shaft torque, and tower top torque. For all three fatigue treatments, some components’ lifetime fatigue increases for the controlled turbine; however, the downwind turbine experienced a reduction in lifetime fatigue and combined effect for the turbine pair results in a reduction of fatigue when wake steering controls are applied.
17 WIND ENERGY↗
Control of Nonlinear Compton Scattering in a Squeezed Vacuum
Electromagnetic radiation by accelerated charges is a fundamental process in physics. Here, we introduce a quantum-optical framework for controlling the emission of radiation of an electron in an intense laser field via squeezed vacuum states. By engineering the quantum fluctuations of the emission modes, we demonstrate that the probability of nonlinear Compton scattering can be significantly enhanced or suppressed through tunable squeezing amplitude and angle. We show numerically that our predictions are experimentally accessible with current squeezing technologies, establishing a new paradigm for quantum control in high-intensity light-matter interactions.
Light-matter interaction↗
Controlled Organization of Inorganic Materials Using Biological Molecules for Activating Therapeutic Functionalities
Precise control over the assembly of biocompatible three-dimensional (3D) nanostructures would allow for programmed interactions within the cellular environment. Nucleic acids can be used as programmable crosslinkers to direct the assembly of quantum dots (QDs) and tuned to demonstrate different interparticle binding strategies. In this work, morphologies of self-assembled QDs are evaluated via gel electrophoresis, transmission electron microscopy, small-angle X-ray scattering, and dissipative particle dynamics simulations, with all results being in good agreement. The controlled assembly of 3D QD organizations is demonstrated in cells via the colocalized emission of multiple assembled QDs, and their immunorecognition is assessed via enzyme-linked immunosorbent assays. RNA interference inducers are also embedded into the interparticle binding strategy to be released in human cells only upon QD assembly, which is demonstrated by specific gene silencing. The programmability and intracellular activity of QD assemblies offer a strategy for nucleic acids to imbue the structure and therapeutic function into the formation of complex networks of nanostructures, while the photoluminescent properties of the material allow for optical tracking in cells in vitro.
36 MATERIALS SCIENCE↗
Temperature-Induced Tunable Assembly of Columnar Phases of Nanorods
Abstract not provided
Kim, Hyeong Jin↗
First large capsule implosions in a frustum-shaped hohlraum
Here, we report on the first indirect-drive implosions driven by a dual conical frustum-shaped hohlraum denoted “frustraum” and the experimental tuning campaigns leading up to two layered implosions. The campaign used 1.2 and 1.4 mm inner radius high density carbon (HDC) capsules and represented the largest HDC capsules to be imploded on the National Ignition Facility via indirect drive. Several techniques were successfully implemented to control the Legendre mode 2 capsule symmetry of the implosions, including changing the wall angle of the frustraum, which is not possible with cylindrical hohlraums. A mode 4 feature was observed and its implications for hotspot mix discussed. Two layered implosions were conducted with 1.2 mm inner radius capsules, the latter of which achieved the highest layered capsule absorbed energy on the National Ignition Facility using only 1.74 MJ of laser energy. The layered implosion results, along with generalized Lawson parameters, suggest that increasing the energy absorbed by the capsule at the expense of long coast times makes it more challenging to achieve ignition and that further reducing coast time (time between end of laser pulse and bang time) closer to the 1 ns level is warranted to improve the areal density and make it easier to achieve the hotspot temperature, alpha heating, and yield amplification required for ignition.
70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
Impact of wake steering on loads of downstream wind turbines at an above-rated condition
Wake steering strategies often seek to gain power at the expense of increased fatigue loads. Here, we investigate the feasibility of applying wake steering at an above-rated condition. In such a condition, the farm is operating at rated power, and thus, increased power output is not the goal. Instead, wake steering is considered in the context of load reduction. We perform a sweep of wind directions and yaw misalignment angles, ranging from negative to positive values. This approach allows us to obtain trends and identify asymmetries in turbine response for symmetric scenarios. We use a wind farm consisting of five aligned IEA Wind 15-MW reference wind turbines, and analyze trends related to the blade-root, low-speed shaft, and tower-base moments, both in terms of standard deviation and damage equivalent loads. We show that for any given fixed wind direction, the turbines can be yawed such that the fatigue loads are reduced. Reductions of up to 5% (depending on the component) in terms of standard deviation and damage equivalent loads can be achieved by negatively yawing the turbine. A negative yaw misalignment has shown to be the direction of larger improvements. Such results contrast those found for below-rated conditions, where a positive yaw misalignment is typically preferred. However, since load reduction is not uniform across all component loads, more study and consideration is required before operational recommendations can be made.
17 WIND ENERGY↗
Twistronics of Janus transition metal dichalcogenide bilayers
Twisted multilayers of two-dimensional (2D) materials are an increasingly important platform for investigating quantum phases of matter, and in particular, strongly correlated electrons. The moiré pattern introduced by the relative twist between layers creates effective potentials of long wavelength, leading to electron localization. However, in contrast to the abundance of 2D materials, few twisted heterostructures have been studied until now. Here, in this study, we develop a first-principles continuum theory to study the electronic bands introduced by moire patterns of twisted Janus transition metal dichalcogenide (TMD) homo- and heterobilayers. The model includes lattice relaxation, stacking-dependent effective mass, and Rashba spin-orbit coupling. We then perform a high-throughput generation and characterization of DFT-extracted continuum models for more than a hundred possible combinations of materials and stackings. Our model predicts that the moiré physics and emergent symmetries depend on chemical composition, vertical layer orientation, and twist angle, so that the miniband wave functions can form triangular, honeycomb, and kagome networks. Rashba spin-orbit effects, peculiar of these systems, can dominate the moiré bandwidth at small angles. Our work enables detailed investigation of Janus twisted heterostructures, allowing the discovery and control of novel electronic phenomena.
36 MATERIALS SCIENCE↗
Bridging length scales in hard materials with ultra-small angle X-ray scattering – a critical review
Owing to their exceptional properties, hard materials such as advanced ceramics, metals and composites have enormous economic and societal value, with applications across numerous industries. Understanding their microstructural characteristics is crucial for enhancing their performance, materials development and unleashing their potential for future innovative applications. However, their microstructures are unambiguously hierarchical and typically span several length scales, from sub-ångstrom to micrometres, posing demanding challenges for their characterization, especially for in situ characterization which is critical to understanding the kinetic processes controlling microstructure formation. This review provides a comprehensive description of the rapidly developing technique of ultra-small angle X-ray scattering (USAXS), a nondestructive method for probing the nano-to-micrometre scale features of hard materials. USAXS and its complementary techniques, when developed for and applied to hard materials, offer valuable insights into their porosity, grain size, phase composition and inhomogeneities. We discuss the fundamental principles, instrumentation, advantages, challenges and global status of USAXS for hard materials. Using selected examples, we demonstrate the potential of this technique for unveiling the microstructural characteristics of hard materials and its relevance to advanced materials development and manufacturing process optimization. We also provide our perspective on the opportunities and challenges for the continued development of USAXS, including multimodal characterization, coherent scattering, time-resolved studies, machine learning and autonomous experiments. Our goal is to stimulate further implementation and exploration of USAXS techniques and inspire their broader adoption across various domains of hard materials science, thereby driving the field toward discoveries and further developments.
36 MATERIALS SCIENCE↗
Evaluation of liquid cloud albedo susceptibility in E3SM using coupled eastern North Atlantic surface and satellite retrievals
The impact of aerosol number concentration on cloud albedo is a persistent source of spread in global climate predictions due to multi-scale, interactive atmospheric processes that remain difficult to quantify. We use 5 years of geostationary satellite and surface retrievals at the US Department of Energy (DOE) Atmospheric Radiation Measurement (ARM) eastern North Atlantic (ENA) site in the Azores to evaluate the representation of liquid cloud albedo susceptibility for overcast cloud scenes in the DOE Energy Exascale Earth System Model version 1 (E3SMv1) and provide possible reasons for model–observation discrepancies. The overall distribution of surface 0.2 % CCN concentration values is reasonably simulated, but simulated liquid water path (LWP) is lower than observed and layer mean droplet concentration (N d ) comparisons are highly variable depending on the N d retrieval technique. E3SMv1's cloud albedo is greater than observed for given LWP and N d values due to a lower cloud effective radius than observed. However, the simulated albedo response to N d is suppressed due to a correlation between the solar zenith angle (SZA) and N d created by the seasonal cycle that is not observed. Controlling for this effect by examining the cloud optical depth (COD) shows that E3SMv1's COD response to CCN concentration is greater than observed. For surface-based retrievals, this is only true after controlling for cloud adiabaticity because E3SMv1's adiabaticities are much lower than observed. Assuming a constant adiabaticity in surface retrievals as done in top-of-atmosphere (TOA) retrievals narrows the retrieved ln N d distribution, which increases the cloud albedo sensitivity to ln N d to match the TOA sensitivity. The greater sensitivity of COD to CCN is caused by a greater Twomey effect in which the sensitivity of N d to CCN is greater than observed for TOA-retrieved N d , and once model–observation cloud adiabaticity differences are removed, this is also true for surface-retrieved N d . The LWP response to N d in E3SMv1 is overall negative as observed. Despite reproducing the observed LWP–N d relationship, observed clouds become much more adiabatic as N d increases, while E3SMv1 clouds do not, associated with more heavily precipitating clouds that are partially but not completely caused by deeper clouds and weaker inversions in E3SMv1. These cloud property differences indicate that the negative LWP–N d relationship is likely not caused by the same mechanisms in E3SMv1 and observations. The negative simulated LWP response also fails to mute the excessively strong Twomey effect, highlighting potentially important confounding factor effects that likely render the LWP–N d relationship non-causal. N d retrieval scales and assumptions, particularly related to cloud adiabaticity, contribute to substantial spreads in the model–observation comparisons, though enough consistency exists to suggest that aerosol activation, drizzle, and entrainment processes are critical areas to focus E3SMv1 development for improving the fidelity of aerosol–cloud interactions in E3SM.
54 ENVIRONMENTAL SCIENCES↗
System and method for determining tow parameters
A system for determining one or more characteristics of a carbon fiber tow. The system including a first laser profilometer, a second laser profilometer, and a controller. The first laser profilometer is located on a first side of the carbon fiber tow. The second laser profilometer is located on a second side of the carbon fiber tow. The controller is configured to receive, from the first profilometer, a first profile of the first side of the carbon fiber tow, and receive, from the second profilometer, a second profile of the second side of the carbon fiber tow. The controller is further configured to determine at least one characteristic selected from a group consisting of a tow width of the carbon fiber tow, a tow fuzz of the carbon fiber tow, a tow thickness of the carbon fiber tow, and a tow angle of the carbon fiber tow, the at least one characteristic based on the first profile and the second profile. The controller further configured to output the at least one characteristic of the carbon fiber tow.
36 MATERIALS SCIENCE↗