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All sourcesNASA NTRSDOE OSTI
NASA NTRSDate not supplied

Numerical Modeling of No Vent Filling of a Cryogenic Tank with Thermo-dynamic Vent System Assisted Injector

This paper presents a multi-node finite volume model of No Vent Filling (NVF) of a cryogenic tank with Thermo-dynamic Vent System (TVS) assisted injector, using the Generalized Fluid System Simulation Program (GFSSP), a general purpose flow network code. NVF tests were conducted in a CRYOgenic Orbital Testbed (CRYOTE) tank which was filled by liquid nitrogen using a TVS assisted injector with vent valve closed during the entire filling process. In TVS assisted injector, the liquid flow splits into two streams: one stream is routed to a Joule-Thomson (J-T) orifice where the flow immediately flashes from liquid to vapor or two phase mixture because the downstream to J-T leg is maintained at vacuum level.; the other stream is injected into the tank after being cooled by cold vapor of J-T leg in a heat exchanger. The flow through J-T leg is also used to cool the outer metal matrix of the injector which in turn cools the vapor in the tank ullage. The cooling of vapor in the ullage by cold injector surface reduces ullage pressure that allows liquid to enter and fill the tank. An integrated numerical model of the test set up was developed. The model included the dual lines of TVS assisted injector, tank and tank wall. The tank was discretized into multiple fluid nodes and branches to represent the ullage and liquid nitrogen and multiple solid nodes to represent the tank wall and structure. The heat transfer between solid to fluid was calculated from pool boiling correlations which include film, transition, and nucleate boiling, as well as natural convection during pre- and post-boiling. The model also accounts for the condensation of vapor at ullage-injector interface and when it comes in contact with the liquid spray. The predicted pressure, resident mass, wall temperature in the tank were compared with the test data.

Alok Majumdar↗
NASA NTRS2024

Exploration Extravehicular Mobility Unit (xEMU) Lunar Boot Chamber B Thermal Vacuum Testing Results

NASA’s Exploration Extravehicular Mobility Unit (xEMU) is the government reference next-generation spacesuit design and is engineered to protect astronauts from extreme lunar environmental temperatures. To evaluate the xEMU hardware thermal requirements, the xEMU Testing Team invented, designed, and executed a dual-suit, uncrewed thermal vacuum (TVAC) test at Johnson Space Center’s (JSC) Chamber B. This paper details the test methodology, hardware setup, and results from the xEMU lunar boots. Eleven unique thermal profiles were tested including both cold and hot environmental cases over the course of five continuous days of testing. This paper will address only the cold environment testing results. The radiative thermal environment was controlled through exposure to liquid-nitrogen shrouds on the chamber walls and through a heater cage surrounding the boots. Notably, the xEMU boots also contacted the liquid-nitrogen chilled floor inside of Chamber B, which provided a conduction pathway to simulate the thermal effects of the lunar surface. Test hardware was developed to extend the water tubing from the Liquid Cooling Ventilation Garment (LCVG) into the boots to set the internal thermal boundary nominally provided by the astronaut’s foot. Thirty-three temperature sensors were used to collect data in critical locations in the xEMU boot assembly as well as for calorimetry to determine heat flux to and from the boots. This paper will document the testing results and provide a high-level interpretation of the testing results. To conclude, this paper will address possible forward work and knowledge gaps present in lunar boot thermal performance and testing.

xEMU↗
NASA NTRS2005

Actively Cooled SLMS(TM) Technology for HEL Applications

Mr. Jacoby is the Chief Scientist for Schafer's Lightweight Optical Systems business area with twenty four years experience in laser and optical systems for space and military applications. He and colleague Dr. Goodman conceived and developed Silicon Lightweight Mirrors (SLMS(TM)) technologies for space applications from the extreme UV to FAR IR wavelengths. Schafer has demonstrated two different methods for actively cooling our Silicon Lightweight Mirrors (SLMS(TM)) technology. Direct internal cooling was accomplished by flowing liquid nitrogen through the continuous open cell core of the SLMS(TM) mirror. Indirect external cooling was accomplished by flowing liquid nitrogen through a CTE matched Cesic square-tube manifold that was bonded to the back of the mirror in the center. Testing was done in the small 4-foot thermal/vacuum chamber located at the NASA/MSFC X-Ray Calibration Facility. Seven thermal diodes were located over the front side of the 5 inch diameter mirror and one was placed on the outlet side of the Cesic manifold. Results indicate that the mirror reaches steady state at 82K in less than four minutes for both cooling methods. The maximum temperature difference of the eight diodes was less than 200 mK when the mirror was internally cooled and covered with MLI to insulate it from the large 300 K aluminum plate that was used to mount it.

Jacoby, Marc T.↗
NASA NTRS1999

Carbon Fiber Reinforced/Silicon Carbide Turbine Blisk Testing in the SIMPLEX Turbopump

A program designed to implement a ceramic matrix composite integrally bladed disk (blisk) into rocket engine style turbomachinery has successfully completed testing. The Marshall Space Flight Center (MSFC) program, utilizing the MSFC turbomachinery design, analysis, and testing capabilities along with materials development capabilities from both Glenn Research Center (GRC) and MSFC, has tested two carbon fiber reinforced silicon carbide blisks in the Simplex Turbopump at MSFC's Test Stand 500. One blisk contained a polar woven fiber preform, while the second blisk tested utilized a quasi-isotropic preform. Vhile earlier papers have chronicled the program's design, material testing, and torque testing efforts, this paper focuses on the testing of the blisks in the Simplex turbopump. Emphasis will be placed on the actual condition of the blisks before and after the testing test program design methodology, and conclusions that can be drawn from the test data and blisk final conditions. The program performed three separate test series. The first series was needed to validate that the Simplex turbopump was correctly re-built following a major incident to the turbopump. The turbopump had two major differences from the original design. The most obvious difference was the sleeve required throughout the bore of the main housing. The second major difference was modifications to the pump diffuser to improve performance. Several areas were burnt during the incident and were either repaired by weld repair (pump inlet housing) or simply smoothed out (turbine nozzle discharge). The test series was designed to weed out any turbopump design and manufacturing flaws or fatigue issues prior to putting the C/SiC blisks into it. The second and third series were the C/SiC blisk test series. The primary goal of these series was to expose the blisks to as much fatigue causing dynamic stress as possible to examine the material's capability. Initially, the test plan was to put equal time on the two blisks, however, as the test series progressed, the funding allowed additional testing to occur. The additional test time was placed on the polar weave blisk. The total test time accrued on the polar blisk was 2550 seconds with 860 seconds near the turbopump design speed of 25,000 rpm. This testing included 6 tests / 775 seconds pumping liquid nitrogen and 7 tests / 1775 seconds pumping liquid oxygen. The drive gas for all of the tests was gaseous nitrogen due to the lack of hot gas source for the Simplex turbopump. The quasi-isotropic blisk was tested for XX total tests and XXXX seconds with X tests/XXXX seconds pumping liquid nitrogen and X tests/XXXX seconds pumping liquid \oxygen.During the test series, the blisks were inspected following each test. Inspections initially were viewed from the downstream side of the blisks only. Midway through the testing, a method of borescoping the leading edges of the blades was devised, and subsequently, both sides of the blades were inspected following each test. The leading and trailing edges of the polar blisk held up better than the quasi-isotropic blisk. This was a known possibility due to the varying fiber direction in the blades as the rectangular preform weave is cut in a circular pattern. The surprising fact about the testing was that there was no measurable performance loss due to the inaccuracies in the blade manufacturing in the C/SiC blisks, the surface roughness C/SiC of the blades, or the loss of the material in the polar blisk. A performance shift was seen in the quasi-isotropic blisk as portions of the leading and trailing edges were lost. After the testing was completed, detailed inspections of the blisks were performed. The largest surprise was the polar blisk had a obvious crack in a single blade that was located nearly midspan which was not detected in test. The crack ran completely through the blade circumferenciary and through the radial length of the blade. However, the crack does not appear to extend into the blisk hub. Although the cause of the crack is still under investigation, the material appears to be tolerant of this crack, and other hairline cracks discovered under higher magnification. This bodies well for eventual use of this material in actual flight turbopumps where monolithic fracture toughness issues limit its use.

Genge, Gary G.↗
NASA NTRS1993

The microstructural evolution, crystallography, and thermal processing of ultrahigh carbon Fe-1.85 pct C melt-spun ribbon

A study is presented to determine if fine microstructures could be achieved using rapid solidification to produce a fine-grained fully austenitic starting structure and then using thermal processing cycles to produce an even finer ferrite-cementite structure. The evolution, mechanisms of grain refinement, and crystallography of the resultant microstructures were examined by TEM. A thermal processing cycle consisted of quenching the ribbon in liquid nitrogen, tempering at 600 C for 10 sec, 'upquenching' to 750 C for 10 sec, and subsequently quenching again in liquid nitrogen. The heat-treatment resulted in martensite grains with sizes of about 1 micron or less in both length and thickness and cementite particles of 0.4 micron or less. It is concluded that these microstructures could be used for producing fine-grained ultrahigh carbon steels of very high strength without the brittleness associated with the formation of coarse carbide particles of the loss of strength due to graphite formation.

Spanos, G.↗
NASA NTRS1991

Liquid oxygen/metal gelled monopropellants

The objectives of this program were to establish the feasibility of metallized/liquid oxygen monopropellants and select the best monopropellant formulation for continued study. The metal powders mixed with the liquid oxygen were aluminum/magnesium (80/20), silicon and iron (Iron was only tested for burning properties). The formulations were first evaluated on whether they detonated when ignited or burned. The formulations only burned when ignited. The viscosity for the formulations ranged from 900 cps to 100 cps at shear rates up to 300 seconds(sup -1). Two percent (by weight) of Cab-O-Sil was added to the aluminum and aluminum/magnesium formulations for gelling while the silicon formulation used three percent. Within a seven hour period, settling was suggested only in the 29 percent aluminum and 29 percent aluminum/magnesium formulations. The monopropellants were burned in a cylinder submerged in a liquid nitrogen bath. Experimental data at ambient pressure indicated that the monopropellants were extinguished when the flame front reached regions submerged under the liquid nitrogen. The burn rate increased dramatically when burned in a cylinder enclosure with less heat sink available to the monopropellant. The test results were inconclusive as to whether the increased burn rate was due to the lower heat sink capacity or the small amount of pressure (2 psi) generated during the burning of the monopropellant. The burning of the aluminum and aluminum/magnesium resulted in a brilliant white flame similar to that of an arc welder. These monopropellants burned in a pulsating manner with the aluminum/magnesium appearing to have less pulsating combustion. The silicon monopropellant burned with an orange glow. No sparks or energetic burning was apparent as with the aluminum or aluminum/magnesium.

Wickman, John H.↗
NASA NTRS1992

Gelled liquid oxygen/metal powder monopropellants

Al, Al-80/Mg-20 wt pct, Si, and Fe powders were mixed with LOX and gelled with 2-3 wt pct Cab-o-Sil to viscosities of 100 to 900 cps, at shear rates of up to 300/sec. These monopropellants were burned in a cylinder that was submerged in a liquid nitrogen bath. Ambient pressure data have shown that the monopropellants were extinguished when the flame front reached regions that had been submerged under the liquid nitrogen. Burning occurred in a pulsed fashion, and was most nearly steady in the case of the Al-Mg mixture. No sparking or energetic burning occurred in any of the cases tested.

Wickman, John H.↗
NASA NTRS1982

Provisions for nonintrusive flow-evaluation tools in the National Transonic Facility

The national transonic facility fan driven, closed circuit, continuous flow, pressurized wind tunnel is examined. The test section is 2.500 m x 2.500 m and 7.620 m long with a slotted wall configuration. There are six slots each in the top and bottom walls and two slots per sidewall. To maintain good flow quality and aerodynamic efficiency over the wide range of test capabilities the test section geometry is variable. The position of the test section and bottom walls, the reentry flaps at the rear of the test section slots, and the step height for reentering slot flow are remotely controlled. The test gas may be dry air or nitrogen, which for the elevated temperature (340 K) mode of operation the test medium is normally air, and heat removal is by a water cooled heat exchanger (cooling coil) located at the upstream end of the settling chamber. For the cryogenic mode of operation, heat removal is by evaporation of liquid nitrogen, which is sprayed into the circuit upstream of the fan. By utilizing liquid nitrogen as a coolant, the tunnel test temperature range is variable from 340 to 78 K. When nitrogen is injected into the circuit, venting must occur to maintain a constant pressure. Thermal insulation is installed internal to the pressure shell to minimize energy consumption.

Fuller, D. E.↗
NASA NTRS1976

Design features and operational characteristics of the Langley 0.3-meter transonic cryogenic tunnel

Experience with the Langley 0.3 meter transonic cryogenic tunnel, which is fan driven, indicated that such a tunnel presents no unusual design difficulties and is simple to operate. Purging, cooldown, and warmup times were acceptable and were predicted with good accuracy. Cooling with liquid nitrogen was practical over a wide range of operating conditions at power levels required for transonic testing, and good temperature distributions were obtained by using a simple liquid nitrogen injection system. To take full advantage of the unique Reynolds number capabilities of the 0.3 meter transonic tunnel, it was designed to accommodate test sections other than the original, octagonal, three dimensional test section. A 20- by 60-cm two dimensional test section was recently installed and is being calibrated. A two dimensional test section with self-streamlining walls and a test section incorporating a magnetic suspension and balance system are being considered.

Kilgore, R. A.↗
NASA NTRS1981

Evaluation of several ultrasonic flowmeter transducers in cryogenic environment

Eighteen piezoelectric ultrasonic flowmeter transducers were laboratory tested to determine their suitability and long range reliability for use by the National Transonic Facility (NTF) to measure the flow rate of 450 Kg/sec of liquid nitrogen (LN2). Tests included thermally cycling each transducer 50 to 150 times over a temperature range of 295 K (ambient) to 77 K (LN2). The transducers were submerged in liquid nitrogen for 1 to 4 hours and the signal strength and quality noted. Results disclose that the current state-of-the-art ultrasonic flow transducers are very reliable and will meet the stringent requirements of the NTF.

Moughon, W. C.↗
NASA NTRS1986

Feedback-Controlled Regulation of Gas Pressure

Internal pressure maintained over wide range of external pressures and exhaust rates. Gaseous pressure in liquid-nitrogen Dewar regulated by movable tapered plug, positioned automatically in response to signals generated by piezoelectric pressure transducer. Designed specifically to maintain airborne infrared detectors at constant temperature in evaporating liquid nitrogen, system modified to regulate pressure in other enclosed systems.

Smith, J. C.↗
NASA NTRS1972

Effect of cryogenic irradiation on NERVA structural alloys

Several alloys (Hastelloy X, AISI 347, A-286 bolts, Inconel 718, Al 7039-T63 and Ti-5Al-2.5Sn ELI) were irradiated in liquid nitrogen (140 R) to neutron fluences between 10 to the 17th power and 10 to the 19th power nvt (E greater than 1.0 Mev). After irradiation, tensile properties were obtained in liquid nitrogen without permitting any warmup except for some specimens which were annealed at 540 R. The usual trend of radiation damage typical for materials irradiated at and above room temperature was observed, such as an increase in strength and decrease in ductility. However, the damage at 140 R was greater because this temperature prevented the annealing of radiation-induced defects which occurs above 140 R.

Dixon, C. E.↗
NASA NTRS1980

Experience in the control of a continuous flow cyrogenic tunnel

The concept of using liquid nitrogen to cool the test gas of a wind tunnel to cryogenic temperatures lead to the achievement of very high Reynolds number flows in relatively small transonic tunnels. The economical operation of liquid nitrogen cooled cryogenic tunnels is critically dependent on fast and accurate control of the tunnel variables. The control problem of a continuous flow fan driven cryogenic tunnel was addressed, first by developing a lumped multivariable mathematical model of a tunnel and validating the model by reconciling the responses of the Langley 0.3 m transonic cryogenic tunnel to the responses of the mathematical model on a simulator. Finally, the development of laws for the closed loop control of the tunnel pressure and temperature and the successful implementation of a control system for the 0.3 m transonic cryogenic tunnel based on these laws are presented.

Kilgore, R. A.↗
NASA NTRS2008

A Cryogenic High-Power-Density Bearingless Motor for Future Electric Propulsion

The NASA Glenn Research Center (GRC) is developing a high-power-density switched-reluctance cryogenic motor for all-electric and pollution-free flight. However, cryogenic operation at higher rotational speeds markedly shortens the life of mechanical rolling element bearings. Thus, to demonstrate the practical feasibility of using this motor for future flights, a non-contact rotor-bearing system is a crucial technology to circumvent poor bearing life that ordinarily accompanies cryogenic operation. In this paper, a bearingless motor control technology for a 12-8 (12 poles in the stator and 8 poles in the rotor) switched-reluctance motor operating in liquid nitrogen (boiling point, 77 K (-196 C or -321 F)) was presented. We pushed previous disciplinary limits of electromagnetic controller technique by extending the state-of-the-art bearingless motor operating at liquid nitrogen for high-specific-power applications. The motor was levitated even in its nonlinear region of magnetic saturation, which is believed to be a world first for the motor type. Also we used only motoring coils to generate motoring torque and levitation force, which is an important feature for developing a high specific power motor.

Choi, Benjamin↗
NASA NTRSDate not supplied

Using Digital Image Correlation for Material Testing at Cryogenic Temperatures

Recent efforts were made to parametrize an aluminum alloy at cryogenic temperatures to calibrate finite element models simulating material deformation. Digital image correlation (DIC) was used to measure material properties using front/back strains of specimens during tensile tests. Data acquired from DIC was compared to physical extensometer measurements. Two camera pairs (front and back) were mounted via aluminum extrusion to the exterior of an environmental chamber of a hydraulic test stand. Images were taken through single-pane optical glass windows of the environment chamber. Positive pressure bags encased the cameras, attaching to the perimeter of the glass to keep out moisture and prevent windows from frosting. Figure 1 shows the environmental setup and the camera setup during cryogenic testing. Some of the challenges during testing at cryogenic temperatures include the gaseous flow of liquid nitrogen in the optical path of the mounted cameras, frost buildup on the windows as seen in Figure 1b, and frost on the test coupon. The temperature gradient present during the introduction of liquid nitrogen into the chamber can increase the projection error of images captured of the specimen. Figure 2 shows the estimated projection error from DIC as a function of temperature during the cool down process. This presentation addresses some of the concerns and observations when using DIC for testing at cryogenic temperatures using methods of isolated camera system and techniques for maintaining the glass panel clear from frost.

Joseph Cochran↗
NASA NTRS1978

Variable-temperature cryogenic trap for the separation of gas mixtures

The paper describes a continuous variable-temperature U-shaped cold trap which can both purify vacuum-line combustion products for subsequent stable isotopic analysis and isolate the methane and ethane constituents of natural gases. The canister containing the trap is submerged in liquid nitrogen, and, as the gas cools, the gas mixture components condense sequentially according to their relative vapor pressures. After the about 12 min required for the bottom of the trap to reach the liquid-nitrogen temperature, passage of electric current through the resistance wire wrapped around the tubing covering the U-trap permits distillation of successive gas components at optimal temperatures. Data on the separation achieved for two mixtures, the first being typical vacuum-line combustion products of geochemical samples such as rocks and the second being natural gas, are presented, and the thermal behavior and power consumption are reported.

Des Marais, D. J.↗
NASA NTRS1996

Low Temperature Performance of a Boost Converter with MPP and HTS Inductors

Low temperature performance of a 150 W, 50 kHz, 24/48 V boost PWM dc-to-dc converter is reported. The efficiency of the converter using a molypermalloy powder (MPP) core based inductor went up from 94% at room temperature (23 C) to 95.9% at liquid nitrogen temperature (-196 C). A BSCCO based high temperature superconducting (HTS) inductor with a transition temperature of approximately -158 C was compared to a MPP core based inductor in terms of the power converter performance at liquid nitrogen temperature. The use of the HTS inductor in the converter tested yielded no significant performance improvement over the same converter with the MPP inductor. The experimental results are discussed along with the HTS inductor characteristics.

Ray, Biswajit↗
DOE OSTI2020

Petrophysical and geomechanical properties of gas hydrate-bearing sediments recovered from Alaska North Slope 2018 Hydrate-01 Stratigraphic Test Well

Knowledge of petrophysical and geomechanical properties of gas hydrate-bearing sediments are essential for predicting reservoir response due to gas production from gas hydrate reservoirs. That information will be critical parameters for designing production well completion such as specification of depressurization pump, water storage tank, and mesh size of sand screen. In December 2018, Stratigraphic Test Well Hydrate-01 was drilled in the western part of the Prudhoe Bay Unit, Alaska North Slope as part of the technical planning effort for a future long-term production test by collaborative team of DOE/NETL, USGS, and MH21-S (Boswell et al., 2020, Collett et al., 2020, Okinaka et al., 2020). Data set of logging-while-drilling (LWD) were acquired (Haines et al., 2020, Suzuki et al., 2019) and core sampling depth was determined on-site.Side-wall pressure coring was conducted to recover gas hydrate-bearing sediments from two reservoir sections named Unit-B and Unit-D. A total of 34 cores were successfully recovered by 5 runs of a wire-line deployed pressure corer (CoreVault® System - Halliburton). Core analysis scheme of this project are shown in Figure 1. All cores were quenched in liquid nitrogen while at high pressure in the laboratory of Stratum Reservoir, LLC. at Anchorage (Figure 1, a)). And the cores were removed from the pressure corer autoclave with temperature support of dry ice and stored under liquid nitrogen at atmospheric pressure. 19 damaged cores were processed to index property measurements directly such as grain size, grain density. 4 of another 17 cores were depressurized and trimmed for making a plug to analyze petrophysical properties of host sediments. Unsteady-state permeability test was conducted to obtain relative water permeability to gas and core scale NMR T2 distribution measurement was performed for evaluating pore size distribution at Houston (Figure 1, b)). Remained high quality 13 cores were preserved with gas hydrate for advanced laboratory analysis. National Institute of Advanced Industrial Science and Technology, as a part of the Japanese National Hydrate Research Program (MH21-S, funded by Ministry of Economy, Trade and Industry), received the samples at Sapporo, Japan for advanced core analysis. High-resolution X-ray CT was used to analyze the quality of the samples, which showed undisturbed lithological layers. Cores were lathed into cylindrical shape and distributed for multi property measurements (Figure 1, c)).<p>As a result, sediment from Unit-D is categorized as silty sand at ~37% porosity with ~80% gas hydrate saturation. An average hydration number n = 6.16 was measured by Raman spectroscopy. An average intrinsic permeability of ~400 mD and in situ effective permeability (with hydrate) on the order of ~10 mD. The Unit B recovered cores consisted of well sorted sand at ~40% porosity with ~95% gas hydrate saturation. An average intrinsic permeability of ~1 Darcy and in situ effective permeability on the order of ~30 mD was measured for the Unit B cores. There was a small permeability reduction due to porosity loss with increasing effective stress that simulated consolidation behavior along with depressurization in the highly permeable sandy sediment. The apparent minimum change in porosity and permeability may be caused by the low compressibility of quartz sand grains in the recovered cores. XRD and thermal conductivity analysis also suggested high quartz content. Triaxial compression tests established internal friction angles based on the Mohr-Coulomb's failure criterion, which are 40° for hydrate-bearing sediment and 29.8° for hydrate free sediment.</p>

Yoneda, Jun↗