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DOE OSTI2024

Qualifying the Instrument Thimble 11 Test Position in the Advanced Test Reactor Critical

The Advanced Test Reactor (ATR) is a versatile nuclear research reactor located at the Idaho National Laboratory (INL) in Eastern Idaho, United States of America. It is one of the most powerful and flexible research reactors in the world and is primarily used for materials testing, isotope production and basic nuclear science research. The ATR is a light-water-cooled, beryllium-moderated reactor with a nominal thermal power capacity of 250 MW utilizing specially designed fuel, arranged in a serpentine pattern to create 9 flux traps. The special design of ATR allows for the neutron flux within each of the flux traps providing flexibility for experiments, programs and allowing experiments with different dose requirements to be irradiated simultaneously. The Advance Test Reactor Critical (ATRC) is a full-scale replica of the ATR core but is housed in a pool instead of a pressure vessel. ATRC is usually operated at less than 600 watts [1]. There are 12 dry instrument thimbles located around the outside of the core tank where a variety of measurement equipment is housed to facilitate reactor operations. Currently Instrument Thimble 11 (IT-11) is not utilized in ATR or ATRC. A range of measurements is ongoing to qualify IT-11 as a test platform for nuclear instrumentation research, development and further experimentation.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2024

Initial Findings in Qualifying the Instrument Thimble 11 Position in the Advanced Test Reactor Critical

46 - INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AN↗

DOE OSTI2019

Evaluation of Anodized and Electroplated Radioactive Check Sources for Radiological Monitoring Instruments

Radioactive check sources are often used for source checking calibrated instruments to confirm accurate readings are obtained from radiological monitoring instruments. Because of the importance of check sources and their application, PNNL conducted a study to evaluate the effectiveness and accuracy of active sources produced using different construction methods. Eleven, randomly selected check sources of both anodized (five) and electroplated (six) construction were evaluated, along with their calculated decay curves, to determine how well they withstand consistent, multi-year use in the field. Results show that the anodized and electroplated check sources evaluated hold up well enough to continue their use, regardless of wear and tear sustained over years of use. This report provides the source information, empirical data for the 11 anodized and electroplated check sources and their representative decay curves, and it documents the conclusion that anodized and electroplated check sources are reliable for routine use in the field over multiple years.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2022

Cyber-Informed Engineering for Nuclear Reactor Digital Instrumentation and Control

As nuclear reactors transition from analog to digital technology, the benefits of enhanced operational capabilities and improved efficiencies are potentially offset by cyber risks. Cyber-Informed Engineering (CIE) is an approach that can be used by engineers and staff to characterize and reduce new cyber risks in digital instrumentation and control systems. CIE provides guidance that can be applied throughout the entire systems engineering lifecycle, from conceptual design to decommissioning. In addition to outlining the use of CIE in nuclear reactor applications, this chapter provides a brief primer on nuclear reactor instrumentation and control and the associated cyber risks in existing light water reactors as well as the digital technology that will likely be used in future reactor designs and applications.

42 ENGINEERING↗

DOE OSTI2020

Software Framework for Federated Science Instruments

There is an unprecedented promise of enhanced capabilities for federations of leadership computing systems and experimental science facilities by leveraging software technologies for fast and efficient operations. These federations seek to unify different science instruments, both computing and experimental, to effectively support science users and operators to execute complex workflows. The FedScI project addresses the software challenges associated with the formation and operation of federated environments by leveraging recent advances in containerization of software and softwarization of hardware. We propose a software framework to streamline the federation usage by science users and it’s provisioning and operations by facility providers. A distinguishing element of our work is the support for improved interaction between experimental devices, such as beam-line instruments, and more traditional high-performance computing resources, including compute, network, storage systems. We present guiding principles for the software framework and highlight portions of a current prototype implementation. We describe our science use case involving neutron imaging beam-lines (SNAP/BL-3, Imaging/CG-1D) at the Spallation Neutron Source and High Flux Isotope Reactor facilities at Oak Ridge National Laboratory. Additionally, we detail plans for a more direct instrument interaction within a federated environment, which could enable more advanced workflows with feedback loops to shorten the time to science.

Naughton III, Thomas↗

DOE OSTI2022

Harmonizing solar induced fluorescence across spatial scales, instruments, and extraction methods using proximal and airborne remote sensing: A multi-scale study in a soybean field

Solar-induced chlorophyll fluorescence (SIF) has been widely used to track vegetation photosynthesis at different scales ranging from in-situ measurements to satellite products. Airborne platforms sample SIF data at a spatial scale intermediate between in-situ and satellite, matching that of ground measurement (e.g. flux tower footprints and other field sampling), enabling us to explore causes of SIF variation and validate satellite-based SIF products. However, harmonizing SIF across sensors and platforms (correcting for systematic errors to yield a consistent, comparable SIF product) is challenging because SIF can be retrieved in different absorption windows, with different instruments and methods complicating the comparison between different observational levels (i.e., ground, airborne, satellites) and between sites equipped with different instruments with varying optical properties (spectral resolution and sampling intervals, spatial resolution). Additionally, the spatial and temporal variability of atmospheric properties can influence the retrieval of the weak SIF signal. Because of these complications, direct comparisons of airborne and ground SIF across scales are rarely attempted. Here, in this study, we combined airborne SIF data with simultaneous ‘ground truth’ data collected by stationary and mobile platforms in a soybean field in Nebraska, USA. In this effort, we tested several SIF extraction methods, including Fraunhofer Line Discrimination (FLD), improved Fraunhofer Line Discrimination (iFLD), Spectral Fitting Method (SFM), SpecFit, and a Singular Vector Decomposition (SVD) method. The SpecFit method was sensitive to the 715–740 nm water bands and removing the water bands in the fitting process yielded better agreement between the airborne and ground SIF spectra. Accurate estimation of the ground level downwelling irradiance obtained by ground measurements over a calibration target improved agreement between airborne and ground SIF retrievals at the O 2 A band, and allowed us to derive a SIF dataset with improved agreement across platforms and sampling scales. This experimental approach provided a method for generating comparable SIF signals across instruments, methods and platforms, which is critical to understanding the SIF-GPP relationship at different scales and to cross-validate the diversity of platforms used for satellite products calibration and validation.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2023

Blowing Snow at McMurdo Station, Antarctica During the AWARE Field Campaign: Multi-Instrument Observations of Blowing Snow

In polar regions, blowing snow (BLSN) can play a substantial role in regional thermodynamics and radiation properties. The extent of the impact depends upon the depth of the BLSN layer, a property that is difficult to measure and not well understood. The West Antarctic Radiation Experiment (AWARE) Field Campaign saw the deployment of a large suite of observational instruments to McMurdo Station, Antarctica, allowing for in-depth investigation of BLSN. During the year of the campaign, BLSN occurred ~7.4% of the time. In this study, additional remote sensing observations are used to supplement an existing ceilometer-based BLSN characterization algorithm creating a multi-instrument (MI) depth estimation algorithm to yield layer depths with more certainty. Backscatter coefficient and linear depolarization ratios from the micropulse and high spectral resolution lidar (HSRL) are incorporated along with color ratio derived from HSRL backscatter and Ka-band radar reflectivity observations. This provided estimates of BLSN depth that were less impacted by noise/artifacts in any one set of observations. When applied to the data from AWARE, the MI algorithm yielded an average depth of 168.2 m with ~60% of plumes less than 200 m in depth. Events occurring with precipitation saw the most value in the additional instruments, with the suite of observations allowing for more separation of BLSN particles from fallstreaks.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2026

Operating advanced scientific instruments with AI agents that learn on the job

Advanced scientific user facilities, such as next generation X-ray light sources and self-driving laboratories, are revolutionizing scientific discovery by automating routine tasks and enabling rapid experimentation and characterizations. However, these facilities must continuously evolve to support new experimental workflows, adapt to diverse user projects, and meet growing demands for more intricate instruments and experiments. This continuous development introduces significant operational complexity, necessitating a focus on usability, reproducibility, and intuitive human-instrument interaction. In this work, we explore the integration of agentic AI, powered by Large Language Models (LLMs), as a transformative tool to achieve this goal. We present our approach to developing a human-in-the-loop pipeline for operating advanced instruments including an X-ray nanoprobe beamline and an autonomous robotic station dedicated to the design and characterization of materials. Specifically, we evaluate the potential of various LLMs as trainable scientific assistants for orchestrating complex, multi-task workflows, which also include multimodal data, optimizing their performance through optional human input and iterative learning. We demonstrate the ability of AI agents to bridge the gap between advanced automation and user-friendly operation, paving the way for more adaptable and intelligent scientific facilities.

Large Language Models↗

DOE OSTI2020

Planck 2018 Results - II. Low Frequency Instrument data processing

We present a final description of the data-processing pipeline for the Planck Low Frequency Instrument (LFI), implemented for the 2018 data release. Several improvements have been made with respect to the previous release, especially in the calibration process and in the correction of instrumental features such as the effects of nonlinearity in the response of the analogue-to-digital converters. We provide a brief pedagogical introduction to the complete pipeline, as well as a detailed description of the important changes implemented. Self-consistency of the pipeline is demonstrated using dedicated simulations and null tests. We present the final version of the LFI full sky maps at 30, 44, and 70 GHz, both in temperature and polarization, together with a refined estimate of the solar dipole and a final assessment of the main LFI instrumental parameters.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2013

Nano-level instrumentation for analyzing the dynamic accuracy of a rolling element bearing

The rotational performance of high-precision rolling bearings is fundamental to the overall accuracy of complex mechanical systems. A nano-level instrument to analyze rotational accuracy of high-precision bearings of machine tools under working conditions was developed. In this instrument, a high-precision (error motion < 0.15 μm) and high-stiffness (2600 N axial loading capacity) aerostatic spindle was applied to spin the test bearing. Operating conditions could be simulated effectively because of the large axial loading capacity. An air-cylinder, controlled by a proportional pressure regulator, was applied to drive an air-bearing subjected to non-contact and precise loaded axial forces. The measurement results on axial loading and rotation constraint with five remaining degrees of freedom were completely unconstrained and uninfluenced by the instrument's structure. Dual capacity displacement sensors with 10 nm resolution were applied to measure the error motion of the spindle using a double-probe error separation method. This enabled the separation of the spindle's error motion from the measurement results of the test bearing which were measured using two orthogonal laser displacement sensors with 5 nm resolution. Finally, a Lissajous figure was used to evaluate the non-repetitive run-out (NRRO) of the bearing at different axial forces and speeds. The measurement results at various axial loadings and speeds showed the standard deviations of the measurements’ repeatability and accuracy were less than 1% and 2%. Future studies will analyze the relationship between geometrical errors and NRRO, such as the ball diameter differences of and the geometrical errors in the grooves of rings.

42 ENGINEERING↗

DOE OSTI2014

A multi-functional testing instrument for heat assisted magnetic recording media

With recent developments in heat assisted magnetic recording (HAMR), characterization of HAMR media is becoming very important. We present a multi-functional instrument for testing HAMR media, which integrates HAMR writing, reading, and a micro-magneto-optic Kerr effect (μ-MOKE) testing function. A potential application of the present instrument is to make temperature dependent magnetic property measurement using a pump-probe configuration. In the measurement, the media is heated up by a heating (intense) beam while a testing (weak) beam is overlapped with the heating beam for MOKE measurement. By heating the media with different heating beam power, magnetic measurements by MOKE at different temperatures can be performed. Compared to traditional existing tools such as the vibrating sample magnetometer, the present instrument provides localized and efficient heating at the measurement spot. The integration of HAMR writing and μ-MOKE system can also facilitate a localized full investigation of the magnetic media by potential correlation of HAMR head independent write/read performance to localized magnetic properties.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

DOE OSTI2014

High-precision instrument for measuring the surface tension, viscosity and surface viscoelasticity of liquids using ripplon surface laser-light scattering with tunable wavelength selection

Here we describe our new high-precision instrument that simultaneously measures the surface tension, viscosity, and surface viscoelasticity of liquids. The instrument works on the ripplon surface-laser light scattering principle and operates with an automatically tunable selection of ripplon wavelength from 4 to 1500 μm, which corresponds to the frequency range of observing surface phenomena from approximately 400 Hz to 3 MHz in the case of water. The heterodyne technique instrument uses a reference laser beam which intersects at an arbitrarily adjustable angle with a vertically directed probing beam. For the determination of the wavelength of selected ripplons we substituted with the interference fringe spacing, measured using a high-resolution beam profiler. To extract reliable surface tension and viscosity data from the experimentally obtained spectrum shape for a selected wavelength of ripplon, we developed an algorithm to calculate the exact solution of the dispersion equation. The uncertainties of surface tension and viscosity measurement were confirmed through the measurement of seven pure Newtonian liquids at 25 °C measured with the selected wavelength of ripplon from 40 μm to 467 μm. To verify the genuine capability of the tunable wavelength selection of ripplon, we measured the surface elasticity of soluble surface molecular layers spread on pentanoic acid solutions.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

DOE OSTI2021

Post-irradiation examination of optical components for advanced fission reactor instrumentation

The use of optical instrumentation in advanced nuclear fission systems, such as molten salt reactors, liquid metal-cooled reactors, and high-temperature gas-cooled reactors, has the potential to enhance reactor safety and economic performance through in situ and online measurement of reactor conditions. Selection of suitable optical components, such as optical windows and fibers, is essential for operation of optical instrumentation in intense radioactive and thermal environments inherent to nuclear reactor systems. We present the development and performance of a self-contained and mobile post-irradiation examination system for rapid characterization of the optical properties of materials. The instrument combines linear absorption and nanosecond Z-scan modules in a compact, relocatable design. The system mobility allows for the evaluation of optical samples at the site of irradiation, minimizing the delay between extraction from the irradiation site and optical characterization. This provides nearly real-time information on the material performance under simultaneous irradiation and thermal annealing, simulating the relevant conditions for the use of those components in nuclear power systems.

Morgan, Bryan William (ORCID:0000000224668764)↗

DOE OSTI2022

An automated fast neutron computed tomography instrument with on-line focusing for non-destructive evaluation

A fast neutron tomography imaging instrument has been designed, built, and tested at The Ohio State University 500 kW Research Reactor on a fast neutron beamline with a peak neutron flux ≈5.4 × 107 n·cm−2·s−1 at 1.6 MeV median neutron energy. The instrument and beamline are also configurable for thermal neutron imaging. The imaging apparatus is composed of a lens coupled, water-cooled Electron Multiplying Charge Coupled Device camera, a front-surface mirror, and a high light yield plastic Polyvinyl toluene scintillator. The instrument sits on a mobile cart. A total of 5 motion-control stages are built into the system for XYZ and rotational degrees of freedom for sample positioning; the fifth stage fine tunes the focal distance between the camera and the scintillator to achieve on-line focusing. A Python code with a user-friendly graphical user interface controls the fully automated image acquisition, not requiring user interaction, yet facilitating tracking of the image acquisition. A complete fast neutron computed tomography dataset with 360 projections requires less than 3 h, with 30 s per projection. On-line focusing is accomplished with a commercial, off-the-shelf, dielectrically actuated liquid lens. Finally, tomographic reconstructions are visualized using the Livermore Tomography Tools software package. The effective pixel size (width and height) is ≈0.1058 mm, yielding a minimum voxel size of 0.1058 × 0.1058 × 0.1058 mm3, and produces a spatial resolution of 231 μm when calculated from knife-edge measurements.

Bisbee, M. G. (ORCID:0000000313466697)↗

DOE OSTI2024

Shock compression experiments using the DiPOLE 100-X laser on the high energy density instrument at the European x-ray free electron laser: Quantitative structural analysis of liquid Sn

X-ray free electron laser (XFEL) sources coupled to high-power laser systems offer an avenue to study the structural dynamics of materials at extreme pressures and temperatures. The recent commissioning of the DiPOLE 100-X laser on the high energy density (HED) instrument at the European XFEL represents the state-of-the-art in combining x-ray diffraction with laser compression, allowing for compressed materials to be probed in unprecedented detail. Here, we report quantitative structural measurements of molten Sn compressed to 85(5) GPa and ~3500 K. The capabilities of the HED instrument enable liquid density measurements with an uncertainty of ~1% at conditions which are extremely challenging to reach via static compression methods. We discuss best practices for conducting liquid diffraction dynamic compression experiments and the necessary intensity corrections which allow for accurate quantitative analysis. We also provide a polyimide ablation pressure vs input laser energy for the DiPOLE 100-X drive laser which will serve future users of the HED instrument.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

DOE OSTI2025

Mechanical design of a parallel flexure-based RADSI instrument for curved x-ray mirror metrology

Modern synchrotron x-ray beamlines demand reflective optics with higher surface profile accuracy to achieve diffraction-limited focusing. This necessitates advanced metrology instruments capable of delivering repeatable measurements in the nanometer to sub-nanometer range. Slope ranges exceeding 15 mrad (0.86°) and greater pose significant challenges for mirror metrology using conventional interferometric methods. Here, to address this, we present a new relative angle determinable stitching interferometry instrument featuring a parallel flexure-based mechanical design. This approach enhances vibration and thermal stability while maintaining a compact and lightweight system. Initial measurements of a cylindrical mirror with a 16 m radius of curvature and a slope range of 5 mrad demonstrate nanometer-level repeatability. Comprehensive system characterization suggests the potential for achieving sub-nanometer repeatability with further refinement to the instrument.

36 MATERIALS SCIENCE↗

DOE OSTI2014

A multi-instrument analysis of sunspot umbrae

The recent solar minimum and rise phase of solar cycle 24 have been unlike any period since the early 1900s. This article examines some of the properties of sunspot umbrae over the last 17 yr with three different instruments on the ground and in space: MDI, HMI and BABO. The distribution of magnetic fields and their evolution over time is shown and reveals that the field distribution in cycle 24 is fundamentally different from that in cycle 23. The annual average umbral magnetic field is then examined for the 17 yr observation period and shows a small decrease of 375 G in sunspot magnetic fields over the period 1996-2013, but the mean intensity of sunspot umbrae does not vary significantly over this time. A possible issue with sample sizes in a previous study is then explored to explain disagreements in data from two of the source instruments. All three instruments show that the relationship between umbral magnetic fields and umbral intensity agrees with past studies in that the umbral intensity decreases as the field strength increases. This apparent contradiction can be explained by the range of magnetic field values measured for a given umbral intensity being larger than the measured 375 G change in umbral field strength over time.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2023

Conceptual Polarization Setup at CENTAUR, the SANS/WANS Instrument at the Second Target Station of SNS

CENTAUR is a multifunctional general purpose small-angle and wide-angle neutron scattering instrument with diffraction and spectroscopic capability in the future Second Target Station at the Spallation Neutron Source of the Oak Ridge National Laboratory. To fill a gap in neutron polarization capability, the instrument will be designed to provide polarization analysis. Here we present the conceptual polarization setup at CENTAUR, as well as the Spin Echo Modulated Small-Angle Neutron Scattering setup which will further expand the length scale covered by the instrument.

Qian, Shuo↗