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At least 253 records · Page 14
All sourcesNASA NTRSDOE OSTI
NASA NTRS1999

Use of Microgravity to Control the Microstructure of Eutectics

This grant began in June of 1996. Its long term goal is to be able to control the microstructure of directionally solidified eutectic alloys, through an improved understanding of the influence of convection. The primary objective of the projects in the present grant is to test hypotheses for the reported influence of microgravity on the microstructure of eutectics. The prior experimental results on the influence of microgravity on the microstructure of eutectics have been contradictory. With lamellar eutectics, microgravity had a negligible effect on the microstructure. Microgravity experiments with fibrous eutectics sometimes showed a finer microstructure and sometimes a coarser microstructure. Most research has been done on the MnBi/Bi rod-like eutectic. Larson and Pirich obtained a two-fold finer microstructure both from microgravity and by use of a magnetic field to quench buoyancy-driven convection. Smith, on the other hand, observed no change in microgravity. Prior theoretical work at Clarkson University showed that buoyancy-driven convection in the vertical Bridgman configuration is not vigorous enough to alter the concentration field in front of a growing eutectic sufficiently to cause a measurable change in microstructure. We assumed that the bulk melt was at the eutectic composition and that freezing occurred at the extremum, i.e. with minimum total undercooling at the freezing interface. There have been four hypotheses attempting to explain the observed changes in microstructure of fibrous eutectics caused by convection: I .A fluctuating freezing rate, combined with unequal kinetics for fiber termination and branching. 2. Off-eutectic composition, either in the bulk melt due to an off-eutectic feed or at the freezing interface because of departure from the extremum condition. 3. Presence of a strong habit modifying impurity whose concentration at the freezing interface would be altered by convection. At the beginning of the present grant, we favored the first of these hypotheses and set out to test it both experimentally and theoretically. We planned the following approaches: I .Pass electric current pulses through the MnBi/Bi eutectic during directional solidification in order to produce an oscillatory freezing rate. 2. Directionally solidify the MnBi/Bi eutectic on Mir using the QUELD II gradient freeze furnace developed by Professor Smith at Queen's University. 3. Select another fibrous eutectic system for investigation using the Accelerated Crucible Rotation Technique to introduce convection. 4. Develop theoretical models for eutectic solidification with an oscillatory freezing rate. Because of the problems with Mir, we substituted ground-based experiments at Queen's University with QUELD II vertical and horizontal, with and without vibration of the furnace. The Al-Si system was chosen for the ACRT experiments. Three related approaches were used to model eutectic solidification with an oscillatory freezing rate. A sharp interface model was used to calculate composition oscillations at the freezing interface in response to imposed freezing rate oscillations.

Wilcox. William R.↗
NASA NTRS1998

Use of Microgravity to Control the Microstructure of Eutectics

This grant began in June of 1996. Its long term goal is to be able to control the microstructure of directionally solidified eutectic alloys, through an improved understanding of the influence of convection. The primary objective of the present projects is to test hypotheses for the reported influence of microgravity on the microstructure of three fibrous eutectics (MnBi-Bi, InSb-NiSb, Al3Ni-Al). A secondary objective is to determine the influence of convection on the microstructure of other eutectic alloys. Two doctoral students and a masters student supported as a teaching assistant were recruited for this research. Techniques were developed for directional solidification of MnBi-Bi eutectics with periodic application of current pulses to produce an oscillatory freezing rate. Image analysis techniques were developed to obtain the variation in MnBi fiber spacing, which was found to be normally distributed. The mean and standard deviation of fiber spacing were obtained for several freezing conditions. Eighteen ampoules were prepared for use in the gradient freeze furnace QUELD developed at Queen's University for use in microgravity. Nine of these ampoules will be solidified soon at Queen's in a ground-based model. We hope to solidify the other nine in the QUELD that is mounted on the Canadian Microgravity Isolation Mount on MIR. Techniques are being developed for directional solidification of the Al-Si eutectic at different freezing rates, with and without application of accelerated crucible rotation to induce convection. For the first time, theoretical methods are being developed to analyze eutectic solidification with an oscillatory freezing rate. In a classical sharp-interface model, we found that an oscillatory freezing rate increases the deviation of the average interfacial composition from the eutectic, and increases the undercooling of the two phases by different amounts. This would be expected to change the volume fraction solidifying and the fiber spacing. Because of difficulties in tracking the freezing interfaces of the two solid phases, a phase-field model is also being developed. A paper demonstrating application of phase field methods to periodic structures has been submitted for publication.

Wilcox, William R.↗
NASA NTRS2018

Evaluation of a Thermodynamic Ice Crystal Icing Model Using Experimental Ice Accretion Data

This paper presents the evaluation of a thermodynamic ice crystal icing model, previously presented to describe the possible mechanisms of icing within the core of a turbofan jet engine. It has been proposed that there are two types of distinct ice accretions based on a surface energy balance: freeze-dominated icing and melt-dominated icing. In the former, ice accretion occurs where a freeze fraction (0 to 1) of melted ice crystals freezes on a surface, along with the existing ice of the impinging water and ice mass. This freeze-dominated icing is characterized by having strong adhesion to the surface. In the latter, icing occurs from accumulated unmelted ice on a surface, where a melt fraction (0 to 1) dictates the amount of unmelted impinged ice. This melt-dominated icing is characterized by weakly bonded surface adhesion. The experimentally observed ice growth rates suggest that only a small fraction of the impinging ice remains on the surface, implying a mass loss mechanism such as splash, runback, bounce, or erosion. This mass loss parameter must be determined in conjunction with the fraction of freezing liquid water or fraction of melting ice on an icing surface. This loss parameter, however, along with the freeze and melt fraction, are the only experimental parameters that are currently not measured directly. Using reported icing growth rates from published ice crystal icing experiments, a methodology is proposed to determine these unknown parameters. This work takes reported ice accretion data from tests conducted by the National Aeronautics and Space Administration (NASA) in 2016 and tests NASA collaborated on with the National Research Council (NRC) of Canada in 2012 that examined the fundamental physics of ice crystal icing. Those research efforts sought to generate icing conditions representative of those that occur inside a jet engine when ingesting ice crystals. This paper presents the fundamental equations of the thermodynamic model, the methodology used to determine the aforementioned unknown icing parameters, and results from model evaluation using experimental data. In addition, this paper builds on the previously proposed model by adding a transient conduction term to explain ice growth behavior at the onset of experimental tests that was observed to be different from steady-state ice growth that occurred later in the test run.With the addition of this energy term, this becomes a quasi-steady model. A key finding from this work suggests that mass loss fractions can exceed 0.90 for steady ice growth periods. In addition, due to conductive heat fluxes when using a warmer-than-freezing airfoil, lower mass loss fraction values were calculated during the initial transient period.

Ice-Crystal Ice Accretion↗
NASA NTRS1972

Mechanisms of deterioration of nutrients phase 1

Experimental methods are studied by which freeze-dried foods of improved quality are produced. Considered are: (1) Factors effecting the loss of butanol from frozen aqueous food solutions during storage; (2) a freeze-drying microscope system for observing solidification processes in organic mixtures and aqueous inorganic salt solutions; (3) browning of high quality freeze-dried foods with minimal organoleptic and nutritional detoriation; (4) retention of PVP-n-propanol in freeze-dried food models; and (5) effects of freezing rate and sucrose immersion on taste and texture of freeze-dried apple slices.

Karel, M.↗
NASA NTRS1996

Development of the gametophyte of the fern Schizaea pusilla

Schizaea pusilla is a pteridophyte with several unique developmental characteristics. In contrast to most other fern species, S. pusilla gametophytes remain filamentous throughout their development, and the gametophytes are associated with an endophytic fungus which appears to be mycorrhizal. In terms of tropistic responses, apical filament cells of young gametophytes are negatively phototropic compared with germ filaments of other ferns which exhibit positive phototropism. Cryofixation (propane jet freezing and high-pressure freezing) in conjunction with freeze substitution electron microscopy was used to study young gametophytes. The results demonstrate that apical filament cells have a distinctive structural polarity and that rhizoids also can be successfully frozen by these methods. The cytoskeleton and endomembrane system were particularly well preserved in cryofixed cells. In addition, Schizaea gametophytes were used as a test system to evaluate potential artifacts of propane jet freezing and high pressure freezing. There was little apparent difference in ultrastructure between cells cryofixed by either freezing method. These gametophytes will be useful in determining the effectiveness of cryofixation techniques and as a model system in tip growth studies.

Non-NASA Center↗
NASA NTRS1978

Easy Meal

The woman pictured below is sitting down to a nutritious, easily-prepared meal similar to those consumed by Apollo astronauts. The appetizing dishes shown were created simply by adding water to the contents of a Mountain House* Easy Meal package of freeze dried food. The Easy Meal line is produced by Oregon Freeze Dry Foods, Inc., Albany, Oreaon, a pioneer in freeze drying technology and a company long associated with NASA in developing suitable preparations for use on manned spacecraft. Designed to provide nutritionally balanced, attractive hot meals for senior adults, Easy Meal is an offshoot of a 1975-77 demonstration project managed by Johnson Space Center and called Meal System for the Elderly. The project sought ways to help the estimated 3.5 million elderly Americans who are unable to take advantage of existing meal programs. Such services are provided by federal, state and local agencies, but they are not available to many who live in rural areas, or others who are handicapped, temporarily ill or homebound for other reasons. Oregon Freeze Dry Foods was a participant in that multi-agency cooperative project. With its Easy Meal assortment of convenience foods pictured above left, the company is making commercially available meal packages similar to those distributed in the Meal System for the Elderly program. In the freeze drying process, water is extracted from freshly-cooked foods by dehydration at very low temperatures, as low as 50 I degrees below zero. Flavor is locked in by packaging the dried food in pouches which block out moisture and oxygen, the principal causes of food deterioration; thus the food can be stored for long periods without refrigeration. Meals are reconstituted by adding hot or cold water, depending on the type of food, and they are table ready in five to 10 minutes. Oregon Freeze Dry Foods offers five different meal packages and plans to expand the line.

Source record↗
NASA NTRS2015

Integration of Product, Package, Process, and Environment: A Food System Optimization

The food systems slated for future NASA missions must meet crew nutritional needs, be acceptable for consumption, and use resources efficiently. Although the current food system of prepackaged, moderately stabilized food items works well for International Space Station (ISS) missions, many of the current space menu items do not maintain acceptability and/or nutritive value beyond 2 years. Longer space missions require that the food system can sustain the crew for 3 to 5 years without replenishment. The task "Integration of Product, Package, Process, and Environment: A Food System Optimization" has the objective of optimizing food-product shelf life for the space-food system through product recipe adjustments, new packaging and processing technologies, and modified storage conditions. Two emergent food processing technologies were examined to identify a pathway to stable, wet-pack foods without the detrimental color and texture effects. Both microwave-assisted thermal sterilization (MATS) and pressure-assisted thermal stabilization (PATS) were evaluated against traditional retort processing to determine if lower heat inputs during processing would produce a product with higher micronutrient quality and longer shelf life. While MATS products did have brighter color and better texture initially, the advantages were not sustained. The non-metallized packaging film used in the process likely provided inadequate oxygen barrier. No difference in vitamin stability was evident between MATS and retort processed foods. Similarly, fruit products produced using PATS showed improved color and texture through 3 years of storage compared to retort fruit, but the vitamin stability was not improved. The final processing study involved freeze drying. Five processing factors were tested in factorial design to assess potential impact of each to the quality of freeze-dried food, including the integrity of the microstructure. The initial freezing rate and primary freeze drying temperature and pressure were linked to final product quality in freeze-dried corn, indicating processing modifications that could lead to improved product shelf life. Storage temperatures and packaging systems were also assessed for the impact to food quality. Reduced temperature storage had inconclusive impact to the progression of rancidity in butter cookies. Frozen storage was detrimental to fruit and vegetable textural attributes but refrigerated storage helped to sustain color and organoleptic ratings for plant-based foods. With regard to packaging systems, the metallized film overwrap significantly decreased the progression of the rancidity of butter cookies as compared to the highest barrier non-metallized film. The inclusion of oxygen scavengers resulted in noticeable moisture gains in butter cookies over time, independent of packaging film systems. Neither emergent processing technology nor the freeze dry optimization resulted in compelling quality differences from current space food provisions such that a five-year shelf life is likely with these processing changes alone. Using a combination of refrigeration and PATS processing is expected to result in organoleptically-acceptable fruit quality for most fruits through five years. The vitamin degradation will be aided somewhat by the cold temperatures but, given the labile nature of vitamin C, a more stable fortification method, such as encapsulation, should also be investigated to ensure vitamin delivery throughout the product life. Similarly, significant improvement to the packaging film used in the MATS processing, optimization of formulation for dielectric properties, vitamin fortification, and reduced temperature storage should be investigated as a hurdle approach to reach a five year shelf life in wet-pack entrees and soups. Baked goods and other environmentally-sensitive spaceflight foods will require an almost impenetrable barrier to protect the foods from oxygen and moisture ingress but scavengers and reduced storage temperature did not improve baked good shelf life and are not recommended at this time for these foods.

Cooper, Maya R.↗
NASA NTRS2023

Seasonal Soil Freeze/Thaw Variability Across North America via Ensemble Land Surface Modeling

Land surface modeling provides the opportunity to investigate winter soil processes such as soil freezing and thawing over large domains. However, the variability in simulated winter soil characteristics among land surface models and forcing datasets is not well understood. In this study, a nine-member ensemble was employed to characterize the spatial and inter-annual variability of three winter soil characteristics, annual number of frozen days, annual minimum temperature and annual number of freeze-thaw cycles over North America during the water years 2010–2016. The ensemble, including three land surface model (JULES, Noah2.7.1 and Noah-MP) and three forcing datasets (ECMWF, GDAS and MERRA2), was developed through the Snow Ensemble Uncertainty Project (SEUP). In many regions, there was remarkably good agreement across the ensemble for the winter soil temperatures. However, the variability among the ensemble's annual number of frozen days, as quantified with standard deviation, exceeded 150 days at the northern Pacific coastline. While the differences among the ensemble members' annual minimum temperature were typically <3 °C, the differences exceeded 6 °C north of 50°N. The ensemble members generally agreed within one to three freeze-thaw cycles in mid latitude regions, Alaska, and the south and west coasts of the USA. High variability among the ensemble, more than six freeze-thaw cycles, occurred in the Great Plains, northern Pacific coastline, and along the Appalachian Mountains. Differences in winter soil temperature characteristics were more apparent among the LSMs rather than the meteorological forcing datasets. Except for maritime regions, the Noah2.7.1 members had the fewest annual number of frozen days and the least number of freeze-thaw cycles. Noah2.7.1 also had the coldest annual minimum temperatures except for ephemeral regions. Comparisons between in-situ observations and the SEUP estimates of winter soil characteristics revealed that the modeled frozen period was much longer than observed, that the modeled annual minimum temperatures were much colder than observed, and the modeled freeze-thaw cycles occurred more frequently than observed. Excluding the high latitude sites, the observed frozen period is less than two months with the minimum temperature above − 5 °C at most of the studied sites, while the ensemble members simulated, on average, a four month frozen period with − 10 °C minimum temperature. Errors in capturing snow during the accumulation period appear to impact differences in modeled versus observed soil temperature throughout the entire winter.

Soil freeze/thaw↗
NASA NTRS2021

Aerosol–Ice Formation Closure: A Southern Great Plains Field Campaign

Prediction of ice formation in clouds presents one of the grand challenges in the atmospheric sciences. Immersion freezing initiated by ice-nucleating particles (INPs) is the dominant pathway of primary ice crystal formation in mixed-phase clouds, where supercooled water droplets and ice crystals coexist, with important implications for the hydrological cycle and climate. However, derivation of INP number concentrations from an ambient aerosol population in cloud-resolving and climate models remains highly uncertain. We conducted an aerosol-ice formation closure pilot study using a field-observational approach to evaluate the predictive capability of immersion freezing INPs. The closure study relies on co-located measurements of the ambient size-resolved and single-particle composition and INP number concentrations. The acquired particle data serve as input in several immersion freezing parameterizations, that are employed in cloud-resolving and climate models, for prediction of INP number concentrations. We discuss in detail one closure case study in which a front passed through the measurement site, resulting in a change of ambient particle and INP populations. We achieved closure in some circumstances within uncertainties, but we emphasize the need for freezing parameterization of potentially missing INP types and evaluation of the choice of parameterization to be employed. Overall, this closure pilot study aims to assess the level of parameter details and measurement strategies needed to achieve aerosol-ice formation closure. The closure approach is designed to accurately guide immersion freezing schemes in models, and ultimately identify the leading causes for climate model bias in INP predictions.

ice formation↗
NASA NTRS1976

Mechanisms of deterioration of nutrients

Methods which produce freeze dried foods of improved quality were examined with emphasis on storage stability. Specific topics discussed include: microstructure of freeze dried systems, investigation of structural changes in freeze dried systems, artificial food matrices, osmotic preconcentration to yield improved quality freeze dried fruits, and storage stability of osmotically preconcentrated freeze dried fruits.

Karel, M.↗
NASA NTRS1958

A Flight Evaluation and Analysis of the Effect of Icing Conditions on the ZPG-2 Airship

A series of test flights was conducted by the U. S. Navy over a 3- year period to evaluate the effects of icing on the operation of the ZPG-2 airship. In supercooled. clouds, ice formed only on the forward edges of small protuberances and wires and presented no serious hazard to operation. Ice accretions of the glaze type which occurred in conditions described as freezing drizzle adversely affected various components to a somewhat greater extent. The results indicated, a need for protection of certain components such as antennas, propellers, and certain parts of the control system. The tests showed that icing of the large surface of the envelope occurred only in freezing rain or drizzle. Because of the infrequent occurrence of these conditions, the potential maximum severity could not be estimated from the test results. The increases in heaviness caused by icing in freezing rain and drizzle were substantial, but well within the operational capabilities of the airship. In order to estimate the potential operational significance of icing in freezing rain, theoretical calculations were used to estimate: (1) the rate of icing as a function of temperature and rainfall intensity, (2) the climatological probability of occurrence of various combinations of these variables, and (3) the significance of the warming influence of the ocean in alleviating freezing-rain conditions. The results of these calculations suggest that, although very heavy icing rates are possible in combinations of low temperature and high rainfall rate, the occurrence of such conditions is very infrequent in coastal areas and virtually impossible 200 or 300 miles offshore.

Lewis, Willilam↗
NASA NTRS1984

Study of eutectic formation

A theory was developed for the influence of convection on the microstructure of lamellar eutectics. Convection is predicted to produce a coarser microstructure, especially at low freezing rates and large volume fractions of the minority phase. Similary convection is predicted to lower the interfacial undercooling, especially at low freezing rates. Experiments using spin-up/spin-down were performed on the Mn-Bi eutectic. This stirring had a dramatic effect on the microstructure, not only making it coarser but at low freezing rates also changing the morphology of the MnBi. The coarsering persisted to moderately high freezing rates. At the lowest freezing rate, vigorous stirring caused the MnBi to be concentrated at the periphery of the ingot and absent along the center. Progress was made on developing a technique for revealing the three-dimensional microstructure of the MnBi eutectic by time-lapse videotaping while etching.

Wilcox, W. R.↗
NASA NTRS2000

How do Polar Stratospheric Clouds Form?

SOLVE measurements have been compared with results from a microphysical model to understand the composition and formation of the polar stratospheric clouds (PSCs) observed during SOLVE. Evidence that the majority of the particles remain liquid throughout the winter will be presented. However, a small fraction of the particles do freeze, and the presence of these frozen particles can not be explained by current theories, in which the only freezing mechanism is homogeneous freezing to ice below the ice frost point. Alternative formation mechanisms, in particular homogeneous freezing above the ice frost point and heterogeneous freezing, have been explored using the microphysical model. Both nitric acid trihydrate (NAT) and nitric acid dihydrate (NAD) have been considered as possible compositions for the solid-phase nitric acid aerosols. Comparisons between the model results and the SOLVE measurements will be used to constrain the possible formation mechanisms. Other effects of these frozen particles will also be discussed, in particular denitrification.

Drdla, Katja↗
NASA NTRS1976

Storing Blood Cells

The National Cancer Institute worked with Goddard Space Flight Center to propose a solution to the blood-cell freezing problem. White blood cells and bone marrow are stored for future use by leukemia patients as a result of Goddard and Jet Propulsion Laboratory expertise in electronics and cryogenics. White blood cell and bone marrow bank established using freezing unit. Freezing unit monitors temperature of cells themselves. Thermocouple placed against polyethylene container relays temperature signals to an electronic system which controls small heaters located outside container. Heaters allow liquid nitrogen to circulate at constant temperature and maintain consistent freezing rate. Ability to freeze, store, and thaw white cells and bone marrow without damage is important in leukemia treatment.

Source record↗
NASA NTRS2023

A 1D Model for Nucleation of Ice From Aerosol Particles: An Application to a Mixed-Phase Arctic Stratus Cloud Layer

Mixed-phase clouds (MPCs) have been identified as significant contributors to uncertainties in climate projections, attributable to model representation of processes controlling the formation and loss of supercooled water droplets and ice particles from the atmosphere. Arctic MPCs are commonly widespread and long-lived, with sustained ice crystal formation processes that challenge current understanding. This study examines the ice-nucleating particle (INP) reservoir dynamics governing immersion-mode heterogeneous freezing in an observed case of Arctic MPCs using a simplified 1D aerosol-cloud model. The model setup includes prescribed dynamical forcings and thermodynamic profiles, and represents INPs as multicomponent and polydisperse particle size distributions. Diagnostic and prognostic approaches to immersion freezing parameterization are compared, including time-independent (singular) number- and surface area-based descriptions and a time-dependent description following classical nucleation theory (CNT). The choice of freezing parameterization defines the size of the INP reservoir. The CNT-based description yields an orders of magnitude larger INP reservoir than the singular parameterizations, which is the dominant factor for sustained ice crystal formation. The efficiency of the freezing process and cloud cooling are of secondary importance. A diagnostic treatment neglecting INP loss is only accurate when the INP reservoir size is large and INP depletion weak. Since a larger INP reservoir sustains ice crystal formation substantially longer, and ice water path scales with ice crystal concentrations for the conditions considered, resolving the source of differences in INP reservoir dynamics due to model implementation is a high priority for advancing climate model physics.

aerosol↗
NASA NTRS1977

Preliminary analysis of aircraft fuel systems for use with broadened specification jet fuels

An analytical study was conducted on the use of broadened specification hydrocarbon fuels in present day aircraft. A short range Boeing 727 mission and three long range Boeing 747 missions were used as basis of calculation for one-day-per-year extreme values of fuel loading, airport ambient and altitude ambient temperatures with various seasonal and climatic conditions. Four hypothetical fuels were selected; two high-vapor-pressure fuels with 35 kPa and 70 kPa RVP and two high-freezing-point fuels with -29 C and -18 C freezing points. In-flight fuel temperatures were predicted by Boeing's aircraft fuel tank thermal analyzer computer program. Boil-off rates were calculated for the high vapor pressure fuels and heating/insulation requirements for the high freezing point fuels were established. Possible minor and major heating system modifications were investigated with respect to heat output, performance and economic penalties for the high freezing point fuels.

Pasion, A. J.↗
NASA NTRS1978

Mechanisms of deterioration of nutrients

Methods for improving the quality of freeze-dried foods were investigated. Areas discussed include: (1) microstructure of freeze-dried systems, (2) structural changes in freeze-dried systems, (3) artificial food matrices, and (4) osmotic preconcentration to yield improved freeze-dried products.

Karel, M.↗
NASA NTRS1981

Experimental Study of Fuel Heating at Low Temperatures in a Wing Tank Model, Volume 1

Scale model fuel heating systems for use with aviation hydrocarbon fuel at low temperatures were investigated. The effectiveness of the heating systems in providing flowability and pumpability at extreme low temperature when some freezing of the fuel would otherwise occur is evaluated. The test tank simulated a section of an outer wing tank, and was chilled on the upper and lower surfaces. Turbine engine lubricating oil was heated, and recirculating fuel transferred the heat. Fuels included: a commercial Jet A; an intermediate freeze point distillate; a higher freeze point distillate blended according to Experimental Referee Broadened Specification guidelines; and a higher freeze point paraffinic distillate used in a preceding investigation. Each fuel was chilled to selected temperature to evaluate unpumpable solid formation (holdup). Tests simulating extreme cold weather flight, without heating, provided baseline fuel holdup data. Heating and recirculating fuel increased bulk temperature significantly; it had a relatively small effect on temperature near the bottom of the tank. Methods which increased penetration of heated fuel into the lower boundary layer improved the capability for reducing holdup.

Stockemer, F. J.↗