CST R9120-B 30x60 Media Pretreatment and Digestion Standard Development to Support Tank Closure Cesium Removal 1A (TCCR-1A) Operations
In support of continued operations of Savannah River Remediation’s (SRR) ion exchange process to remove radioactive cesium from Savannah River Site (SRS) dissolved saltcake, referred to as the Tank Closure Cesium Removal 1A process (TCCR-1A; containing the second set of at-tank ion exchange columns), SRNL was tasked with: 1) validating the field protocol planned for pretreating the crystalline silicotitanate (CST) ion exchange media to be used in the columns, 2) preparing CST media for use in in-tank batch contact testing, and 3) developing a digestion standard to verify complete CST dissolution prior to characterization following each in-tank batch contact test. A procedure (SRNL L29 Manual, ITS-0229) was developed previously in support of the TCCR Demonstration (which contained the first set of ion exchange columns) based on evaluations of a different CST production lot with a larger particle size range to document the protocol for pretreating CST utilizing conditions similar to what will be performed in the field.