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Influence of stress on corrosion behavior of refractory alloy in potassium, and corrosion mass transfer effects in stainless steel-niobium alloy-potassium system
Stress corrosion reflux capsule tests of niobium alloy in potassium
High temperature nickel and cobalt superalloys for turbojet engines
Relative erosion resistance of ablative materials for nozzle sections of storable-propellant rocket engine
NASA programs for composite space shuttle structures
Ceramic material systems are being considered for potential use as turbine blade tip gas path seals at temperatures up to 1370 1/4 C. Silicon carbide and silicon nitride structures were selected for study since an initial analysis of the problem gave these materials the greatest potential for development into a successful materials system. Segments of silicon nitride and silicon carbide materials over a range of densities, processed by various methods, a honeycomb structure of silicon nitride and ceramic blade tip inserts fabricated from both materials by hot pressing were tested singly and in combination. The evaluations included wear under simulated engine blade tip rub conditions, thermal stability, impact resistance, machinability, hot gas erosion and feasibility of fabrication into engine components. The silicon nitride honeycomb and low-density silicon carbide using a selected grain size distribution gave the most promising results as rub-tolerant shroud liners. Ceramic blade tip inserts made from hot-pressed silicon nitride gave excellent test results. Their behavior closely simulated metal tips. Wear was similar to that of metals but reduced by a factor of six.
The Task 1 (thirty-six-month) and Task 2 (twelve-month) exposure of composite materials to fuel and fluid environments are reported. Narmco T300/5209 (Task 1) shows no significant degradation. Slightly lower mechanical properties were obtained from fuel/water immersion exposure of this material. Kevlar 49/2544 (also Task 1) exhibits significant drop in short-beam shear when exposed to fuel/water immersion. Task 2 materials (T300/5208, Kevlar 49 fabric/5209, and Kevlar 49 fibers) have not shown any significant mechanical property degradation to date.
An overview of the fire toxicology program, its principal objectives and approach, is outlined. The laboratory methods of assessing pyrolysis product toxicity for two experiments are presented. The two experiments are: a comparison of test end points; and an evaluation of operant techniques. A third experiment is outlined for a comparison of full-scale and laboratory toxicity tests, with the purpose of determining animal survivability in full-scale tests. Future research plans are also outlined.
Forty-one material systems were evaluated for potential use in turbine blade tip seal applications at 1370 C. Both ceramic blade tip inserts and abradable ceramic tip shoes were tested. Hot gas erosion, impact resistance, thermal stability, and dynamic rub performance were the criteria used in rating the various materials. Silicon carbide and silicon nitride were used, both as blade tips and abradables. The blade tip inserts were fabricated by hot pressing while low density and honeycomb abradables were sintered or reaction bonded.
Work performed on the chemical system characterized by chrome sulfide, chrome selenide, lanthanum selenide, and lanthanum sulfide is described. Most materials within the chemical systems possess the requisites for attractive thermoelectric materials. The preparation of the alloys is discussed. Graphs show the Seebeck coefficient, electrical resistivity, and thermal conductivity of various materials within the chemical systems. The results of selected doping are included.
An attempt was made to improve methods for producing powder metallurgy aircraft gas turbine engine parts from the nickel base superalloy known as Rene 95. The parts produced were the high pressure turbine aft shaft for the CF6-50 engine and the stages 5 through 9 compressor disk forgings for the CFM56/F101 engines. A 50% cost reduction was achieved as compared to conventional cast and wrought processing practices. An integrated effort involving several powder producers and a major forging source were included.
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The periodic testing and evaluation of graphite/epoxy and Kevlar/epoxy material systems after subjecting test specimens to prolonged exposure to several laboratory-controlled environments deemed typical of normal aircraft operations is discussed. It is noted that specimen immersion in water or water-based fluids resulted in the greatest effect on the mechanical properties tested. Also, the environmental fluids showed a tendency to affect Kevlar/epoxy systems at an earlier exposure period than the graphite/epoxy systems. Results also indicate mechanical property strength retention generally being lower for the Kevlar/epoxy systems when compared to the corresponding graphite/epoxy systems in similar environments, after prolonged exposure.
The effect of temperature on the tension-tension fatigue life of the T300/5208 graphite/epoxy angle-ply laminate system was investigated in an effort to develop an acceptable and reliable method of accelerated loading. Typical S log sub 10 N curves were determined experimentally at 25 C, 75 C, and 115 C. The time-temperature superposition principle was employed to find the shift factors of uniaxial fatigue strength, and a general linear equation of S log sub 10 N for shifting purpose was established. The combined techniques of cyclic creep measurements and optical microscopy upon fatigue failure allow some assessment of the possible physical basis of S log 10 N curve shifting. Before fatigue, the laminates at all test temperatures and stress levels undergo a unique damage mechanism during fatigue loading. It is concluded that an accelerated loading method is feasible.
Project 3, the subject of this technical report, was structured toward the successful engine demonstration of an improved-efficiency, long-life, tip-seal system for turbine blades. The advanced tip-seal system was designed to maintain close operating clearances between turbine blade tips and turbine shrouds and, at the same time, be resistant to environmental effects including high-temperature oxidation, hot corrosion, and thermal cycling. The turbine blade tip comprised an environmentally resistant, activated-diffussion-bonded, monocrystal superalloy combined with a thin layer of aluminium oxide abrasive particles entrapped in an electroplated NiCr matrix. The project established the tip design and joint location, characterized the single-crystal tip alloy and abrasive tip treatment, and established the manufacturing and quality-control plans required to fully process the blades. A total of 171 blades were fully manufactured, and 100 were endurance and performance engine-tested.
The present conference on the mechanics of composites discusses microstructure's influence on particulate and short fiber composites' thermoelastic and transport properties, the elastoplastic deformation of composites, constitutive equations for viscoplastic composites, the plasticity and fatigue of metal matrix composites, laminate damping mechanisms, the micromechanical modeling of Kevlar/epoxy composites' time-dependent failure, the variational characterization of waves in composites, and computational methods for eigenvalue problems in composite design. Also discussed are the elastic response of laminates, elastic coupling nonlinear effects in unsymmetrical laminates, elasticity solutions for laminate problems having stress singularities, the mechanics of bimodular composite structures, the optimization of laminated plates and shells, NDE for laminates, the role of matrix cracking in the continuum constitutive behavior of a damaged composite ply, and the energy release rates of various microcracks in short fiber composites.
The results of the engine testing of Rene 150 Stage 1 high pressure turbine blades in CF6-50 core and fan engines are presented. The core engine test was conducted for 233 hours with a variety of test cycles, and the fan engine test was conducted for 1000 C cycles. Post-test analysis of the core engine test data confirmed the suitability of the Rene 150 HPT blade for fan engine testing. Post-test evaluation and analysis of the fan engine test blades included visual and dimensional inspection as well as metallographic examination of selected blades. The Rene 150 HPT blade met the target goal of this project by demonstrating increased metal temperature capability; however, the post-test analysis revealed several areas that would have to be addressed in designing a long-life Rene 150 CF6-50 HPT blade.
The properties of eleven alloys were investigated to select an improved bearing material for the High Pressure Oxygen Turbo Pump which delivers liquid oxygen to the Space Shuttle Main Engine. The alloys, selected through detailed literature analysis, X 405, MRC-2001, T440V, 14-4/6V, D-5, V-M Pyromet 350, Stellite 3, FerroTic CS-40, Tribaloy 800, WD-65, and CBS-600. The alloys were tested in hardness, corrosion resistance, wear resistance, fatigue resistance, and fracture toughness tests, and their performance was compared with the baseline 440C test alloy. As a result, five alloys were eliminated, leaving the remaining six (X 405, MRC-2001, T440V, 14-4/6V, D-5, and WD-65 to be evaluated in the next phase of NASA tests which will include fracture toughness, rolling contact fatigue, wear resistance, and corrosion resistance. From these, three alloys will be selected, which will be made into ninety bearings for subsequent testing.