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At least 253 records · Page 14

Coded-mask-based wavefront sensing technique for APS nanofocusing beamline diagnostics

Here, we extend our recently developed coded-mask wavefront sensing technique to enable single-shot measurements of nanofocused x-ray beams. This method accurately reconstructs the focal beam profile by backpropagating the wavefront measured downstream of the beam focus. To validate its performance, we benchmarked it against the conventional fluorescence wire scan method, successfully measuring ∼120 nm focal spots at the 28-ID-B beamline of the Advanced Photon Source using a polymeric compound refractive lens. The results highlight the effectiveness of coded-mask wavefront sensing for high-precision beam profiling and its application as a real-time wavefront monitoring tool.

Shi, Xianbo [Argonne National Laboratory (ANL), Ar↗

Radiation Shielding Analysis of Linac Extension Area in APS Using FLUKA and PHITS Monte Carlo Radiation Transport Codes

The Linac extension area tunnel can accept 300- to 500-MeV electrons for experiments. Radiations from various normal and accident beam loss scenarios were analyzed with the FLUKA and PHITS Monte Carlo radiation transport codes. In normal beam loss scenarios, the beam was dumped on the horizontal and vertical beam dumps, while the accident scenarios were horizontal and vertical mis-steered beams that can occur due to incorrect beam energy and magnet settings. The extent of beam deviation, which was established using particle tracking studies, was used to define the beam directions in the Monte Carlo transport calculations. Further, a mis-steered condition, where the beam was not intercepted by the dumps, was also analyzed. For the horizontal dump, the PHITS results above the berm were higher for neutrons and somewhat lower for photons, compared to the FLUKA results. Comparison of the secondary particle yields from FLUKA and PHITS from an Al block with dimensions comparable to what was used in the beam dumps showed a 40% higher neutron yield and a 10% lower photon yield. Finally, to ensure compliance with Argonne National Laboratory's shielding policy, the design of the horizontal beam dump was modified, and additional shielding was recommended.

FLUKA↗

Practices and Standards for Data and Processing at the APS

The handling of datasets at scientific user facilities is becoming progressively more challenging as advances in sources and detectors drive increasingly aggressive data acquisition rates. The ability to share and process these data depends on the ability of the originator of the data and the persons making use of that data to unequivocally agree on what these data mean. This understanding is driven by use of standardized data formats.

96 KNOWLEDGE MANAGEMENT AND PRESERVATION↗

Etched Silicon Planar CRL Optics for the High-Energy X-ray Diffraction Beamlines 11-ID-B and 11-ID-C at the APS

We report the focusing of high-energy X-rays is most commonly achieved by commercially available compound refractive lenses (CRL), which are added together in larger structures. There is a need for high-energy X-ray beamlines to enable focusing in only one dimension down to a few micrometers to study layered materials and thin films. High-energy X-rays above 50 keV require often 100 lenses or more, therefore it is more efficient to etch the complete arrays of lenses into a monolithic substrate like a silicon wafer. Custom lens arrays were fabricated for the high-energy x-ray beamlines 11-ID-B, and 11-ID-C at the Argonne National Laboratory. The fabrication required tuning parameters of the Bosch process to optimize the etching of deep vertical sidewalls at a reasonable speed without overheating. The beamline 11-ID-B is equipped with lens arrays of 85-110 lenses for 59 keV and 190-250 lenses for 87 keV photon energy, focusing the beam vertically below 5.0 µm at the sample positions between 1600 mm to 2100 mm. 11-ID-C has received arrays of 435 lenses that focus 106 keV X-rays to a vertical height of 2.0 µm at the sample position. In both cases, the flux density gain in the focal spot is larger than a factor of 20, relative to using slits to cut the beam size. The lens setup is permanently installed and can be moved in and out of the beam during the experiment without further alignment. The lenses have enabled operando diffraction studies on interfaces in batteries and the development of pair distribution function (PDF) analysis using grazing incidence geometry.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

Thermal Analysis of a Superconducting Undulator Cryostat for the APS Upgrade

The Advanced Photon Source Upgrade includes four 4.8-m-long superconducting undulator (SCU) cryostats, each containing two planar undulator NbTi magnets up to 1.9 m long. The cooling is provided by six cryocoolers arranged in three thermal circuits. The magnets are indirectly cooled with LHe penetrating through channels in the magnet cores. This 4 K circuit, which also includes a LHe tank, is cooled by five 4 K cryocooler 2nd stages. A beam vacuum, which is thermally isolated from the magnets, is cooled by one 10 K cryocooler 2nd stage. A thermal shield and warm parts of current leads are cooled by the 1st stages of all six cryocoolers. This paper presents an ANSYS-based thermal analysis of the new SCU cryostat including all thermal circuits. The benchmarked thermal conductance between the cryocooler cold heads and the LHe tank are used in the calculations as well as the measured cryocooler load lines. The model predicts temperatures in the system, total 4 K heat loads, and excess cooling power for various operational modes of the undulator.

Shiroyanagi, Y.↗

FAST $\mathrm{G}$ AP $\mathrm{F}$ ILL : efficient gap filling in metabolic networks

Genome-scale metabolic reconstructions summarize current knowledge about a target organism in a structured manner and as such highlight missing information. Such gaps can be filled algorithmically. Scalability limitations of available algorithms for gap filling hinder their application to compartmentalized reconstructions. We present fastGapFill, a computationally efficient tractable extension to the COBRA toolbox that permits the identification of candidate missing knowledge from a universal biochemical reaction database (e.g. Kyoto Encyclopedia of Genes and Genomes) for a given (compartmentalized) metabolic reconstruction. The stoichiometric consistency of the universal reaction database and of the metabolic reconstruction can be tested for permitting the computation of biologically more relevant solutions. We demonstrate the efficiency and scalability of fastGapFill on a range of metabolic reconstructions.

59 BASIC BIOLOGICAL SCIENCES↗

APS Data Management System

As the capabilities of modern X-ray detectors and acquisition technologies increase, so do the data rates and volumes produced at synchrotron beamlines. This brings into focus a number of challenges related to managing data at such facilities, including data transfer, near real-time data processing, automated processing pipelines, data storage, handling metadata and remote user access to data. The Advanced Photon Source Data Management System software is designed to help beamlines deal with these issues. Finally, this paper presents the system architecture and describes its components and functionality; the system's current usage is discussed, examples of its use have been provided and future development plans are outlined.

97 MATHEMATICS AND COMPUTING↗

Longitudinal Gradient Dipole Magnet Prototype for APS at ANL

We planned an upgrade of the Advanced Photon Source at Argonne National Laboratory (ANL). The main goal of the upgrade is to improve the storage ring performance based on more advanced optics. One of the key magnet system elements is bending dipole magnets having a field strength change along the electron beam path. Moreover, a prototype of one such longitudinal gradient dipole magnet has been designed, built, and measured in a collaborative effort of ANL and Fermilab. Our paper discusses various magnetic design options, the selected magnet design, and the fabrication technology. The prototype magnet has been measured by rotational coils, a stretched wire, and a Hall probe. Measurement results are discussed and compared with simulations.

43 PARTICLE ACCELERATORS↗

APS Science 2014

This report is an overview of all research performed by Argonne National Laboratory's Advanced Photon Source department in 2014.

Fenner, Richard B.↗

Recommendations on Implementing the Energy Conservation Building Code in Visakhapatnam, AP, India

Visakhapatnam can play an important role in improving energy efficiency in its buildings by implementing ECBC. This document seeks to capture stakeholder recommendations on a road map for implementation, which can help all market players plan for implementation. Visakhapatnam also has an opportunity to serve as a role model for other Smart Cities and cities in general in India. The road map and steps that VUDA adopts to implement ECBC can provide helpful examples to these other cities.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗

Plasma Sciences Exposition at APS-DPP

Plasma Sciences Expo provides an exhibition that focuses on interactive, hands-on informal science education for students at all levels, parents, teachers and the general public. DPP research students and scientists inform this audience of the wonders of science with a particular focus on fusion and plasma science. School groups attend 8:00 am to 2:00 pm and the public attends 6 to 8 pm.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Separation and Speciation of Mercury from Hanford 241-AP-107 Tank Waste Supernatant

Mercuric nitrate, Hg(NO 3 ) 2 , was introduced into the Hanford flowsheet when it was used to catalyze nitric acid dissolution of certain aluminum alloy fuels and to suppress radioiodine volatilization during nitric acid dissolution of short-cooled uranium metal fuel. Inventory estimates, based primarily on Hanford process-knowledge, suggest a total mercury inventory of 2,100 kg 1 in the Hanford Tank Farms. Aside from the obvious human exposure concerns via tank vapors, mercury species in the tank waste liquid and solid fraction pose risk to the implementation and execution of the River Protection Project mission due to mercury limits imposed under waste acceptance criteria, toxicity characteristic leaching procedure restrictions for secondary waste disposal, and air emission permits. Although there is currently no processing of tank waste at Hanford, waste processing is imminent and representative mercury inventory tracking will be important to anticipate and mitigate stack emissions and secondary liquid waste disposal issues like those experienced at the Savannah River Site.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗