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At least 235 records · Page 13
All sourcesNASA NTRSDOE OSTI
DOE OSTI2019

Assessment of Impacts of Dissolved Organic Matter and Dissolved Iron on the Performance of Amidoxime-Based Adsorbents for Seawater Uranium Extraction

Research on extraction of uranium from seawater has been active in recent years because this technology can provide an additional supply of uranium for nuclear fuel from a much larger uranium reservoir (the oceans) and the processes are more environment friendly. One critical challenge of the development of this technology is to make uranium adsorbents perform well not just in the oversimplified laboratory system (e.g. artificial seawater) but also in the complex real seawater matrix, which is comprised of many competing ions and natural organic substances. Here, we conducted a systematic study using a continuous-flow seawater flume system to assess the potential impacts of dissolved organic matter (DOM) and dissolved iron on the uranium uptake performance (including adsorbent reusability) of amidoxime-based adsorbents. In the 28-day exposure, the adsorbent exposed in dissolved Fe-spiked seawater (low DOM/high Fe) and humic acid-spiked seawater (high DOM/high Fe) showed lower uranium adsorption loadings (73% and 56% of adsorption loading, respectively) than the same adsorbent exposed in seawater without spiking (low DOM/low Fe). Interestingly, the uranium adsorption loading of the reused adsorbent (after uranium stripping by a mild bicarbonate elution) in the dissolved Fe-spiked seawater dropped substantially to only 24% of the loading in the unspiked clean seawater counterpart; while not much change was observed in the performance of adsorbent exposed to the humic acid-spiked seawater. From comparison of FTIR signatures of adsorbent before and after the seawater exposure, we found that the amidoxime ligands in the adsorbent exposed to dissolved Fe-spiked seawater had severer degradation than the adsorbents exposed to humic acid-spiked seawater and unspiked clean seawater. Notably, unlike the adsorbent exposed to dissolved Fe-spiked seawater, the adsorbent exposed to humic acid-spiked seawater didn’t adsorb elevated level of Fe compared to the adsorbent in the unspiked clean seawater. This suggests that the species of Fe in the humic acid-spiked seawater (primarily humic acid bound Fe) didn’t interact with amidoxime-based adsorbent; while the Fe species in the Fe-spiked seawater strongly interacted with adsorbent and caused significant degradation of amidoxime ligands. On the other hand, highly variable uranium adsorption loadings were observed in adsorbent in contact with humic acid-spiked seawater, but not in the adsorbents exposed to dissolved Fe-spiked seawater and seawater without spike. Our observations thus indicate that seawater receiving high inputs of DOM and dissolved Fe, such as coastal waters, is not ideal for efficient extraction of uranium.

Uranium, Seawater, amidoxime-based adsorbents, dis↗
DOE OSTI2017

Phonon linewidth due to electron-phonon interactions with strong forward scattering in FeSe thin films on oxide substrates

Here, the discovery of an enhanced superconducting transition temperature T c in monolayers of FeSe grown on several oxide substrates has opened a new route to high- T c superconductivity through interface engineering. One proposal for the origin of the observed enhancement is an electronphonon (e-ph) interaction across the interface that peaked at small momentum transfers. In this paper, we examine the implications of such a coupling on the phononic properties of the system. We show that a strong forward scattering leads to a sizable broadening of phonon lineshape, which may result in charge instabilities at long-wavelengths. However, we further find that the inclusion of Coulombic screening significantly reduces the phonon broadening. Our results show that one might not expect anomalously broad phonon linewidths in the FeSe interface systems, despite the fact that the e-ph interaction has a strong peak in the forward scattering (small q ) direction.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2016

Research in Lattice Gauge Theory and in the Phenomenology of Neutrinos and Dark Matter

Research in theoretical elementary particle physics was performed by the PI Yannick Meurice and co-PI Mary Hall Reno. New techniques designed for precision calculations of strong interaction physics were developed using the tensor renormalization group method. Large-scale Monte Carlo simulations with dynamical quarks were performed for candidate models for Higgs compositeness. Ab-initio lattice gauge theory calculations of semileptonic decays of B-mesons observed in collider experiments and relevant to test the validity of the standard model were performed with the Fermilab/MILC collaboration. The phenomenology of strong interaction physics was applied to new predictions for physics processes in accelerator physics experiments and to cosmic ray production and interactions. A research focus has been on heavy quark production and their decays to neutrinos. The heavy quark contributions to atmospheric neutrino and muon fluxes have been evaluated, as have the neutrino fluxes from accelerator beams incident on heavy targets. Results are applicable to current and future particle physics experiments and to astrophysical neutrino detectors such as the IceCube Neutrino Observatory.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2020

Epitaxial and Strong Support Interactions between Pt and LaFeO 3 Films Stabilize Pt Dispersion

The ability to stabilize very small Pt crystallites in supported-metal catalysts following harsh treatments is an important industrial problem. Herein, we demonstrate that Pt particles can be maintained in the 1- to 2-nm range following multiple oxidation and reduction cycles at 1073 K when the particles are supported on 0.5-nm LaFeO 3 films that have been deposited onto MgAl 2 O 4 using atomic layer deposition (ALD). Characterization by Scanning Transmission Electron Microscopy (STEM) suggest that, when the catalyst is oxidized at 1073 K, the Pt crystallites are oriented with respect to the underlying LaFeO 3 . X-Ray Absorption Spectroscopy (XAS) also shows evidence for changes in the Pt environment. CO-oxidation rates for the reduced catalyst remain unchanged after five redox cycles at 1073 K. Epitaxial growth of Pt clusters and the consequent strong metal-support interaction between Pt and LaFeO 3 are indicated to be prime reasons for the enhanced catalytic performances.

36 MATERIALS SCIENCE↗
DOE OSTI2014

Scientific/Technical Report

Measurements of the thermoelectric power of the dilute, strongly-interacting two-dimensional electron system in high-mobility, low-disorder silicon MOSFETs were obtained at low temperatures down to 0.2 K. With decreasing density n_s, the thermopower was found to exhibit a sharp increase by more than an order of magnitude, tending to a divergence at a finite, disorder-independent density n_t. The critical behavior of the thermopower observed in our experiments provides clear evidence for an interaction-induced quantum phase transition to a new phase at low density in a strongly interacting 2D electron system, thereby settling a 20-year debate.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2020

Strong QCD Insights from Excited Nucleon Structure Studies with CLAS and CLAS12

Studies of the spectrum of hadrons and their structure in experiments with electromagnetic probes offer unique insight into many facets of the strong interaction in the regime of large quark-gluon running coupling, i.e. the regime of strong QCD. The experimental program within Hall B at Jefferson Laboratory based on data acquired with the CLAS spectrometer using electron and photon beams with energies up to 6 GeV has already considerably extended the scope of research in hadron physics in joint efforts between experiment and phenomenological data analysis. Impressive progress in relating the hadron structure observables inferred from the data to the strong QCD mechanisms underlying hadron mass generation has been achieved in the past decade. Furthermore, these results will be considerably extended with data from the experimental program with the new CLAS12 spectrometer that has begun data taking using electron beams with energies up to 11 GeV. With this extended kinematic reach the structure of nucleon resonances will be probed at the highest photon virtualities ever achieved in the studies of exclusive electroproduction, which will allow for the exploration of the distance scale where>98% of light hadron mass emerges from QCD in the transition of the strong interaction from the regime of quark-gluon confinement to perturbative QCD.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2015

Dense electron-positron plasmas and gamma-ray bursts generation by counter-propagating quantum electrodynamics-strong laser interaction with solid targets

We use quantum electrodynamics (QED) particle-in-cell simulations to investigate and compare the generation of dense electron-positron plasmas and intense γ-ray bursts in the case of counter-propagating laser solid interaction (two-side irradiation) and single laser solid interaction (one-side irradiation). In the case of counter-propagating linearly polarized laser pulses irradiating a thin aluminum foil with each pulse peak power of 12.5 PW (I = 4 × 10{sup 23 }W/cm{sup 2}), we calculate that about 20% of the laser energy is converted into a burst of γ-rays with flux exceeding 10{sup 14 }s.{sup −1} This would be one of the most intense γ-ray sources among those currently available in laboratories. The γ-ray conversion efficiency in the case of two-side irradiation is three times higher than in the case of one-side irradiation using a single 12.5 PW laser. Dense electron-positron plasma with a maximum density of 6 × 10{sup 27 }m{sup −3} are generated simultaneously during the two-side irradiation which is eightfold denser compared to the one-side irradiation. The enhancement of the effects in the case of counter-propagating lasers are the results of the symmetrical compression of the foil target and the formation of electric potential and standing wave around the target. Realizing experimentally the proposed counter-propagating QED-strong laser-solid interaction to produce dense electron-positron pairs and prolific γ-rays will be made possible by the Extreme Light Infrastructure-Nuclear Physics facility under construction.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2014

Structural and magnetic characterization of La{sub 0.8}Sr{sub 0.2}MnO{sub 3} nanoparticles prepared via a facile microwave-assisted method

Nanoparticles of La{sub 0.8}Sr{sub 0.2}MnO{sub 3} (LSMO) with different particle sizes are synthesized by a very fast, inexpensive, reproducible, and environmentally friendly method: the microwave irradiation of the corresponding mixture of nitrates. The structural and magnetic properties of the samples are investigated by the X-Ray diffraction (XRD), Fourier transform infra-red (FT-IR) spectroscopy, field-emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), and magnetic (DC magnetization and AC susceptibility) measurements. The XRD study coupled with the Rietveld refinement show that all samples crystallize in a rhombohedral structure with the space group of R−3C. The FT-IR spectroscopy and FE-SEM images indicate formation of the perovskite structure of LSMO. The DC magnetization measurements confirm the decrease in the particle size effects on the magnetic properties, e.g. reduction in the ferromagnetic (FM) moment and increase in the surface spin disorder. Magnetic dynamics of the samples studied by AC magnetic susceptibility shows that the magnetic behavior of the nanometer-sized samples is well-described by the Vogel-Fulcher and critical slowing down laws. Strong interaction between magnetic nanoparticles of LSMO was detected by fitting the experimental data with the mentioned models. - Graphical abstract: Temperature dependence of the magnetization M(T) was measured in the zero-field-cooling (ZFC) and field-cooling (FC) modes at the applied magnetic field of 100 Oe for the La{sub 0.8}Sr{sub 0.2}MnO{sub 3} with different size prepared via a facile microwave-assisted method. - Highlights: • Nanoparticles of La{sub 0.8}Sr{sub 0.2}MnO{sub 3} were synthesized by the microwave irradiation process. • The structural studies show that all samples crystallize in a rhombohedral structure with space group of R−3C. • The DC magnetic studies confirm tuning of the magnetic properties due to the particle size effects. • Magnetic dynamic studied by AC magnetic susceptibility indicate strong interaction between magnetic nanoparticles.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2014

Energy density fluctuations in early universe

The primordial nucleosinthesys of the element can be influenced by the transitions of phase that take place after the Big Bang, such as the QCD transition. In order to study the effect of this phase transition, in this work we compute the time evolution of thermodynamical quantities of the early universe, focusing on temperature and energy density fluctuations, by solving the relevant equations of motion using as input the lattice QCD equation of state to describe the strongly interacting matter in the early universe plasma. We also study the effect of a primordial strong magnetic field by means of a phenomenological equation of state. Our results show that small inhomogeneities of strongly interacting matter in the early Universe are moderately damped during the crossover.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2015

Effect of the scrape-off layer in AORSA full wave simulations of fast wave minority, mid/high harmonic, and helicon heating regimes

Several experiments on different machines and in different fast wave (FW) heating regimes, such as hydrogen minority heating and high harmonic fast waves, have found strong interactions between radio-frequency (RF) waves and the scrape-off layer (SOL) region. This paper examines the propagation and the power loss in the SOL by using the full wave code AORSA, in which the edge plasma beyond the last closed flux surface (LCFS) is included in the solution domain and a collisional damping parameter is used as a proxy to represent the real, and most likely nonlinear, damping processes. 3D AORSA results for the National Spherical Torus eXperiment (NSTX), where a full antenna spectrum is reconstructed, are shown, confirming the same behavior found for a single toroidal mode results in Bertelli et al, Nucl. Fusion, 54 083004, 2014, namely, a strong transition to higher SOL power losses (driven by the RF field) when the FW cut-off is moved away from in front of the antenna by increasing the edge density. Additionally, full wave simulations have been extended to “conventional” tokamaks with higher aspect ratios, such as the DIII-D, Alcator C-Mod, and EAST devices. DIII-D results show similar behavior found in NSTX and NSTX-U, consistent with previous DIII-D experimental observations. In contrast, a different behavior has been found for Alcator C-Mod and EAST, which operate in the minority heating regime unlike NSTX/NSTX-U and DIII-D, which operate in the mid/high harmonic regime. A substantial discussion of some of the main aspects, such as (i) the pitch angle of the magnetic field; (ii) minority heating vs. mid/high harmonic regimes is presented showing the different behavior of the RF field in the SOL region for NSTX-U scenarios with different plasma current. Finally, the preliminary results of the impact of the SOL region on the evaluation of the helicon current drive efficiency in DIII-D is presented for the first time and briefly compared with the different regimes mentioned above.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2014

Keggin (K{sub 5}, H{sub 3}O)[SiV{sub 3}W{sub 9}O{sub 40}H]·xH{sub 2}O: Characterization and crystal structure

Single crystals of the potassium salt (K{sub 5}, H{sub 3}O)[SiV{sub 3}W{sub 9}O{sub 40}H]·xH{sub 2}O of the vanadium tri-substituted α-Keggin dodecatungstosilicate were prepared and analyzed by vibrational, EPR and {sup 51}V NMR spectroscopy. Varying the synthesis conditions allows crystallization of partially reduced anions. The crystal structure was determined for both oxidized (V{sup 5+}) and partially reduced (V{sup 4+/5+}) potassium salts. Single crystal X-ray diffraction data and solid state {sup 51}V-NMR spectra confirm the occurrence of a single vanadium site in a cubic structure due to rotational disorder of the Keggin ion. Partially reduced compounds crystallize within the same structure as fully oxidized ones. EPR experiments confirm strong interaction of V{sup 4+} with two V{sup 5+} ions, in accordance with insertion of a V{sub 3} subunit into the lacunary Keggin ion as designed in the synthesis method. The 3D-edifice is composed of K{sup +}/H{sub 2}O counter-sublattice with evidence of tunable water occupancy. - Graphical abstract: Relative arrangements of HPA clusters in (K{sub 5}, H{sub 3}O)[SiV{sub 3}W{sub 9}O{sub 40}]·xH{sub 2}O. - Highlights: • We prepared single crystals of the potassium salt (K{sub 5}, H{sub 3}O)[SiV{sub 3}W{sub 9}O{sub 40}H]·xH{sub 2}O. • The synthesis was designed to give the α-1,2,3-[SiV{sub 3}W{sub 9}O{sub 40}] Keggin ion. • Strict pH control was necessary to avoid vanadium partial reduction. • Reduced compounds crystallize within the same structure as fully oxidized ones. • EPR confirms strong interaction of V{sup 4+} with two V{sup 5+} ions in a V{sub 3} subunit.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2017

Electrodynamical forbiddance of a strong quadrupole interaction in surface enhanced optical processes. Experimental confirmation of the existence in fullerene C{sub 60}

It is demonstrated that in the SERS and SEIRA spectra of the fullerene C{sub 60}, the lines, which are forbidden in usual Raman and IR spectra and allowed in SERS and SEIRA, are absent. In addition the enhancement SERS coefficient in a single molecule detection regime is ~10{sup 8} instead of the value 10{sup 14}–10{sup 15}, characteristic for this phenomenon. These results are explained by the existence of so-called electrodynamical forbiddance of a strong quadrupole light-molecule interaction, which arises because of belonging of C{sup 60} to the icosahedral symmetry group and due to the electrodynamical law divE = 0.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2014

Physics with charmonium - Highlights of BESIII and PANDA

The physics of the strong interaction is undoubtedly one of the most challenging areas of modern science. Quantum ChromoDynamics (QCD) is reproducing successfully the physics phenomena at distances much shorter than the size of the nucleon, where perturbation theory can be used yielding results of high precision and predictive power. At larger distance scales, however, perturbative methods cannot be applied anymore, although spectacular phenomena, such as the generation of hadron masses and quark confinement, occur. Studies using charmed quarks and gluon-rich matter have the potential to connect the perturbative and the non-perturbative QCD region. The annihilation of matter with antimatter in the mass regime of charmonium is an ideal environment to discover new states or transitions that could reveal the secrets of the strong interaction. Hadronic and electromagnetic transitions between charmonium states and their decays have been measured with a world-record in precision with the BESIII spectrometer at the electron-positron collider at IHEP Beijing, China. Moreover, unconventional narrow charmonium-rich states have been discovered recently in an energy regime above the open-charm threshold, thereby, possibly initiating a new era in charmonium spectroscopy. The near future experiment, PANDA, at the research facility FAIR in Germany, Darmstadt, will exploit the annihilation of cooled anti-protons with protons to perform charmonium spectroscopy with an incredible precision. I will present the most promising results that have been recently obtained with BESIII together with the future perspectives of PANDA in the field of charmonium spectroscopy.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2015

WIMP and SIMP dark matter from the spontaneous breaking of a global group

We propose and study a scalar extension of the Standard Model which respects a ℤ{sub 3} symmetry remnant of the spontaneous breaking of a global U(1){sub DM} symmetry. Consequently, this model has a natural dark matter candidate and a Goldstone boson in the physical spectrum. In addition, the Higgs boson properties are changed with respect to the Standard Model due to the mixing with a new particle. We explore regions in the parameter space taking into account bounds from the measured Higgs properties, dark matter direct detection as well as measurements of the effective number of neutrino species before recombination. The dark matter relic density is determined by three classes of processes: the usual self-annihilation, semi-annihilation and purely dark matter 3→2 processes. The latter has been subject of recent interest leading to the so-called ‘Strongly Interacting Massive Particle’ (SIMP) scenario. We show under which conditions our model can lead to a concrete realization of such scenario and study the possibility that the dark matter self-interactions could address the small scale structure problems. In particular, we find that in order for the SIMP scenario to work, the dark matter mass must be in the range 7−115 MeV, with the global symmetry energy breaking scale in the TeV range.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2016

Strong coupling of plasmon and nanocavity modes for dual-band, near-perfect absorbers and ultrathin photovoltaics

In this study, when optical resonances interact strongly, hybridized modes are formed with mixed properties inherited from the basic modes. Strong coupling therefore tends to equalize properties such as damping and oscillator strength of the spectrally separate resonance modes. This effect is here shown to be very useful for the realization of near-perfect dual-band absorption with ultrathin (~10 nm) layers in a simple geometry. Absorber layers are constructed by atomic layer deposition of the heavy-damping semiconductor tin monosulfide (SnS) onto a two-dimensional gold nanodot array. In combination with a thin (55 nm) SiO 2 spacer layer and a highly reflective Al film on the back, a semiopen nanocavity is formed. The SnS-coated array supports a localized surface plasmon resonance in the vicinity of the lowest order antisymmetric Fabry–Perot resonance of the nanocavity. Very strong coupling of the two resonances is evident through anticrossing behavior with a minimum peak splitting of 400 meV, amounting to 24% of the plasmon resonance energy. The mode equalization resulting from this strong interaction enables simultaneous optical impedance matching of the system at both resonances and thereby two near-perfect absorption peaks, which together cover a broad spectral range. When paired with the heavy damping from SnS band-to-band transitions, this further enables approximately 60% of normal incident solar photons with energies exceeding the band gap to be absorbed in the 10 nm SnS coating. Thereby, these results establish a distinct relevance of strong coupling phenomena to efficient, nanoscale photovoltaic absorbers and more generally for fulfilling a specific optical condition at multiple spectral positions.

77 NANOSCIENCE AND NANOTECHNOLOGY↗
DOE OSTI2021

Revealing the structure of light pseudoscalar mesons at the electron–ion collider

The questions of how the bulk of the Universe's visible mass emerges and how it is manifest in the existence and properties of hadrons are profound, and probe the heart of strongly interacting matter. Paradoxically, the lightest pseudoscalar mesons appear to be key to a further understanding of the emergent mass and structure mechanisms. These mesons, namely, the pion and kaon, are the Nambu-Goldstone boson modes of quantum chromodynamics (QCD). Unravelling their partonic structure and the interplay between emergent and Higgs-boson mass mechanisms is a common goal of three interdependent approaches - continuum QCD phenomenology, lattice-regularised QCD, and the global analysis of parton distributions - linked to experimental measurements of hadron structure. Experimentally, the anticipated electron-ion collider will enable a revolution in our ability to study pion and kaon structures, accessed by scattering from the 'meson cloud' of the proton through the Sullivan process. With the goal of enabling a suite of measurements that can address these questions, we examine key reactions that identify the critical detector-system requirements needed to map tagged pion and kaon cross-sections over a wide range of kinematics. The excellent prospects for extracting pion structural, functional, and form-factor data are outlined, and similar prospects for kaon structures are discussed in the context of a worldwide programme. Finally, the successful completion of the programme outlined herein will deliver deep, far-reaching insights into the emergence of pions and kaons, their properties, and their role as QCD's Goldstone boson modes.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗
DOE OSTI2015

Alpha channeling with high-field launch of lower hybrid waves

Although lower hybrid waves are effective at driving currents in present-day tokamaks, they are expected to interact strongly with high-energy particles in extrapolating to reactors. In the presence of a radial alpha particle birth gradient, this interaction can take the form of wave amplification rather than damping. While it is known that this amplification more easily occurs when launching from the tokamak high-field side, the extent of this amplification has not been made quantitative. Here, by tracing rays launched from the high-field-side of a tokamak, the required radial gradients to achieve amplification are calculated for a temperature and density regime consistent with a hot-ion-mode fusion reactor. These simulations, while valid only in the linear regime of wave amplification, nonetheless illustrate the possibilities for wave amplification using high-field launch of the lower hybrid wave.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2014

Preparation of graphene-Fe{sub 3}O{sub 4} nanocomposites using Fe{sup 3+} ion-containing magnetic ionic liquid

Graphene-Fe{sub 3}O{sub 4} (GN-Fe{sub 3}O{sub 4}) magnetic nanocomposites were prepared, GN-coated magnetic ionic liquid (MIL) as its precursors, which were used as both a magnetic resource and solvent. The method has proved to be valuable for the Fe{sub 3}O{sub 4} nanoparticles (NPs) well dispersed in the solution through strong interactions with GN, which are of interest because of their stability and chemical properties. In the process, strong interactions creates a condition for uniform dispersion in GN and [BMIm]FeCl{sub 4} (MIL) solution, and accelerate the formation of Fe{sub 3}O{sub 4} NPs. A transmission electron microscopy image has shown that the as-formed Fe{sub 3}O{sub 4} NPs with a diameter as small as 5–7 nm were deposited on GN sheets. Furthermore, the final material showed a superior properties than conventional method, which can be ascribed to the fact that [BMIm]FeCl{sub 4} plays a vital role in the process of producing small NPs size.

36 MATERIALS SCIENCE↗