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At least 235 records · Page 13

Thermal conductivity and dielectric constant of silicate materials

Report on the thermal conductivity and dielectric constant of nonmetallic materials evaluates the mechanisms of heat transfer in evacuated silicate powders and establishes the complex dielectric constant of these materials. Experimental measurements and results are related to postulated lunar surface materials.

Simon, I.↗

Arc Jet Testing of 3D Mid-Density Carbon Phenolic (3MDCP) for Mars Sample Return

When accounting for the highest-heating trajectory with margin, dispersion, and greatest system mass, MSR-EES is predicted to experience the highest heat flux and pressure (approximately 3300 W/cm2 hot-wall, 200 kPa) of any earth entry vehicle todate. To verify performance requirements are met by the forebody TPS, the material must be tested to validate model predictions and give confidence to stakeholder’s expectation of performance. 3D Mid-Density Carbon Phenolic (3MDCP) is NASA’s baseline material for the forebody heatshield of the MSR-EES. As part of the arc jet campaign to evaluate material performance, recent testing has completed in the Interaction Heating Facility (IHF) using a new facility setting to achieve the necessary environments.

arcjet↗

ENDF/B-VIII.1: Photonuclear Sublibrary

The photonuclear sublibrary aims to describe nuclear reactions between incident gamma particles and different nuclei. For ENDF/B-VIII.1, we adopted around 200 evaluations from the IAEA Coordinated Research Project (CRP) on photonuclear data while, for a few select mission-critical materials, evaluations from ENDF/B-VIII.0 were maintained. Additionally, many fixes to many files were implemented. Finally, ENDF/B-VIII.1 includes a new photonuclear file, 242 Pu, which was adopted from JENDL-5.0.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

Evaluation available encapsulation materials for low-cost long-life silicon photovoltaic arrays

Experimental evaluation of selected encapsulation designs and materials based on an earlier study which have potential for use in low cost, long-life photovoltaic arrays are reported. The performance of candidate materials and encapsulated cells were evaluated principally for three types of encapsulation designs based on their potentially low materials and processing costs: (1) polymeric coatings, transparent conformal coatings over the cell with a structural-support substrate; (2) polymeric film lamination, cells laminated between two films or sheets of polymeric materials; and (3) glass-covered systems, cells adhesively bonded to a glass cover (superstrate) with a polymeric pottant and a glass or other substrate material. Several other design types, including those utilizing polymer sheet and pottant materials, were also included in the investigation.

Carmichael, D. C.↗

Impact of divertor material on neutral recycling and discharge fueling in DIII-D

We report that experiments with the lower divertor of DIII-D during the Metal Rings Campaign (MRC) show that the fraction F of atomic D in the total recycling flux is material-dependent and varies through the ELM cycle, which may affect divertor fueling. Between ELMs, F C ~ 10% and FW ~ 40%, consistent with expectations if all atomic recycling is due to reflections. During ELMs, F C increases to 50% and F W to 60%. In contrast, the total D recycling coefficient including atoms and molecules R stays close to unity near the strike point where the surface is saturated with D. During ELMs, R can deviate from unity, increasing during high energy ELM-ion deposition (net D release) and decreasing at the end of the ELM which leads to ability of the target to trap the ELM-deposited D. The increase of R > 1 in response to an increase in ion impact energy Ei has been studied with small divertor target samples using Divertor Materials Evaluation System (DiMES). An electrostatic bias was applied to DiMES to change E i by 90 eV. On all studied materials including C, Mo, uncoated and W-coated TZM (>99% Mo, Ti, and Zr alloy), W, and W fuzz, an increase of E i transiently increased the D yield (and R) by ~10%. On C there was also an increase in the molecular D 2 yield, probably due to ion-induced D 2 desorption. Despite the measured increase in F on W compared to C, attached H-mode shots with OSP on W during MRC did not demonstrate a higher pedestal density. About 8% increase in the edge density could be seen only in attached L-mode scenarios. The difference can be explained by higher D trapping in the divertor and lower divertor fueling efficiency in H- versus L-mode.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

A computer program incorporating fatigue and fracture criteria in the preliminary design of transport aircraft: An evaluation

The APAS program a multistation structural synthesis procedure developed to evaluate material, geometry, and configuration with various design criteria usually considered for the primary structure of transport aircraft is described and evaluated. Recommendations to improve accuracy and extend the capabilities of the APAS program are given. Flow diagrams are included.

Berger, P. E.↗

InSight's Reconstructed Aerothermal Environments

The InSight Mars Lander successfully landed on the surface on November 26, 2018. This poster will describe the methodologies and margins used in developing the aerothermal environments for design of the thermal protection systems (TPS), as well as a prediction of as-flown environments based on the best estimated trajectory. The InSight mission spacecraft design approach included the effects of radiant heat flux to the aft body from the wake for the first time on a US Mars Mission, due to overwhelming evidence in ground testing for the European ExoMars mission (2009/2010) [1] and 2010 tests in the Electric Arc Shock Tube (EAST) facility [2]. The radiant energy on an aftbody was also recently confirmed via measurement on the Schiaparelli mission [3]. In addition, the InSight mission expected to enter the Mars atmosphere during the dust storm season, so the heatshield TPS was designed to accommodate the extra recession due to the potential dust impact. This poster will compare the predicted aerothermal environments using the reconstructed best estimated trajectory to the design environments. Design Approach: The InSight spacecraft was planned to be a near-design-to-print copy of the Phoenix spacecraft. The determination of the heatshield TPS requirements was approached as if it was a new design due to the new requirement of flying through a dust storm. The baseline for aftbody was build-to-print, and all analyses focused on ensuring adequate margin. This proved to be a challenge because the Phoenix aftbody was designed to withstand only convective heating and the InSight aftbody was evaluated for both convective and radiative heating. Aerothermal environments were predicted using the Langley Aerothermodynamic Upwind Relaxation Algorithm (LAURA) and the Data Parallel Line Relaxation (DPLR) CFD codes, and the Nonequilibrium Radiative Transport and Spectra Program (NEQAIR) utilizing bounding design trajectories derived from Monte Carlo analyses from the Program to Optimize Simulated Trajectories II (POST2). In all cases, super-catalytic flowfields were assigned to ensure the most conservative heating results. Two trajectories were evaluated: 1) the trajectory with the maximum heat flux was utilized to determine the flowfield characteristics and the viability of the selection of TPS materials; and 2) the trajectory with the maximum heat load was used to determine the required thicknesses of the TPS materials. Evaluation of the MEDLI data [4], along with ground test data [5] led to the determination of whether or not the flow would transition from laminar to turbulent on the heatshield, which also determined the TPS sizing location for the heatshield. Aerothermal margins were added for the convective heating and developed for the radiative heating. TPS material sizing was determined with the Reaction Kinetic Ablation Program (REKAP) and the Fully Implicit Ablation and Thermal Analysis program (FIAT) using a three-branched approach to account for aerothermal, material response, and material properties uncertainties. In addition, the heatshield recession was augmented by an analysis of the effect of entry through a potential dusty atmosphere using a methodology developed in References [6] and [7]. These analyses resulted in an increase to the Phoenix heatshield TPS thickness. Reconstruction Efforts: Once the best estimated trajectory is reconstructed by the team, the LAURA/HARA (High-Temperature Aerothermo-dynamic Radiation model) and DPLR/NEQAIR code pairs will be used to predict the as-flown aerothermal conditions. In these runs, fully-catalytic flowfields will be assigned because it is a more physically accurate description of the chemistry in the flow. Once again, determination of the onset of turbulence on the heatshield will be evaluated. The as-flown aerothermal environments will then be compared to the design environments.

Beck, R. A.↗

The Effect of Material Properties on Oxygen Evolution Activity and Assessing Half-Cell Screening as a Predictive Tool in Electrolysis

Iridium-based oxygen evolution catalysts are screened in this study for activity and stability with rotating disk electrode (RDE) half-cells. This study focuses on the electrochemical and materials approaches needed to characterize oxygen evolution catalysts, and include testing for activity, stability, composition, oxide content, and structure. Findings also discuss recommendations for data interpretation and detail the difficulties of comparing catalysts across materials sets with different elemental and oxide compositions, and linking RDE activity to device-level performance. The materials evaluated are a mixture of oxides and metals, and several methods are used to quantify metal content, qualitatively assess oxide content, and determine total surface area. Oxygen evolution activities and stabilities are compared, where a wide range of results are reported. In general, higher RDE performances are found for catalysts that contained larger amounts of ruthenium and metals. Higher durability, however, is found for catalysts that only contained iridium and a higher proportion of oxides. Additionally, catalysts are evaluated for performance in membrane electrode assemblies to assess RDE as a predictive tool in electrolysis. While activity trends within individual material sets generally held between ex- and in-situ testing, RDE tends to overestimate the activity of more metallic catalysts when compared to device-level performance. These results stress the need for multiple metal/oxide baselines for mixed catalysts, to better project in-situ kinetics.

36 MATERIALS SCIENCE↗

NASA-STD-6001B Test 1 Upward Flame Propagation; Sample Length Impact on MOC Investigation

Understanding the combustion behavior of materials in the elevated oxygen environments of habitable spacecraft is of utmost importance to crew safety and mission success. Currently, certification for unrestricted flight usage of a material with respect to flammability involves passing the Upward Flame Propagation Test of NASA-STD-6001B (Test 1). This test evaluates materials in a standardized test configuration for two failure criteria: self-extinguishment within 15 cm (6 in.) and the propensity of flame propagation by means of flaming material transfer. By the NASA standard, full-length samples are 30 cm (12 in.) in length; however, factors independent of the test method such as limited material availability or various nonstandard test configurations limit the full pretest sample lengths available for test. This paper characterizes the dependence, if any, of pretest sample length on NASA-STD-6001B Test 1 results. Testing was performed using the Maximum Oxygen Concentration (MOC) Threshold Method to obtain a data set for each sample length tested. In addition, various material types, including cloth (Nomex), foam (TA-301) and solids (Ultem), were tested to investigate potential effects of test specimen types. Though additional data needs to be generated to provide statistical confidence, preliminary findings are that use of variable sample lengths has minimal impact on NASA-STD-6001B flammability performance and MOC determination.

Harper, Susana Tapia↗

Non-destructive evaluation of composite materials using ultrasound

Investigation of the nondestructive evaluation of advanced composite-laminates is summarized. Indices derived from the measurement of fundamental acoustic parameters are used in order to quantitatively estimate the local material properties of the laminate. The following sections describe ongoing studies of phase insensitive attenuation measurements, and discuss several phenomena which influences the previously reported technique of polar backscatter. A simple and effective programmable gate circuit designed for use in estimating attenuation from backscatter is described.

Miller, J. G.↗

Thick film silicon growth techniques

One inch wide silicon ribbons up to 14 inches long have been produced from graphite dies. Several different techniques have been employed to improve the semiconductor purity of silicon. This has resulted in a general increase in quality although the techniques involved have not been optimized. The power factor of uncoated ribbon solar cells produced for material evaluation has increased to approximately 75% of those evaluation cells made from commercial silicon. The present limitation is believed due to low lifetime. Additional work has continued with new die materials; however, only composite dies of SiO2 and C show significant potential at this time.

Bates, H. E.↗

Molten Salt Reactors: What about Materials? An Overview and Future Needs

ORNL Molten Salt Reactor Experiment (MSRE) – 60’s- early 70’s Developed INOR-8 (aka Hastelloy N); MSRE operated over the period Dec 1965 to 1969. (not continuous); Operated for >13,000 hr at T from ~550 to ~650°C using U, Li-7, Be and Zr fluoride salt fuel; Post-Irradiation Material Evaluation (corrosion + neutron irradiation) of surveillance specimens; Noted ”beneficial effect of Nb” in alloy (on intergranular Te embrittlement) More recent (post-1980) Materials R&D for Gen IV …. Alloys 316L, 316H, 304, Alloy 800H, Alloy 617 (!!), Hastelloy N (mod), plus numerous experimental alloys developed

36 - MATERIALS SCIENCE↗

CARES/Life Ceramics Durability Evaluation Software Used for Mars Microprobe Aeroshell

The CARES/Life computer program, which was developed at the NASA Lewis Research Center, predicts the probability of a monolithic ceramic component's failure as a function of time in service. The program has many features and options for materials evaluation and component design. It couples commercial finite element programs-which resolve a component's temperature and stress distribution-to-reliability evaluation and fracture mechanics routines for modeling strength-limiting defects. These routines are based on calculations of the probabilistic nature of the brittle material's strength. The capability, flexibility, and uniqueness of CARES/Life has attracted many users representing a broad range of interests and has resulted in numerous awards for technological achievements and technology transfer.

Nemeth, Noel N.↗