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All sources NASA NTRS DOE OSTI

DOE OSTI2024

A Method for Dynamic Kolsky Bar Compression at High Temperatures: Application to Ti-6Al-4V

Abstract An experimental apparatus for measuring the dynamic behavior of materials subjected to strain rates on the order of 10 $$^3$$ 3 s $$^{-1}$$ - 1 and temperatures up to 800°C with a unique triple actuation system is developed in this work. This system is based on the traditional Kolsky (or split-Hopkinson pressure) bar design, with the addition of an external furnace used to heat the specimen to the desired temperature. A synchronized triple pneumatic actuation system is used to control the motion and timing of the the sample, incident, and transmitted bars. The cold contact time (CCT), or the time during which the heated sample is in contact with the room temperature bars before compression, is measured experimentally and carefully controlled to minimize the development of a temperature gradient across the sample and avoid heating of the bars. Experiments are performed in conjunction with ultra high speed imaging and 2D digital image correlation (DIC), as well as high speed thermal imaging. To verify the viability of the proposed system, experiments were conducted on Ti-6Al-4V (wt.%) at temperatures from 25°C up to and 800°C at an average strain rate of approximately 1200 s $$^{-1}$$ - 1 .

36 MATERIALS SCIENCE↗

NASA NTRS1990

Characteristics of the GOES I-M Imager and Sounder

The design and the parameters of the improved thermal-imaging and sounding instruments (the Imager and the Sounder) that will be part of the instrument complements of the next-generation Geostationary Operational Environmental Satellite (GOES I-M) are discussed. The new design incorporates many features that enhance instrumental reliability over the previous GOES radiometric instruments, such as independently functioning Sounder and Imager, redundancy, and more reliable position sensors and lubrication methods. Tables are presented which list the instrument parameters of the GOES I-M Imager and Sounder and the performance characteristics of the two instruments.

Ernst, Thomas J.↗

NASA NTRS1998

Automation of the Image Analysis for Thermographic Inspection

Several data processing procedures for the pulse thermal inspection require preliminary determination of an unflawed region. Typically, an initial analysis of the thermal images is performed by an operator to determine the locations of unflawed and the defective areas. In the present work an algorithm is developed for automatically determining a reference point corresponding to an unflawed region. Results are obtained for defects which are arbitrarily located in the inspection region. A comparison is presented of the distributions of derived values with right and wrong localization of the reference point. Different algorithms of automatic determination of the reference point are compared.

Plotnikov, Yuri A.↗

NASA NTRS1993

Ground truth spectrometry and imagery of eruption clouds to maximize utility of satellite imagery

Field experiments with thermal imaging infrared radiometers were performed and a laboratory system was designed for controlled study of simulated ash clouds. Using AVHRR (Advanced Very High Resolution Radiometer) thermal infrared bands 4 and 5, a radiative transfer method was developed to retrieve particle sizes, optical depth and particle mass involcanic clouds. A model was developed for measuring the same parameters using TIMS (Thermal Infrared Multispectral Scanner), MODIS (Moderate Resolution Imaging Spectrometer), and ASTER (Advanced Spaceborne Thermal Emission and Reflection Radiometer). Related publications are attached.

Rose, William I.↗

DOE OSTI2021

Multiscale Characterization of Photovoltaic Modules—Case Studies of Contact and Interconnect Degradation

The current popularity of photovoltaic (PV) systems is due in large part to their exceptional reliability and significantly lower cost than other energy sources. Studying cell and module degradation is key to promote further development in the state of the art. Fielded or accelerated aged modules exhibit different failure modes, of which metallization degradation (contacts and interconnections) is prevalent. In this work, we discuss how multiscale characterization methods can be applied to a variety of module technologies that have been field exposed and have undergone accelerated age testing. These methods include performing characterization on the module level, cell level, and finally the materials level. The observed performance losses from the module- and cell-level characterization can be correlated with materials properties to find out the root cause of degradation. We recommend an initial nondestructive characterization suite, including module- and cell-level current-voltage ( I--V ), Suns-V OC , photoluminescence and electroluminescence imaging, quantum efficiency, ultraviolet fluorescence imaging, and thermal infrared imaging. Samples are then extracted from particularly degraded regions of the module and prepared for materials characterization techniques, such as top-down and cross-sectional scanning electron microscopy, energy-dispersive X-ray spectroscopy, X-ray photoelectron spectroscopy, secondary ion mass spectrometry, Raman spectroscopy, and transmission electron microscopy, allowing a deeper look into the mechanism behind the metallization degradation. This article serves as an instructional review to introduce the different multiscale characterization methods and how they can be effectively applied to perform PV degradation studies. Furthermore, we also share some of our examples and discuss the strengths, limitations, and best practices for each of the characterization techniques.

14 SOLAR ENERGY↗

DOE OSTI2023

Enhancing Crystallization in Hybrid Perovskite Solar Cells Using Thermally Conductive 2D Boron Nitride Nanosheet Additive

Controlling crystallization and grain growth is crucial for realizing highly efficient hybrid perovskite solar cells (PSCs). In this work, enhanced PSC photovoltaic performance and stability by accelerating perovskite crystallization and grain growth via 2D hexagonal boron nitride (hBN) nanosheet additives incorporated into the active perovskite layer are demonstrated. Specifically, in situ X-ray scattering and infrared thermal imaging during the perovskite annealing process revealed the highly thermally conductive hBN nanosheets promoted the phase conversion and grain growth in the perovskite layer by facilitating a more rapid and spatially uniform temperature rise within the perovskite film. Complementary structural, physicochemical, and electrical characterizations further showed that the hBN nanosheets formed a physical barrier at the perovskite grain boundaries and the interfaces with charge transport layers, passivating defects, and retarding ion migration. As a result, the power conversion efficiency of the PSC is improved from 17.4% to 19.8%, along with enhanced device stability, retaining ≈90% of the initial efficiency even after 500 h ambient air storage. Here, the results not only highlight 2D hBN as an effective additive for PSCs but also suggest enhanced thermal transport as one of the pathways for improved PSC performance by 2D material additives in general.

2D materials↗

NASA NTRS1981

Estimation of surface temperature variations due to changes in sky and solar flux with elevation

The magnitude of elevation effects due to changes in solar and sky fluxes, on interpretation of single thermal images and composite products such as temperature difference and thermal inertia, are examined. Simple expressions are derived for the diurnal behavior of the two parameters, by fitting field observations in one tropic (Hawaii) and two semi-arid climates (Wyoming and Colorado) (Hummer-Miller, 1981). It is shown that flux variations with elevation can cause changes in the mean diurnal temperature gradient from -4 to -14 degrees C/km, evaluated at 2000 m. Changes in the temperature-difference gradient of 1 to 2 degrees C/km are also produced which is equivalent to an effective thermal-inertia gradient of 100 W s(exp 1/2)/sq m-K-km. An example is presented showing an elevation effect of 12 degrees C on the day and night thermal scenes of a test site in Arizona.

Hummer-Miller, S.↗

NASA NTRS1993

Evolution of miniature detectors and focal plane arrays for infrared sensors

Sensors that are sensitive in the infrared spectral region have been under continuous development since the WW2 era. A quest for the military advantage of 'seeing in the dark' has pushed thermal imaging technology toward high spatial and temporal resolution for night vision equipment, fire control, search track, and seeker 'homing' guidance sensing devices. Similarly, scientific applications have pushed spectral resolution for chemical analysis, remote sensing of earth resources, and astronomical exploration applications. As a result of these developments, focal plane arrays (FPA) are now available with sufficient sensitivity for both high spatial and narrow bandwidth spectral resolution imaging over large fields of view. Such devices combined with emerging opto-electronic developments in integrated FPA data processing techniques can yield miniature sensors capable of imaging reflected sunlight in the near IR and emitted thermal energy in the Mid-wave (MWIR) and longwave (LWIR) IR spectral regions. Robotic space sensors equipped with advanced versions of these FPA's will provide high resolution 'pictures' of their surroundings, perform remote analysis of solid, liquid, and gas matter, or selectively look for 'signatures' of specific objects. Evolutionary trends and projections of future low power micro detector FPA developments for day/night operation or use in adverse viewing conditions are presented in the following test.

Watts, Louis A.↗

NASA NTRS1995

Chromatic Image Analysis For Quantitative Thermal Mapping

Chromatic image analysis system (CIAS) developed for use in noncontact measurements of temperatures on aerothermodynamic models in hypersonic wind tunnels. Based on concept of temperature coupled to shift in color spectrum for optical measurement. Video camera images fluorescence emitted by phosphor-coated model at two wavelengths. Temperature map of model then computed from relative brightnesses in video images of model at those wavelengths. Eliminates need for intrusive, time-consuming, contact temperature measurements by gauges, making it possible to map temperatures on complex surfaces in timely manner and at reduced cost.

Buck, Gregory M.↗

DOE OSTI2021

Pyroelectric thin films—Past, present, and future

Pyroelectrics are a material class that undergoes a change in polarization as the temperature of the system is varied. This effect can be utilized for applications ranging from thermal imaging and sensing to waste-heat energy conversion to thermally driven electron emission. Here, we review recent advances in the study and utilization of thin-film pyroelectrics. Leveraging advances in modeling, synthesis, and characterization has provided a pathway forward in one of the more poorly developed subfields of ferroelectricity. We introduce the complex physical phenomena of pyroelectricity, briefly explore the history of work in this space, and highlight not only new advances in the direct measurement of such effects but also how our ability to control thin-film materials is changing our understanding of this response. Finally, we discuss recent advances in thin-film pyroelectric devices and introduce a number of potentially new directions the field may follow in the coming years.

36 MATERIALS SCIENCE↗

NASA NTRS1991

Optical data storage and metallization of polymers

The utilization of polymers as media for optical data storage offers many potential benefits and consequently has been widely explored. New developments in thermal imaging are described, wherein high resolution lithography is accomplished without thermal smearing. The emphasis was on the use of poly(ethylene terephthalate) film, which simultaneously serves as both the substrate and the data storage medium. Both physical and chemical changes can be induced by the application of heat and, thereby, serve as a mechanism for high resolution optical data storage in polymers. The extension of the technique to obtain high resolution selective metallization of poly(ethylene terephthalate) is also described.

Roland, C. M.↗

NASA NTRS2018

Multi-Angle Imager for Aerosols Thermal Control System

The Multi-Angle Imager for Aerosols (MAIA) Thermal Control System is a NASA funded instrument that will collect data to help characterize airborne particulate matter over a number of population centers across the globe using multi-angle spectropolarimetric imagery. The data collected by MAIA will facilitate assessments of the impacts of different types of particulate matter on adverse health outcomes. MAIA is a hosted payload meant to operate in a near-circular sun-synchronous polar orbit, with a mean altitude between 600 km and 850 km. The nominal on-orbit mission design lifetime is three years. Temperature control of the MAIA instrument is accomplished with a combination of passive radiators and heaters. The focal plane module (FPM) is cooled to ≤ 235K with a disc shaped radiator that faces the anti-sun side of the sun-synchronous orbit. The temperature of the MAIA cameras and associated electronics is controlled with a cylindrical shaped radiator that projects a near constant area in the nadir direction as the cameras rotate. A noteworthy feature of the MAIA thermal control system design is the novel, low cost, rotationally articulating thermal strap used to transfer heat from the FPMs to their associated FPM Radiator. The strap spans one of the axes of rotation, sweeping out an arc of approximately 60° as the instrument operates. A prototype of the articulating thermal strap was life tested to 260,000 cycles with no signs of significant degradation. An overview of the MAIA thermal control system baseline design is presented, with focus on its novel aspects, including life testing of the prototype articulating thermal strap. In addition, a discussion of the considerations involved in designing a thermal control system for a hosted instrument is provided.

Rosas, Rogelio↗

NASA NTRS1992

Radiometric infrared focal plane array imaging system for thermographic applications

This document describes research performed under the Radiometric Infrared Focal Plane Array Imaging System for Thermographic Applications contract. This research investigated the feasibility of using platinum silicide (PtSi) Schottky-barrier infrared focal plane arrays (IR FPAs) for NASA Langley's specific radiometric thermal imaging requirements. The initial goal of this design was to develop a high spatial resolution radiometer with an NETD of 1 percent of the temperature reading over the range of 0 to 250 C. The proposed camera design developed during this study and described in this report provides: (1) high spatial resolution (full-TV resolution); (2) high thermal dynamic range (0 to 250 C); (3) the ability to image rapid, large thermal transients utilizing electronic exposure control (commandable dynamic range of 2,500,000:1 with exposure control latency of 33 ms); (4) high uniformity (0.5 percent nonuniformity after correction); and (5) high thermal resolution (0.1 C at 25 C background and 0.5 C at 250 C background).

Esposito, B. J.↗

NASA NTRS1980

Geologic application of thermal-inertia mapping from satellite

The author has identified the following significant results. Two night-time thermal images of the Powder River Basin, Wyoming distinctly show a major thermal feature. This feature is substantially coincident with a drainage divide and the southward facing slope appears cooler, suggesting a lower thermal inertia. An initial examination of regional geologic maps provides no clear evidence to suggest what type of geologic feature or structure may be present, although it can be noted that its northeastern end passes directly through Lead, South Dakota where the Homestake Gold Mine is located.

Offield, T. W.↗

NASA NTRS1996

Robot For Infrared Mapping Of A Large Assembly In A Vacuum

Robotic system devised for use in infrared mapping of large assembly of equipment under test in vacuum chamber. Thermal images recorded from almost any direction. In original intended application, assembly thermally mapped is spacecraft, but system also used on integrated-circuit-fabrication equipment or other industrial equipment operating in vacuum. Mechanism operated in high vacuum and extreme cold.

Mcaffee, Douglas A.↗

NASA NTRS2003

High Spatial Resolution Thermal Satellite Technologies

This document in the form of viewslides, reviews various low-cost alternatives to high spatial resolution thermal satellite technologies. There exists no follow-on to Landsat 7 or ASTER high spatial resolution thermal systems. This document reviews the results of the investigation in to the use of new technologies to create a low-cost useful alternative. Three suggested technologies are examined. 1. Conventional microbolometer pushbroom modes offers potential for low cost Landsat Data Continuity Mission (LDCM) thermal or ASTER capability with at least 60-120 ground sampling distance (GSD). 2. Backscanning could produce MultiSpectral Thermal Imager performance without cooled detectors. 3. Cooled detector could produce hyperspectral thermal class system or extremely high spatial resolution class instrument.

Ryan, Robert↗

NASA NTRS2015

Real Time Fatigue Damage Growth Assessment of a Composite Three-Stringer Panel Using Passive Thermography

Fatigue testing of advanced composite structures is critical to validate both structural designs and damage prediction models. In-situ inspection methods are necessary to track damage onset and growth as a function of load cycles. Passive thermography is a large area, noncontact inspection technique that is used to detect composite damage onset and growth in real time as a function of fatigue cycles. The thermal images are acquired in synchronicity to the applied compressive load using a dual infrared camera acquisition system for full (front and back) coverage. Image processing algorithms are investigated to increase defect contrast areas. The thermal results are compared to non-immersion ultrasound inspections and acoustic emission data.

Zalameda, Joseph N.↗

NASA NTRS2004

High-speed Imaging of Global Surface Temperature Distributions on Hypersonic Ballistic-Range Projectiles

The NASA-Ames ballistic range provides a unique capability for aerothermodynamic testing of configurations in hypersonic, real-gas, free-flight environments. The facility can closely simulate conditions at any point along practically any trajectory of interest experienced by a spacecraft entering an atmosphere. Sub-scale models of blunt atmospheric entry vehicles are accelerated by a two-stage light-gas gun to speeds as high as 20 times the speed of sound to fly ballistic trajectories through an 24 m long vacuum-rated test section. The test-section pressure (effective altitude), the launch velocity of the model (flight Mach number), and the test-section working gas (planetary atmosphere) are independently variable. The model travels at hypersonic speeds through a quiescent test gas, creating a strong bow-shock wave and real-gas effects that closely match conditions achieved during actual atmospheric entry. The challenge with ballistic range experiments is to obtain quantitative surface measurements from a model traveling at hypersonic speeds. The models are relatively small (less than 3.8 cm in diameter), which limits the spatial resolution possible with surface mounted sensors. Furthermore, since the model is in flight, surface-mounted sensors require some form of on-board telemetry, which must survive the massive acceleration loads experienced during launch (up to 500,000 gravities). Finally, the model and any on-board instrumentation will be destroyed at the terminal wall of the range. For these reasons, optical measurement techniques are the most practical means of acquiring data. High-speed thermal imaging has been employed in the Ames ballistic range to measure global surface temperature distributions and to visualize the onset of transition to turbulent-flow on the forward regions of hypersonic blunt bodies. Both visible wavelength and infrared high-speed cameras are in use. The visible wavelength cameras are intensified CCD imagers capable of integration times as short as 2 ns. The infrared camera uses an Indium Antimonide (InSb) sensor in the 3 to 5 micron band and is capable of integration times as short as 500 ns. The projectiles are imaged nearly head-on using expendable mirrors offset slightly from the flight path. The proposed paper will discuss the application of high-speed digital imaging systems in the NASA-Ames hypersonic ballistic range, and the challenges encountered when applying these systems. Example images of the thermal radiation from the blunt nose of projectiles flying at nearly 14 times the speed of sound will be given.

Wilder, Michael C.↗