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At least 235 records · Page 13

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NASA NTRS1978

Response of defects to illumination in silicon solar cells

The enhancement of diffusion length with intensity was examined using spectral response measurements in solar cells based on Silso silicon and EFG silicon ribbon. Local diffusion length variations at defect sites were investigated as a function of illumination level using a scanning electron microscope operated in the electron beam induced current mode. An increase of diffusion length was observed at defect sites as the intensity level was increased. The diffusion length improvements are explained on the basis of saturation of minority carrier traps in these materials. The trap distribution in Silso silicon is shown to be peaked near (Ec - 0.7)eV. EFG silicon ribbon shows a broad, Gaussian distribution of traps located near (Ec - 0.5)eV.

Hari Rao, C. V.↗

NASA NTRS1979

Analysis of the interaction of an electron beam with a solar cell. III - The effect of spacial variations of the number density of recombination centers on SEM measurements

By means of an exactly soluble model the short circuit current generated by a scanning electron microscope in a P-N junction has been determined in cases where the trap density is inhomogeneous. The diffusion length for minority carriers becomes then dependent on the spacial coordinates. It is shown that in this case the dependence of the Isc on characteristic parameters as cell thickness, distance of the beam excitation spot from ohmic contacts, etc., becomes very intricate. This fact precludes the determination of the local diffusion length in the usual manner. Although the model is somewhat simplified in order to make it amenable to exact solutions, it is nevertheless realistic enough to lead to the conclusion that SEM measurements of bulk transport parameters in inhomogeneous semiconductor material are impractical since they may lead to serious errors in the interpretation of the data by customary means.

Von Roos, O.↗

NASA NTRS1980

Fracture modes of high modulus graphite/epoxy angleplied laminates subjected to off-axis tensile loads

Angelplied laminates of high modulus graphite fiber/epoxy were studied in several ply configurations at various tensile loading angles to the zero ply direction in order to determine the effects of ply orientations on tensile properties, fracture modes, and fracture surface characteristics of the various plies. It was found that fracture modes in the plies of angleplied laminates can be characterized by scanning electron microscope observation. The characteristics for a given fracture mode are similar to those for the same fracture mode in unidirectional specimens. However, no simple load angle range can be associated with a given fracture mode.

Sinclair, J. H.↗

NASA NTRS1979

Thermographic measurement of fatigue damage

The paper presents a thermographic technique developed to measure the extent of fatigue damage in composite materials during fatigue loading. It is noted that heat generated by cyclic loading of fatigue damaged material raises the surface temperature. These temperatures were measured with an infrared camera and were used as boundary conditions in a finite element heat transfer program, which has been developed especially to calculate the extent of the heat generation zone, and thereby to define the fatigue damage zone. It is reported that the finite element program was verified by comparing calculated heat generation with the actual heat generation for a simple heat transfer problem that had a closed form solution. Damage zones are calculated for several boron/epoxy fatigue specimens from thermograms of specimens. The calculated damage zones were compared with damage detected by C-scan, X-ray, and scanning electron microscope (SEM) examinations. It is concluded that the analysis was effective in locating the boundaries of the fatigue damage zones.

Whitcomb, J. D.↗

NASA NTRS1980

Fracture modes of high modulus graphite/epoxy angleplied laminates subjected to off-axis tensile loads

Angleplied laminates of high modulus graphite fiber/epoxy were examined in several ply configurations at various tensile loading angles to the zero ply direction to determine the effects of ply orientations on tensile properties, fracture modes, and fracture surface characteristics of the various plies. Experimental results consist of stress-strain data, selected plots, fracture stresses and strains, and scanning electron microscope (SEM) photographs of fracture surfaces. It was found that the stress-strain curves were linear to fracture, and that although fracture surface characteristics for a given fracture mode are similar to those for the same fracture mode in uniaxial specimens, no simple load angle range can be associated with a given fracture mode. It was also concluded that SEM results must be supplemented with ply stress calculations in order to identify ranges of fracture modes occurring as a function of ply orientation with respect to the load direction.

Sinclair, J. H.↗

NASA NTRS1980

Examples of realistic aerosol particles collected in a cascade impactor

In this paper some scanning electron microscope photomicrographs showing examples of a variety of particulate aerosol shapes are presented. Compositions of particles also are presented. These particles represent samples from a number of different sources and locations including: solid propellant rocket motor plumes, active volcano plumes, the lower stratosphere over Sondrestrom, Greenland, and the upper troposphere over northern Texas. The particles were collected from aboard an aircraft with a cascade impactor which classified them according to aerodynamic size into 10 size intervals ranging from submicron to greater than 25 micrometers in diameter. The cascade impactor also served to measure the mass concentration as a function of particle size. The variety of shapes and compositions found among these particles suggest difficulties in obtaining reliable size distribution data from light scattering measurements.

Woods, D. C.↗

NASA NTRS1980

Measurement of minority-carrier drift mobility in solar cells using a modulated electron beam

A determination of diffusivity on solar cells is here reported which utilizes a one dimensional treatment of diffusion under sinusoidal excitation. An intensity-modulated beam of a scanning electron microscope was used as a source of excitation. The beam was injected into the rear of the cell, and the modulated component of the induced terminal current was recovered phase sensitively. A Faraday cup to measure the modulated component of beam current was mounted next to the sample, and connected to the same electronics. A step up transformer and preamplifier were mounted on the sample holder. Beam currents on the order of 400-pA were used in order to minimize effects of high injection. The beam voltage was 34-kV, and the cell bias was kept at 0-V.

Othmer, S.↗

NASA NTRS1981

A cause of the non-solderability of ceramic capacitor terminations

The results of an analysis into the cause of the non-solderability of multiple defective part lots from two capacitor manufacturers are described. This analysis consisted of visual, scanning electron microscopic, surface, and metalographic examinations and analyses. The results indicated that non-solderability results from areas of excess porosity in the termination which are caused by segregation of ink constituents during manufacturing. This segregation can be minimized by proper monitoring and control of process variables; where excess porosity does occur, solderability can be improved by proper precleaning of parts.

Cozzolino, M. J.↗

NASA NTRS1981

The Structure and Properties of Diffusion Assisted Bonded Joints in 17-4 PH, Type 347, 15-5 PH and Nitronic 40 Stainless Steels

Diffusion assisted bonds are formed in 17-4 PH, 15-5 PH, type 347 and Nitronic 40 stainless steels using electrodeposited copper as the bonding agent. The bonds are analyzed by conventional metallographic, electron microprobe analysis, and scanning electron microscopic techniques as well as Charpy V-notch impact tests at temperatures of 77 and 300 K. Results are discussed in terms of a postulated model for the bonding process.

Wigley, D. A.↗

NASA NTRS1981

The matrices of unequilibrated ordinary chondrites - Implications for the origin and history of chondrites

The matrices of 16 unequilibrated chondrites were examined by optical microscopy, an electron microprobe, and a scanning electron microscope. The fine-grained, opaque, silicate matrix of type 3 unequilibrated chondrites was compositionally, mineralogically, and texturally different from the chondrules and their fragments; it may be the low temperature condensate proposed by Larimer and Anders (1967, 1970). Each meteorite has been metamorphosed by a combination of processes including thermal metamorphism and the passage of shock waves; the appearance of each chondrite results from the temperature and pressure conditions which formed it, and subsequent metamorphic alterations.

Huss, G. R.↗

NASA NTRS1980

Microcrack closure in rocks under stress - Direct observation

Direct observations of the closure of microcracks in rocks under increasing stress are reported. Uniaxial stresses up to 300 bars were applied to untreated and previously heated samples of Westerly granite and Frederick diabase by a small hydraulic press which fit entirely within a scanning electron microscope. Crack closure characteristics are found to depend on crack orientation, with cracks perpendicular to the applied stress closing and those parallel tending to open, as well as crack aspect ratio, crack intersection properties, stress concentrations and surface roughness. Uniaxial and hydrostatic stress measurements are found to be strongly dependent on fracture content as observed by SEM, and the observed hysteresis in strain measurements in the first stress cycles is also related to microscopic processes

Batzle, M. L.↗

NASA NTRS1981

Investigation into the role of NaCl deposited on oxide and metal substrates in the initiation of hot corrosion

Morphological aspects of the conversion to Na2SO4 of NaCl deposits over the temperature range 500-700 C, in air with added SO2 and H2O. Progress of the reaction was observed by withdrawing samples at various times and examining them under the scanning electron microscope using EDAX to assess the extent of chloride to sulfate conversion. These initial results show that the conversion to Na2SO4 proceeds directly on the sodium chloride surface as well as on the surrounding substrate due to evaporation of NaCl from the solid particle. The mechanism of this reaction could involve reaction in the vapor to produce Na2SO4 which then deposits, alternatively Na2SO4 could form directly on the substrate surface due to direct reaction there between the vapors NaCl, SO2 and O2.

Birks, N.↗

NASA NTRS1981

Effects of AP size distribution on the pressure-coupled response function

Progress in theoretical and experimental research to determine effects of AP size distribution on the pressure-coupled response function is presented. The theoretical model was based upon a preferred frequency mechanism in which ordered fluctuations in the propellant formulation, dependent upon the heterogeneity, contributed to the response. Experiments to charaterize and relate the heterogeneity to response function behavior consisted of scanning electron microscope studies and measurements of dynamic burning at constant pressure. The concept, differences between ideal models and real propellants, and results thus far obtained are discussed.

Cohen, N. S.↗

NASA NTRS1982

Compression behavior of unidirectional fibrous composite

The longitudinal compression behavior of unidirectional fiber composites is investigated using a modified Celanese test method with thick and thin test specimens. The test data obtained are interpreted using the stress/strain curves from back-to-back strain gages, examination of fracture surfaces by scanning electron microscope, and predictive equations for distinct failure modes including fiber compression failure, Euler buckling, delamination, and flexure. The results show that the longitudinal compression fracture is induced by a combination of delamination, flexure, and fiber tier breaks. No distinct fracture surface characteristics can be associated with unique failure modes. An equation is described which can be used to extract the longitudinal compression strength knowing the longitudinal tensile and flexural strengths of the same composite system.

Sinclair, J. H.↗

NASA NTRS1982

Long-term thermal degradation and alloying constituent effects on five boron/aluminum composites

Thermal exposure effects on the properties of five boron/aluminum composite systems were experimentally investigated. The composite systems were 49 volume percent boron fibers (203 micron diameter) in aluminum-alloy matrices 1100 Al, 2024 Al, 3003 Al, 5052 Al, and 6061 Al. Specimens were thermally exposed up to 10,000 hours at 500 K and 590 K, up to 500 hours at 730 K, and up to 10,000 hours at 500 K and 590 K, up to 500 hours at 730 K, and up to 2000 thermal cycles between 200 K and 590 K. Composite longitudinal and transverse tensile strengths, longitudinal compression strength, and in-plane shear strength were determined. None of the systems was severely degraded by exposure at 590 K. The best performing system was B-2024 Al. Effects of matrix alloys on degradation mechanisms were experimentally investigated. Composite specimens and individual fibers were metallurgically analyzed with a scanning electron microscope and an electron microprobe to determine failure characteristics, chemical element distribution, and reaction layer morphology. Alloying constituents were found to be affect the composite degradation mechanisms as follows: alloys containing iron, but without manganese as a stabilizer, caused increased low-temperature degradation; alloys containing magnesium, iron, or manganese caused increased degradation; and alloys containing copper caused increased fiber strength.

Olsen, G. C.↗

NASA NTRS1982

The Orthogonal In-Situ Machining of Single and Polycrystalline Aluminum and Copper, Volume 1

Metal cutting is a unique deformation process characterized by large strains, exceptionally high strain rates and few constraints to the deformation. These factors, along with the difficulty of directly measuring the shear angle, make chip formation difficult to model and understand. One technique for skirting the difficulty of post mortem chip measurement is to perform a cutting experiment dynamically in a scanning electron microscope. The performance of the in-situ experiment with full instrumentation allows for component force measurement, orientation measurement (on a round single crystal disk) and a timing device, all superimposed below the deformation on the TV monitor and recorded for future viewing. This allows the sher angle to be directly measured for the screen along with the other needed information.

Cohen, P. H.↗

NASA NTRS1982

An EBIC study of HEM polycrystalline silicon

Low-cost silicon for solar cells grown by the heat exchanger method (HEM) was studied in the electron beam induced current (EBIC) mode of a scanning electron microscope (SEM). Comparisons were made between the defects observed optically and the recombination centers visible in EBIC. Much of the HEM material was single crystalline, but structural defects were found from areas near the corners of the grown material. Most of these defects consisted of linear twin boundaries and grain boundaries. The electrical activity of these boundaries was dependent on symmetry of the boundaries. Symmetric twin boundaries did not exhibit recombination activity while unsymmetric twin boundaries were electrically active.

Koch, T.↗

NASA NTRS1981

Microscopy and microstructure of Shuttle thermal protection system materials

Examples of the contribution of microstructural analysis to the development of the Space Shuttle tile insulation system are presented, with photographic examples of the scanning electron microscope (SEM) investigations. After the basic thermal protection system materials had been selected, it was neccessary to analyze the mechanical responses of the combined materials; which included: (1) the polymer strain isolation pad (SIP), (2) the room temperature-vulcanizing silicone rubber bond, (RTV), and (3) rigid ceramic fiber reusable surface insulation (RSI). Microstructural analysis was used to provide information on deformation and fracture mechanisms, load transfer mechanisms, and structural alterations occurring before final failure. Both quantitative and qualitative information was obtained in the open, three-dimensional fibrous structures of the ceramic tiles by means of novel techniques of encapsulation and dissolution.

Newquist, C. W.↗